3,5-Bis(trifluoromethyl)benzylamine
- Product Name
- 3,5-Bis(trifluoromethyl)benzylamine
- CAS No.
- 85068-29-7
- Chemical Name
- 3,5-Bis(trifluoromethyl)benzylamine
- Synonyms
- MBT-BYM;TIMTEC-BB SBB000829;RARECHEM AL BW 0137;3,5-DI(TRIFLUOROMETHYL)BENZYLAMINE;3,5-Bis(TrifluroMethyl)BenzylAmine;3,5-BIS(TRIFLUOROMETHYL)BENZYLAMINE;3,5-Bis(trifluoromethyl)benzylamine95%;3,5-Bis(trifluoromethyl)benzylamine 95%;(3,5-Bis(trifluoromethyl)phenyl)methamine;3,5-Bis(trifluoromethyl)benzenemethanamine
- CBNumber
- CB8350048
- Molecular Formula
- C9H7F6N
- Formula Weight
- 243.15
- MOL File
- 85068-29-7.mol
3,5-Bis(trifluoromethyl)benzylamine Property
- Melting point:
- 50-55 °C(lit.)
- Boiling point:
- 82-84 °C (15 mmHg)
- Density
- 1.3653 (estimate)
- Flash point:
- 173 °F
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- solubility
- soluble in Methanol
- form
- Crystalline Mass, Powder, Crystals and/or Chunks
- pka
- 8.32±0.10(Predicted)
- color
- White to beige
- Sensitive
- Air Sensitive
- BRN
- 7209267
- CAS DataBase Reference
- 85068-29-7(CAS DataBase Reference)
Safety
- Hazard Codes
- C
- Risk Statements
- 34-21/22
- Safety Statements
- 26-36/37/39-45
- RIDADR
- UN 3259 8/PG 2
- WGK Germany
- 3
- F
- 10-34
- Hazard Note
- Corrosive
- HazardClass
- 8
- PackingGroup
- III
- HS Code
- 29214990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P363Wash contaminated clothing before reuse.
N-Bromosuccinimide Price
- Product number
- 263389
- Product name
- 3,5-Bis(trifluoromethyl)benzylamine
- Purity
- technical grade, 80%
- Packaging
- 1g
- Price
- $26.8
- Updated
- 2025/07/31
- Product number
- 263389
- Product name
- 3,5-Bis(trifluoromethyl)benzylamine
- Purity
- technical grade, 80%
- Packaging
- 5g
- Price
- $32.58
- Updated
- 2025/07/31
- Product number
- B2949
- Product name
- 3,5-Bis(trifluoromethyl)benzylamine
- Packaging
- 1G
- Price
- $34
- Updated
- 2025/07/31
- Product number
- B2949
- Product name
- 3,5-Bis(trifluoromethyl)benzylamine
- Packaging
- 5G
- Price
- $116
- Updated
- 2025/07/31
- Product number
- 005828
- Product name
- 3,5-Bis(trifluoromethyl)benzylamine
- Purity
- 97%
- Packaging
- 100g
- Price
- $425
- Updated
- 2021/12/16
3,5-Bis(trifluoromethyl)benzylamine Chemical Properties,Usage,Production
Chemical Properties
Colorless to light yellow liqui
Uses
3,5-bis(Trifluoromethyl)benzylamine is used in preparation of nitrile by catalytic oxidation of amines.
Synthesis
401-95-6
85068-29-7
The general procedure for the synthesis of 3,5-bis(trifluoromethyl)benzenemethanamine from 3,5-bis(trifluoromethyl)benzaldehyde was as follows: to a 300 mL autoclave was added 145.3 g (0.60 mol) of 3,5-bis(trifluoromethyl)benzenemethanaldehyde and 60 mL of cooled ethanol solution containing 10.3 g (0.60 mol) of liquid ammonia, followed by the addition of 2 g of nickel ruanide. The mixture was heated to 40 °C and the reaction was stirred under hydrogen pressure (9 MPa) for 1 hour. The temperature was then raised to 70 °C and the reaction was continued for 30 min. Upon completion of the reaction, the reaction product solution was drained and filtered to remove the catalyst. Analysis of the reaction solution by gas chromatography confirmed the formation of 128.9 g (0.53 mol) of 3,5-bis(trifluoromethyl)benzylamine in 89% yield and 93% selectivity. 124.0 g (0.51 mol) of 3,5-bis(trifluoromethyl)benzylamine was isolated by vacuum distillation in 85% yield, and the purity determined by gas chromatography was ≥99%.The results of ICP analysis of the total elements showed that Li, Na, K, Mg, Ca, Sr, Ba, Sc, Y, Ti, Zr, V, Nb, Cr, Mo, W, Mn, Fe, Ru, Co were not detected; Rh, Ni, Pd, Pt, Cu, Ag, Au, Zn, Cd, Al, In, Si, Sn, Pb, P, Sb, and S were detected, and the contents of group 1 and group 2 elements were ≤1 ppm.
References
[1] Patent: EP1500641, 2005, A1. Location in patent: Page 12
3,5-Bis(trifluoromethyl)benzylamine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-Bis(trifluoromethyl)benzylamine manufacturers
- Product
- 3,5-Bis(trifluoromethyl)benzylamine 85068-29-7
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2020-01-10