ChemicalBook > CAS DataBase List > 2,6-Dichloronitrobenzene

2,6-Dichloronitrobenzene

Product Name
2,6-Dichloronitrobenzene
CAS No.
601-88-7
Chemical Name
2,6-Dichloronitrobenzene
Synonyms
2,6-Dichloronitrobenzene;2,6-Dichloronitrobenezene;1-Nitro-2,6-dichlorobenzene;Benzene, 1,3-dichloronitro-;1,3-Dichloro-2-nitrobenzene;1,3-DICHLORO-3-NITROBENZENE;Benzene, 1,3-dichloro-2-nitro-;1,3-Dichloro-2-nitrobenzene>TIANFUCHEM--High purity 2,6-Dichloronitrobenzene factory price
CBNumber
CB8500733
Molecular Formula
C6H3Cl2NO2
Formula Weight
192
MOL File
601-88-7.mol
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2,6-Dichloronitrobenzene Property

Melting point:
71 °C
Boiling point:
130 °C / 8mmHg
Density 
1.6030
refractive index 
1.5929 (estimate)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
form 
Solid
color 
Pale Yellow to Pale Green
CAS DataBase Reference
601-88-7(CAS DataBase Reference)
NIST Chemistry Reference
1,3-dichloro-2-nitrobenzene(601-88-7)
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Safety

Hazard Codes 
T
RIDADR 
1578
HS Code 
2904990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
D3449
Product name
1,3-Dichloro-2-nitrobenzene
Purity
>98.0%(GC)
Packaging
25g
Price
$88
Updated
2025/07/31
TRC
Product number
D438275
Product name
1,3-Dichloro-2-nitrobenzene
Packaging
5g
Price
$50
Updated
2021/12/16
AK Scientific
Product number
F887
Product name
2,6-Dichloronitrobenzene
Packaging
25g
Price
$54
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-5-Z7
Product name
2,6-Dichloronitrobenzene
Packaging
25g
Price
$44
Updated
2021/12/16
ChemScene
Product number
CS-W007920
Product name
1,3-Dichloro-2-nitrobenzene
Purity
99.55%
Packaging
100g
Price
$100
Updated
2021/12/16
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2,6-Dichloronitrobenzene Chemical Properties,Usage,Production

Uses

1,3-Dichloro-2-nitrobenzene is an olfactory mucosa (OM) toxicants.Also, it is a starting material for 9-Chloro Quetiapine (C366040), which is an impurity of Quetiapine hemifumarate (Q510000), a dibenzothiazepine antipsychotic medication used in the treatment of schizophrenia.

Synthesis

608-31-1

601-88-7

2.1.5. Synthesis of 1,3-dichloro-2-nitrobenzene[4]. 2,6-Dichloroaniline (8.10 g, 50.0 mmol) was dissolved in dichloromethane (200 mL) and the solution was cooled to 0 °C. A solution of 3-chloroperbenzoic acid (24.6 g, 100 mmol) in dichloromethane (250 mL) was slowly added dropwise at 0 °C for a controlled time of 1.5 hours. After the dropwise addition, the reaction mixture was continued to be stirred at room temperature for 2 hours. Subsequently, the reaction mixture was diluted with dichloromethane (250 mL). The reaction mixture was washed sequentially with 2 wt% aqueous sodium thiosulfate (2 x 100 mL), aqueous sodium bicarbonate (4 x 50 mL) and deionized water (200 mL). The organic layer was dried with magnesium sulfate and concentrated under reduced pressure to remove the solvent. The residue was suspended in n-hexane (40 mL), sonicated for 5 min and filtered, and the filter cake was washed with n-hexane (2 x 20 mL) to afford 1,3-dichloro-2-nitrobenzene (6.63 g, 37.7 mmol, 75% yield) as a beige solid.

References

[1] Patent: US2014/163256, 2014, A1. Location in patent: Paragraph 0161-0162
[2] Tetrahedron Letters, 1983, vol. 24, # 14, p. 1505 - 1508
[3] Tetrahedron, 1987, vol. 43, # 8, p. 1753 - 1758
[4] Beilstein Journal of Organic Chemistry, 2017, vol. 13, p. 768 - 778
[5] Journal of Medicinal Chemistry, 1968, vol. 11, # 4, p. 814 - 819

2,6-Dichloronitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2,6-Dichloronitrobenzene manufacturers

Honest Joy Holdings Limited
Product
2,6-Dichloronitrobenzene 601-88-7
Price
US $0.00/KG
Min. Order
1KG
Purity
97.6%
Supply Ability
100 tons
Release date
2022-02-20
Career Henan Chemical Co
Product
2,6-Dichloronitrobenzene 601-88-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-12

601-88-7, 2,6-DichloronitrobenzeneRelated Search:

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