1-Hydroxymethylbenzocyclobutene

Product Name: 1-Hydroxymethylbenzocyclobutene
CAS No.: 15100-35-3
Chemical Name: 1-Hydroxymethylbenzocyclobutene
Synonyms: 1-Benzocyclobutenmethanol;1-Hydroxymethyl-benzocyclobuten;1-hydroxymethylbenzocyclobutene;Bicyclo[4.2.0]octa-1,3,5-triene-7-m;7-bicyclo[4.2.0]octa-1,3,5-trienylmethanol;Bicyclo[4.2.0]octa-1,3,5-triene-7-methanol;Bicyclo[4.2.0]octa-1,3,5-trien-7-ylmethanol;Bicyclo[4.2.0]octa-1,3,5,7-tetraen-7-ylMethanol;7-bicyclo[4.2.0]octa-1(8),2,4,6-tetraenylmethanol;1-Hydroxymethylbenzocyclobutene ISO 9001：2015 REACH
CBNumber: CB8966416
Molecular Formula: C9H10O
Formula Weight: 134.18
MOL File: 15100-35-3.mol

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1-Hydroxymethylbenzocyclobutene Property

Boiling point:: 249.4±9.0 °C(Predicted)
Density: 1.124±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.77±0.10(Predicted)

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Safety

HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: API0004893
Product name: 1-HYDROXYMETHYLBENZOCYCLOBUTENE
Purity: 95.00%
Packaging: 1G
Price: $584.85
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: API0004893
Product name: 1-HYDROXYMETHYLBENZOCYCLOBUTENE
Purity: 95.00%
Packaging: 5G
Price: $909.56
Updated: 2021/12/16

AccelPharmtech

Product number: C1488
Product name: 1-hydroxymethylbenzocyclobutene
Purity: 97.00%
Packaging: 1G
Price: $2070
Updated: 2021/12/16

AHH

Product number: MB-18178
Product name: 1-HYDROXYMETHYLBENZOCYCLOBUTENE
Purity: 97%
Packaging: 10g
Price: $2100
Updated: 2021/12/16

AccelPharmtech

Product number: C1488
Product name: 1-hydroxymethylbenzocyclobutene
Purity: 97.00%
Packaging: 5G
Price: $2330
Updated: 2021/12/16

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1-Hydroxymethylbenzocyclobutene Chemical Properties,Usage,Production

Synthesis

163222-89-7

15100-35-3

Step A: Borane-THF solution (1M, 4 mL, 1.2 equiv) was slowly added dropwise to a solution of bicyclo[4.2.0]octa-1,3,5-triene-7-carboxylic acid (500 mg, 3.38 mmol) in THF (6 mL) at 0 °C. The reaction mixture was gradually warmed to room temperature and stirred overnight. Upon completion of the reaction, the reaction was quenched with water, the organic phase was extracted with EtOAc and dried with anhydrous MgSO4. Purification by silica gel column chromatography (eluent: 5-20% EtOAc/hexane gradient) afforded bicyclo[4.2.0]octa-1,3,5-trien-7-ylmethanol (388 mg, 86% yield).

References

[1] Patent: US2016/31875, 2016, A1. Location in patent: Paragraph 0276; 0277
[2] Journal of Medicinal Chemistry, 1965, vol. 8, p. 255 - 257

1-Hydroxymethylbenzocyclobutene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Hydroxymethylbenzocyclobutene Suppliers

China 57 Germany 2 India 2 Switzerland 1 United States 5 Global 67

Beijing Ouhe Technology Co., Ltd

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Shijiazhuang Sdyano Fine Chemical Co., Ltd.

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Amadis Chemical Company Limited

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View Lastest Price from 1-Hydroxymethylbenzocyclobutene manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 1-Hydroxymethylbenzocyclobutene 15100-35-3
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-09-19

Henan Fengda Chemical Co., Ltd

Product: 1-Hydroxymethylbenzocyclobutene 15100-35-3
Price: US $5.00-0.50/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-13

Career Henan Chemical Co

Product: 1-Hydroxymethylbenzocyclobutene 15100-35-3
Price: US $7.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2018-12-14

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1-hydroxymethylbenzocyclobutene

Bicyclo[4.2.0]octa-1,3,5,7-tetraen-7-ylMethanol

1-HMBCB 1-hydroxymethy lbenzocyclobutene

Bicyclo[4.2.0]octa-1,3,5-trien-7-ylmethanol

Bicyclo[4.2.0]octa-1,3,5-triene-7-methanol

Bicyclo[4.2.0]octa-1,3,5-triene-7-m

7-bicyclo[4.2.0]octa-1,3,5-trienylmethanol

7-bicyclo[4.2.0]octa-1(8),2,4,6-tetraenylmethanol

1-Hydroxymethylbenzocyclobutene ISO 9001：2015 REACH

1-Benzocyclobutenmethanol

1-Hydroxymethyl-benzocyclobuten

15100-35-3