2-Pyridinecarboxamide,5-fluoro-(9CI)
- Product Name
- 2-Pyridinecarboxamide,5-fluoro-(9CI)
- CAS No.
- 499796-71-3
- Chemical Name
- 2-Pyridinecarboxamide,5-fluoro-(9CI)
- Synonyms
- 5-fluoropicolinaMide;5-Fluoro-2-pyridinecarboxaMide;2-PyridinecarboxaMide, 5-fluoro;2-Pyridinecarboxamide,5-fluoro-(9CI)
- CBNumber
- CB91271084
- Molecular Formula
- C6H5FN2O
- Formula Weight
- 140.12
- MOL File
- 499796-71-3.mol
2-Pyridinecarboxamide,5-fluoro-(9CI) Property
- Boiling point:
- 272.9±25.0 °C(Predicted)
- Density
- 1.327±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 15.00±0.50(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
N-Bromosuccinimide Price
- Product number
- F621508
- Product name
- 5-Fluoropicolinamide
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- F621508
- Product name
- 5-Fluoropicolinamide
- Packaging
- 100mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- PC408426
- Product name
- 5-Fluoro-2-pyridinecarboxamide
- Packaging
- 1g
- Price
- $78
- Updated
- 2021/12/16
- Product number
- 6778AB
- Product name
- 5-Fluoropicolinamide
- Packaging
- 5g
- Price
- $172
- Updated
- 2021/12/16
- Product number
- 4H48-3-3E
- Product name
- 5-Fluoro-2-pyridinecarboxamide
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
2-Pyridinecarboxamide,5-fluoro-(9CI) Chemical Properties,Usage,Production
Synthesis
717871-83-5
499796-71-3
A solution of tetrahydrofuran (THF, 40 mL) of 5-fluoro-2-pyridinecarbonyl chloride (2.30 g, 14.4 mmol, 1.00 eq.) was slowly added dropwise to a stirred saturated ammonium hydroxide solution (40 mL) at 0 °C. The reaction mixture was stirred continuously at 10 °C for 30 min. Subsequently, the solvent was removed by distillation under reduced pressure. The residue was dissolved in dichloromethane (30 mL) and washed with saturated saline (2 x 30 mL). The organic phase was dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give 1.82 g of 5-fluoro-2-pyridine carboxamide as a yellow solid in 71% yield. Mass spectrum (electrospray ionization, m/z): 140.9 ([M+H]+).
References
[1] Patent: WO2015/51479, 2015, A1. Location in patent: Page/Page column 65; 66
[2] Patent: WO2015/54038, 2015, A1. Location in patent: Page/Page column 57; 65; 66
2-Pyridinecarboxamide,5-fluoro-(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Pyridinecarboxamide,5-fluoro-(9CI) manufacturers
- Product
- 2-Pyridinecarboxamide,5-fluoro-(9CI) 499796-71-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2019-07-11