ChemicalBook > CAS DataBase List > 3-Iodo-2-methoxypyridine

3-Iodo-2-methoxypyridine

Product Name
3-Iodo-2-methoxypyridine
CAS No.
112197-15-6
Chemical Name
3-Iodo-2-methoxypyridine
Synonyms
2-METHOXY-3-IODOPYRIDINE;3-IODO-2-METHOXYPYRIDINE;5-Iodo-2-Methoxypyridinne;Anhydrous lithium acetate;Pyridine,3-iodo-2-Methoxy-;3-Iodo-2-methoxypyridine>3-IODO-2-METHOXYPYRIDINE 99%;3-Iodo-2-methoxypyridine,96%;3-Iodo-2-Methoxypyridine, 97+%;2-Amino-3-bromo-6-nitropyridine
CBNumber
CB9175624
Molecular Formula
C6H6INO
Formula Weight
235.02
MOL File
112197-15-6.mol
More
Less

3-Iodo-2-methoxypyridine Property

Melting point:
66 °C(Solv: hexane (110-54-3))
Boiling point:
131-133 °C (43 mmHg)
Density 
1.831 g/mL at 25 °C
refractive index 
1.617-1.619
Flash point:
>110℃
storage temp. 
2-8°C
pka
1.38±0.10(Predicted)
form 
clear liquid
color 
Light yellow to Brown
Sensitive 
Light Sensitive
InChI
InChI=1S/C6H6INO/c1-9-6-5(7)3-2-4-8-6/h2-4H,1H3
InChIKey
BXCHJERCAUZLOE-UHFFFAOYSA-N
SMILES
C1(OC)=NC=CC=C1I
CAS DataBase Reference
112197-15-6(CAS DataBase Reference)
More
Less

Safety

Hazard Codes 
Xn,Xi
Risk Statements 
36/37/38-20/21/22-41-37/38-22-36/37/39
Safety Statements 
36/37/39-26-37
RIDADR 
UN 3334
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29339900
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
692816
Product name
3-Iodo-2-methoxypyridine
Purity
97%
Packaging
1g
Price
$49.8
Updated
2023/06/20
TCI Chemical
Product number
I0924
Product name
3-Iodo-2-methoxypyridine
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$39
Updated
2025/07/31
TCI Chemical
Product number
I0924
Product name
3-Iodo-2-methoxypyridine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$143
Updated
2025/07/31
TRC
Product number
I737070
Product name
3-Iodo-2-methoxypyridine
Packaging
10mg
Price
$45
Updated
2021/12/16
Matrix Scientific
Product number
016060
Product name
3-Iodo-2-methoxy-pyridine
Packaging
500mg
Price
$90
Updated
2021/12/16
More
Less

3-Iodo-2-methoxypyridine Chemical Properties,Usage,Production

Chemical Properties

Light yellow Cryst

Synthesis

1628-89-3

112197-15-6

The general procedure for the synthesis of 3-iodo-2-methoxypyridine using 2-methoxypyridine as starting material was as follows: firstly, [Li(TMP)Zn(tBu)2] was prepared in 0.4 mmol scale THF solution according to the literature method. To this solution, 2-methoxypyridine (0.042 mL, 0.4 mmol) was added and the reaction mixture was stirred at room temperature for 2 h to obtain a light orange solution. Subsequently, the solution was cooled to 0°C and the reaction was quenched with I2 (508 mg, dissolved in 1 mL THF) and stirring was continued for 1 hour. Upon completion of the reaction, 10% Na2S2O3 solution was added until the solution was bleached and the product was extracted with DCM (3 x 1 mL). The organic phases were combined, dried with MgSO4 and concentrated under reduced pressure to remove the solvent. The residue was purified by silica gel column chromatography using heptane:DCM (20:80→40:60) as eluent to afford 3-iodo-2-methoxypyridine (2a) as a colorless oil (87.1 mg, 92% yield).1H NMR (400 MHz, CDCl3) δ ppm 4.00 (s, 3H), 6.65 (dd, J = 7.61, 4.88 Hz, 1H), 8.03 (dd, J = 7.61, 1.76 Hz, 1H), 8.13 (dd, J = 4.88, 1.76 Hz, 1H). The data obtained are in agreement with literature reports.

References

[1] Tetrahedron, 2016, vol. 72, # 17, p. 2196 - 2205
[2] Tetrahedron Letters, 2011, vol. 52, # 36, p. 4590 - 4594
[3] Journal of the American Chemical Society, 2004, vol. 126, # 34, p. 10526 - 10527
[4] Journal of the American Chemical Society, 2007, vol. 129, # 7, p. 1921 - 1930
[5] Chemical Communications, 2014, vol. 50, # 85, p. 12859 - 12862

3-Iodo-2-methoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

3-Iodo-2-methoxypyridine Suppliers

Americas 1 China 167 Europe 3 France 1 Germany 4 India 5 Japan 1 Poland 1 United Kingdom 4 United States 32 Global 219
Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
Accela ChemBio Inc.
Tel
+1(858) 699-3322
Fax
+1(858) 876-1948
Email
marketing@accelachem.com
Country
United States
ProdList
6024
Advantage
65
AbaChemScene
Tel
732-484-9848
Fax
888-484-5008
Email
sales@chemscene.com
Country
United States
ProdList
3982
Advantage
60
Accela ChemBio Inc.
Tel
+1-858-6993322
Fax
(+1)-858-876-1948
Email
info@accelachem.com
Country
United States
ProdList
21193
Advantage
58
Alchem Pharmtech,Inc.
Tel
8485655694
Email
sales@alchempharmtech.com
Country
United States
ProdList
63687
Advantage
58
Aladdin Scientific
Tel
Email
tp@aladdinsci.com
Country
United States
ProdList
57505
Advantage
58
Synthonix Inc
Tel
--
Fax
--
Email
info@synthonix.com
Country
United States
ProdList
6872
Advantage
58
Rosewell Industry Co., Ltd.
Tel
--
Fax
--
Email
synbiochem@gmail.com
Country
United States
ProdList
310
Advantage
0
AlliChem, LLC
Tel
--
Fax
--
Email
sales@allichemllc.com
Country
United States
ProdList
6516
Advantage
60
Waterstone Technology, LLC
Tel
--
Fax
--
Email
sales@waterstonetech.com
Country
United States
ProdList
6786
Advantage
30
AOBChem
Tel
--
Fax
--
Email
sales@aobchem.com
Country
United States
ProdList
885
Advantage
58
Alichem Inc.
Tel
--
Fax
--
Email
sales@alichem.com
Country
United States
ProdList
6167
Advantage
58
OChem Incorporation
Tel
--
Fax
--
Email
sales@ocheminc.com
Country
United States
ProdList
6501
Advantage
60
SynQuest Laboratories, Inc.
Tel
--
Fax
--
Email
info@synquestlabs.com
Country
United States
ProdList
6871
Advantage
62
Riedel-de Haen AG
Tel
--
Fax
--
Country
United States
ProdList
6773
Advantage
87
TCI America
Tel
--
Fax
--
Email
sales@tciamerica.com
Country
United States
ProdList
6909
Advantage
75
Frontier Scientific, Inc.
Tel
--
Fax
--
Email
sales@frontiersci.com
Country
United States
ProdList
6222
Advantage
86
Matrix Scientific
Tel
--
Fax
--
Email
sales@matrixscientific.com
Country
United States
ProdList
6632
Advantage
80
AOBChem USA
Tel
--
Fax
--
Email
sales@aobchem.com
Country
United States
ProdList
3487
Advantage
50
Oakwood Products, Inc.
Tel
--
Fax
--
Email
sales@oakwoodchemical.com
Country
United States
ProdList
6193
Advantage
74
NOVASYN ORGANICS PVT LTD
Tel
--
Fax
--
Email
info@novasynorganics.com
Country
United States
ProdList
1316
Advantage
55
Alfa Aesar
Tel
--
Fax
--
Email
tech@alfa.com
Country
United States
ProdList
6814
Advantage
81
Chem-Impex International, Inc.
Tel
--
Fax
--
Country
United States
ProdList
6730
Advantage
64
Adesis, Inc.
Tel
--
Fax
--
Email
info@adesisinc.com
Country
United States
ProdList
512
Advantage
64
HONEST JOY HOLDINGS LIMITED
Tel
--
Fax
--
Email
sales@honestjoy.cn
Country
United States
ProdList
6675
Advantage
54
AK Scientific, Inc.
Tel
--
Fax
--
Email
sales@aksci.com
Country
United States
ProdList
6347
Advantage
65
APAC Pharmaceutical, LLC
Tel
--
Fax
--
Email
sales@apacpharma.com
Country
United States
ProdList
6322
Advantage
38
ASDI Incorporated
Tel
--
Fax
--
Email
customerservice@asdi.net
Country
United States
ProdList
6922
Advantage
67
J & W PharmLab, LLC
Tel
--
Fax
--
Email
services@jwpharmlab.com
Country
United States
ProdList
4156
Advantage
63
Atlantic SciTech Group, Inc.
Tel
--
Fax
--
Email
sales@astginc.com
Country
United States
ProdList
2308
Advantage
43
ChemPacific Corporation
Tel
--
Fax
--
Email
sales@chempacific.com
Country
United States
ProdList
6891
Advantage
51
Asymchem Laboratories, Inc.
Tel
--
Fax
--
Email
info@asymchem.com
Country
United States
ProdList
1315
Advantage
69
More
Less

View Lastest Price from 3-Iodo-2-methoxypyridine manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
3-Iodo-2-methoxypyridine 112197-15-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10000KGS
Release date
2025-06-03
Henan Fengda Chemical Co., Ltd
Product
3-Iodo-2-methoxypyridine 112197-15-6
Price
US $5.00-0.10/KG
Min. Order
1KG
Purity
98%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-08
Hebei Zhanyao Biotechnology Co. Ltd
Product
3-Iodo-2-methoxypyridine 112197-15-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 Tons
Release date
2021-10-18

112197-15-6, 3-Iodo-2-methoxypyridineRelated Search:

4-Methoxybenzylchloride 4-Methoxyphenylacetic acid 4-Methoxyphenylacetone (Trifluoromethoxy)benzene Anisole 2-Methoxypyridine 3-(METHOXYMETHOXY)BENZALDEHYDE p-Anisidine p-Anisaldehyde 3-BROMO-5-CHLORO-2-METHOXY-PYRIDINE 3-BROMO-2-METHOXY-6-PICOLINE 3-BROMO-5-FLUORO-2-METHOXYPYRIDINE 5-AMINO-3-BROMO-2-METHOXYPYRIDINE 2-Methoxy-3-nitropyridine 5-BROMO-2-METHOXY-3-NITRO-PYRIDINE 5-AMINO-2-METHOXY-3-METHYLPYRIDINE HCL 2-Methoxy-3-fluoro-5-bromopyridine 6-Chloro-2-methoxy-3-nitropyridine

  • 3-IODO-2-METHOXYPYRIDINE
  • 3-Iodo-2-Methoxypyridine, 97+%
  • 2-METHOXY-3-IODOPYRIDINE
  • 3-Iodo-2-methoxypyridine,96%
  • 3-IODO-2-METHOXYPYRIDINE 99%
  • Pyridine,3-iodo-2-Methoxy-
  • 3-Iodo-2-methoxypyridine&gt
  • 2-Amino-3-bromo-6-nitropyridine
  • Anhydrous lithium acetate
  • 5-Iodo-2-Methoxypyridinne
  • 112197-15-6
  • C6H6INO
  • alkyl Iodine
  • Pyridines
  • Pyridine
  • Furans