ChemicalBook > CAS DataBase List > Dimethyl 5-nitroisophthalate
Dimethyl 5-nitroisophthalate
Uses- Product Name
- Dimethyl 5-nitroisophthalate
- CAS No.
- 13290-96-5
- Chemical Name
- Dimethyl 5-nitroisophthalate
- Synonyms
- 5-NITROISOPHTHALIC ACID DIMETHYL ESTER;Dimethyl- 5–Nitroisophathalate;5-NIPA-DME;Iohexol Impurity R;Dimethyl-5-nitrophthalate;DIMETHYLNITROISOPHTHALATE-5;Dimethyl-5itroisophathalate;DIMETHYL 5-NITROISOPHTHALATE;Dimethyl5-Nitromisophthalate;5-NITRO DIMETHYL ISOPHTHALATE
- CBNumber
- CB9205602
- Molecular Formula
- C10H9NO6
- Formula Weight
- 239.18
- MOL File
- 13290-96-5.mol
More
Less
Dimethyl 5-nitroisophthalate Property
- Melting point:
- 123-125 °C (lit.)
- Boiling point:
- 381.83°C (rough estimate)
- Density
- 1.4504 (rough estimate)
- refractive index
- 1.5310 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Light yellow
- BRN
- 2140916
- InChI
- InChI=1S/C10H9NO6/c1-16-9(12)6-3-7(10(13)17-2)5-8(4-6)11(14)15/h3-5H,1-2H3
- InChIKey
- GGTSJKFPGKFLCZ-UHFFFAOYSA-N
- SMILES
- C1(C(OC)=O)=CC([N+]([O-])=O)=CC(C(OC)=O)=C1
- CAS DataBase Reference
- 13290-96-5(CAS DataBase Reference)
- NIST Chemistry Reference
- 1,3-Benzenedicarboxylic acid, 5-nitro-, dimethyl ester(13290-96-5)
- EPA Substance Registry System
- Dimethyl 5-nitroisophthalate (13290-96-5)
More
Less
Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22
- Safety Statements
- 22-24/25-36
- RIDADR
- UN 2811
- WGK Germany
- 2
- RTECS
- CZ4340000
- TSCA
- Yes
- HS Code
- 29173990
More
Less
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
More
Less
N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 237361
- Product name
- Dimethyl 5-nitroisophthalate
- Purity
- 98%
- Packaging
- 25g
- Price
- $34.6
- Updated
- 2023/06/20
TCI Chemical
- Product number
- N0567
- Product name
- Dimethyl 5-Nitroisophthalate
- Packaging
- 25g
- Price
- $27
- Updated
- 2025/07/31
TCI Chemical
- Product number
- N0567
- Product name
- Dimethyl 5-Nitroisophthalate
- Packaging
- 500g
- Price
- $181
- Updated
- 2025/07/31
TRC
- Product number
- D480553
- Product name
- Dimethyl 5-nitroisophthalate
- Packaging
- 50g
- Price
- $75
- Updated
- 2021/12/16
Apolloscientific
- Product number
- OR18375
- Product name
- Dimethyl 5-nitroisophthalate
- Purity
- 98+%
- Packaging
- 100g
- Price
- $22
- Updated
- 2021/12/16
More
Less
Dimethyl 5-nitroisophthalate Chemical Properties,Usage,Production
Uses
Dimethyl 5-Nitroisophthalate is a useful chemical in organic synthesis.
Chemical Properties
slightly yellow fine crystalline powder
Uses
Dimethyl 5-nitroisophthalate has been used as starting reagent in the synthesis of 5-nitro-1,3-bis(ethylenediamine) and 5-nitroisophthaldihydrazide.
Synthesis
67-56-1
618-88-2
13290-96-5
In a 100 mL three-necked round-bottomed flask equipped with a condenser tube, an electric stirrer and a thermometer, 5.0 g of 5-nitroisophthalic acid and 33.3 mL of methanol were added sequentially. The mixture was stirred under nitrogen protection at room temperature for about 3 minutes until the solid was completely dissolved to give a colorless transparent solution. Subsequently, 1.0 mL of concentrated sulfuric acid was slowly added dropwise and heated to reflux, and after the reaction for about 3 hours, white solid precipitation was observed. The progress of the reaction was monitored by thin layer chromatography (TLC, unfolding agent ratio of dichloromethane:methanol=10:1). Upon completion of the reaction, it was cooled to room temperature, crystals were precipitated and the solid product was collected by filtration. The filter cake was washed with deionized water and finally mixed with a small amount of water and dried to obtain dimethyl 5-nitroisophthalate. The product yield was 98%.
References
[1] Patent: CN105254521, 2016, A. Location in patent: Paragraph 0025
[2] Journal of the Chemical Society, 1905, vol. 87, p. 1265
[3] Journal fuer Praktische Chemie (Leipzig), 1882, vol. <2> 25, p. 491
[4] Patent: US2005/281746, 2005, A1. Location in patent: Page/Page column 15-16
Dimethyl 5-nitroisophthalate Preparation Products And Raw materials
Raw materials
Preparation Products
More
Less
Dimethyl 5-nitroisophthalate Suppliers
- Tel
- 18072846723 18072846723
- 2493446488@qq.com
- Country
- China
- ProdList
- 568
- Advantage
- 58
- Tel
- 021-50182298 021-50180596
- Fax
- +86-21-57758967
- sales@boylechem.com
- Country
- China
- ProdList
- 2208
- Advantage
- 55
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 4006356688 18621169109
- Fax
- 86-21-61259102
- market03@meryer.com
- Country
- China
- ProdList
- 40228
- Advantage
- 62
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 010-010-82967028 13522913783
- Fax
- +86-10-82967029
- 2355560935@qq.com
- Country
- China
- ProdList
- 12000
- Advantage
- 60
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9309
- Advantage
- 66
- Tel
- 0576-88221739
- Fax
- +86 (576) 88811295
- sales@haizhoupharm.com
- Country
- China
- ProdList
- 44
- Advantage
- 60
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11035
- Advantage
- 64
- Tel
- 021-58099652-8005 13585536065
- Fax
- 021-58099609
- bin.wu@shlschem.com
- Country
- China
- ProdList
- 9883
- Advantage
- 59
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- 15527621225
- 1791901229@qq.com
- Country
- China
- ProdList
- 6945
- Advantage
- 52
- Tel
- 010-82954736 13391601435
- sales@isomersyn.com
- Country
- China
- ProdList
- 3295
- Advantage
- 57
- Tel
- 4009903999 13355009207
- Fax
- 0539-6365991
- 3007715519@qq.com
- Country
- China
- ProdList
- 18729
- Advantage
- 57
- Tel
- 0086-21-58956006
- Fax
- 0086-21-58956100
- Country
- China
- ProdList
- 7811
- Advantage
- 57
- Tel
- 400-188-0725 +86 21 34310725 13611771617
- Fax
- +86 21 34311076
- Country
- China
- ProdList
- 2002
- Advantage
- 57
- Tel
- 400 638 7771
- sales@heowns.com
- Country
- China
- ProdList
- 14435
- Advantage
- 57
- Tel
- 86-21-63210123
- Fax
- 86-21-63290778 86-21-63218885
- sj_scrc@sinopharm.com
- Country
- China
- ProdList
- 9815
- Advantage
- 79
- Tel
- 027-85736489
- Fax
- 86-27-85736485
- info@kemiworks.net
- Country
- China
- ProdList
- 540
- Advantage
- 57
- Tel
- 0731-85526065 13308475853
- ivy@hnhbsj.com
- Country
- China
- ProdList
- 7247
- Advantage
- 62
- Tel
- +86 (573) 82222445 (0)18006601000 452520369
- Fax
- +86 (573) 82222643
- sales@maya-r.com
- Country
- China
- ProdList
- 11707
- Advantage
- 57
- Tel
- 021-56491756 13512199871
- Fax
- 021-5649-1756
- 2819742715@qq.com
- Country
- China
- ProdList
- 3997
- Advantage
- 55
- Tel
- 86-21-34053660
- Fax
- 86-21-34053661
- sale@labgogo.com
- Country
- China
- ProdList
- 9865
- Advantage
- 52
- Tel
- +86-21-60341587
- Fax
- +86-21-61294319
- sales@topbiochem.com
- Country
- China
- ProdList
- 6175
- Advantage
- 58
- Tel
- 86-21-62506791
- Fax
- 86-21-63636419
- record@recordpharm.com
- Country
- China
- ProdList
- 38
- Advantage
- 73
- Tel
- 400-6206333 13167063860
- Fax
- 021-50323701
- anhua.mao@aladdin-e.com
- Country
- China
- ProdList
- 25003
- Advantage
- 65
- Tel
- 021-61552785
- Fax
- 021-55660885
- sales@shshiji.com
- Country
- China
- ProdList
- 9546
- Advantage
- 55
- Tel
- 021-62960152
- Fax
- 021-52212593
- 934678158@qq.com
- Country
- China
- ProdList
- 9899
- Advantage
- 55
- Tel
- +86-021-50935922
- Fax
- +86-021-33847795
- Country
- China
- ProdList
- 7865
- Advantage
- 55
- Tel
- 15928766785 15928766785
- Fax
- QQ961458712
- wupengcheng@astatech.cn
- Country
- China
- ProdList
- 1987
- Advantage
- 55
- Tel
- +86-28-85122536 85324413
- Fax
- +86-28-85326443
- market@astatech.cn
- Country
- China
- ProdList
- 8026
- Advantage
- 55
- Tel
- 0570-3066667
- Fax
- 0570-3063388
- Country
- China
- ProdList
- 3930
- Advantage
- 58
- Tel
- 021-68367562 15002147577;
- Fax
- 021-68369562
- sales@haoyunchem.com
- Country
- China
- ProdList
- 457
- Advantage
- 55
- Tel
- 13971561712, 13995564702, 027-50664929
- Fax
- 027-50664927
- hbeixys2001@163.com
- Country
- China
- ProdList
- 3120
- Advantage
- 55
- Tel
- 400-0066400 13621662912
- Fax
- 021-55660885
- 422131432@qq.com
- Country
- China
- ProdList
- 9979
- Advantage
- 55
- Tel
- 0371-0371-13526885213 15637198702
- Fax
- 0371-63709726
- hsyykjchem@163.com
- Country
- China
- ProdList
- 3852
- Advantage
- 58
- Tel
- 021-021-56795766
- Fax
- +86-21-56795266
- sales@worldyachem.com
- Country
- China
- ProdList
- 9476
- Advantage
- 58
- Tel
- 86-0411-62789512
- Fax
- 86-0411-62789510
- xj_cui@dlrivin.com
- Country
- China
- ProdList
- 122
- Advantage
- 56
- Tel
- 021-58957966 18930537195
- Fax
- 021-60899437
- wouchina@126.com
- Country
- China
- ProdList
- 3027
- Advantage
- 58
- Tel
- 400-8592883
- Fax
- 0731-82251112
- sales@huatengsci.com
- Country
- China
- ProdList
- 5872
- Advantage
- 58
- Tel
- 021-60345187 13671753212
- Fax
- 021-34702061
- lzz841106@aliyun.com
- Country
- China
- ProdList
- 10263
- Advantage
- 55
- Tel
- 025-66028182 18626450290
- yftan@aikonchem.com
- Country
- China
- ProdList
- 16679
- Advantage
- 50
- Tel
- 0731-82251112-821 18974822355
- Fax
- 0731-82251112
- 2956573907@qq.com
- Country
- China
- ProdList
- 62
- Advantage
- 55
- Tel
- +86 (21) 61124340
- Fax
- +86 (21) 6129-4103
- Country
- China
- ProdList
- 9756
- Advantage
- 58
- Tel
- Fax
- -
- xg01_gj@163.com
- Country
- China
- ProdList
- 9484
- Advantage
- 50
- Tel
- 0512-67302433
- Fax
- 0512-67302433
- 3223436747@qq.com
- Country
- China
- ProdList
- 21
- Advantage
- 55
- Tel
- 021-61415566 800-8193336
- orderCN@merckgroup.com
- Country
- China
- ProdList
- 51395
- Advantage
- 80
More
Less
View Lastest Price from Dimethyl 5-nitroisophthalate manufacturers
Asia Chem I and E (Jiangsu) Co Ltd
- Product
- Dimethyl 5-nitroisophthalate 13290-96-5
- Price
- US $13.95/Kg/Drum
- Min. Order
- 25Kg/Drum
- Purity
- 99.00%HPLC
- Supply Ability
- 10tons/month
- Release date
- 2021-09-23
Hebei Chuanghai Biotechnology Co., Ltd
- Product
- Dimethyl 5-Nitroisophthalate 13290-96-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10mt
- Release date
- 2025-03-10
Hebei Chuanghai Biotechnology Co,.LTD
- Product
- Dimethyl 5-Nitroisophthalate 13290-96-5
- Price
- US $5.00-2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10000kg
- Release date
- 2024-08-21
13290-96-5, Dimethyl 5-nitroisophthalateRelated Search:
4-Nitrophenyl chloroformate
N,N-Dimethylformamide
Dimethyl acetylenedicarboxylate
Dimethyl carbonate
2-Nitrobenzoic acid
Dimethyl disulfide
Dimethyl isophthalate
Dacthal
Dimethyl succinate
Dimethyl sulfoxide
Methyl 5-nitroisophthalate
Dimethyl maleate
Dimethyl chloromalonate
Dimethyl ether
Dimethyl malonate
ETHANE
Dimethyl phthalate
Mono-methyl isophthalate