3-Phenoxypropyl bromide
- Product Name
- 3-Phenoxypropyl bromide
- CAS No.
- 588-63-6
- Chemical Name
- 3-Phenoxypropyl bromide
- Synonyms
- 1-Bromo;3-Phenoxypropyl;3-Phenoxypropyl brom;3-PHENOXYBROMOPROPANE;1-bromopropoxybenzene;3-Phenoxyethylbromide;3-PHENOXYPROPYL BROMIDE;(3-bromopropoxy)-benzen;2-phenoxypropyi bromide;3-BROMOISOPROPOXYBENZENE
- CBNumber
- CB9228553
- Molecular Formula
- C9H11BrO
- Formula Weight
- 215.09
- MOL File
- 588-63-6.mol
3-Phenoxypropyl bromide Property
- Melting point:
- 10-11 °C (lit.)
- Boiling point:
- 130-134 °C/14 mmHg (lit.)
- Density
- 1.365 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.546(lit.)
- Flash point:
- 228 °F
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Chloroform, DMSO (Slightly), Methanol (Slightly)
- form
- Liquid
- Specific Gravity
- 1.365
- color
- Clear slightly brown
- BRN
- 508978
- InChIKey
- NIDWUZTTXGJFNN-UHFFFAOYSA-N
- LogP
- 3.290 (est)
- CAS DataBase Reference
- 588-63-6(CAS DataBase Reference)
- NIST Chemistry Reference
- Benzene, (3-bromopropoxy)-(588-63-6)
- EPA Substance Registry System
- Benzene, (3-bromopropoxy)- (588-63-6)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36-24/25
- WGK Germany
- 3
- TSCA
- Yes
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- P16303
- Product name
- 3-Phenoxypropyl bromide
- Purity
- 96%
- Packaging
- 25g
- Price
- $206
- Updated
- 2025/07/31
- Product number
- P1027
- Product name
- 3-Phenoxypropyl Bromide
- Purity
- >95.0%(GC)
- Packaging
- 25g
- Price
- $87
- Updated
- 2025/07/31
- Product number
- P1027
- Product name
- 3-Phenoxypropyl Bromide
- Purity
- >95.0%(GC)
- Packaging
- 250g
- Price
- $578
- Updated
- 2025/07/31
- Product number
- P318870
- Product name
- 3-Phenoxypropyl Bromide
- Packaging
- 5g
- Price
- $55
- Updated
- 2021/12/16
- Product number
- J91347
- Product name
- 3-Phenoxypropyl Bromide
- Packaging
- 5g
- Price
- $10
- Updated
- 2021/12/16
3-Phenoxypropyl bromide Chemical Properties,Usage,Production
Chemical Properties
lightbrown liquid
Uses
3-Phenoxypropyl Bromide is a reagent used in the synthesis of damidines in the study of myotonic dystrophy. Also used in thepreparation pf phenoxyalkylbenzimidazoles with antitubercular activity.
Synthesis
109-64-8
108-95-2
588-63-6
General procedure for the synthesis of 3-phenoxybromopropane (26) from 1,3-dibromopropane and phenol: Phenol (1.0 g, 10.6 mmol) was dissolved in acetone (20 ml). To this solution anhydrous potassium carbonate (7.34 g, 53.1 mmol) and 1,3-dibromopropane (8.58 g, 42.5 mmol) were added. The reaction mixture was refluxed in an oil bath for 12 hours. Upon completion of the reaction, the potassium carbonate was removed by filtration and the solvent was subsequently removed by distillation under reduced pressure to give the crude product. The crude product was purified by column chromatography (eluent: ethyl acetate:hexane = 3:7) to give the final target product 26 (2.05 g, 90% yield). The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 2.24 (m, 2H), 3.54 (t, J=6.4 Hz, 2H), 4.03 (t, J=5.8 Hz, 2H), 6.86 (m, 3H), 7.21 (m, 2H).
References
[1] Bioorganic and Medicinal Chemistry, 2010, vol. 18, # 3, p. 1244 - 1251
[2] Chemical Communications, 2012, vol. 48, # 52, p. 6517 - 6519
[3] Patent: WO2013/163321, 2013, A1. Location in patent: Paragraph 000181
[4] Dyes and Pigments, 2010, vol. 84, # 2, p. 183 - 189
[5] European Journal of Medicinal Chemistry, 2012, vol. 53, p. 292 - 299
3-Phenoxypropyl bromide Preparation Products And Raw materials
Raw materials
Preparation Products
3-Phenoxypropyl bromide Suppliers
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View Lastest Price from 3-Phenoxypropyl bromide manufacturers
- Product
- 3-Phenoxypropyl bromide 588-63-6
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2020-01-02
- Product
- 3-Phenoxypropyl bromide 588-63-6
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 99.5%min
- Supply Ability
- 20kg/week
- Release date
- 2019-10-28