5-Amino-2-bromo-6-iodopyridine

Product Name: 5-Amino-2-bromo-6-iodopyridine
CAS No.: 915006-52-9
Chemical Name: 5-Amino-2-bromo-6-iodopyridine
Synonyms: 6-bromo-2-iodopyridin-3-amine;3-AMino-6-broMo-2-iodopyridine;5-Amino-2-bromo-6-iodopyridine;3-PyridinaMine, 6-broMo-2-iodo-;6-BroMo-2-iodo-pyridin-3-ylaMine;5-Amino-2-bromo-6-iodopyridine ISO 9001：2015 REACH
CBNumber: CB92484995
Molecular Formula: C5H4BrIN2
Formula Weight: 298.91
MOL File: 915006-52-9.mol

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5-Amino-2-bromo-6-iodopyridine Property

Boiling point:: 362.5±42.0 °C(Predicted)
Density: 2.426±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: -0.19±0.10(Predicted)
Appearance: Brown to reddish brown Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FA152973
Product name: 5-Amino-2-bromo-6-iodopyridine
Packaging: 2mg
Price: $59
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA152973
Product name: 5-Amino-2-bromo-6-iodopyridine
Packaging: 5mg
Price: $117
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA152973
Product name: 5-Amino-2-bromo-6-iodopyridine
Packaging: 10mg
Price: $203
Updated: 2021/12/16

AK Scientific

Product number: 5369AC
Product name: 6-Bromo-2-iodopyridin-3-amine
Packaging: 1g
Price: $384
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA152973
Product name: 5-Amino-2-bromo-6-iodopyridine
Packaging: 25mg
Price: $405
Updated: 2021/12/16

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5-Amino-2-bromo-6-iodopyridine Chemical Properties,Usage,Production

Synthesis

13534-97-9

915006-52-9

General procedure for the synthesis of 5-amino-2-bromo-6-iodopyridine from 5-amino-2-bromopyridine: To a stirring solution of 6-bromo-pyridin-3-ylamine (10.2 g, 0.0580 mol) and Ag2SO4 (18.1 g, 0.0580 mol) in ethanol (150 mL) was added iodine (7.59 g, 0.0580 mol). The reaction mixture was stirred overnight. Subsequently, hexane (200 mL) was added and the mixture was filtered through diatomaceous earth. The solvent was removed under reduced pressure and the residue was dissolved in chloroform (200 mL), washed sequentially with saturated aqueous sodium thiosulfate (100 mL) and water (1 x 100 mL), and dried over anhydrous sodium sulfate. The solvent was concentrated under reduced pressure and the residue was dissolved in hot ethyl acetate (100 mL), filtered and treated with hexane (100 mL). Filtration afforded a white crystalline product 5-amino-2-bromo-6-iodopyridine 11.2 g in 65% yield. 1H-NMR (CDCl3; 400 MHz): δ 7.10 (d, 1H, J=8.2 Hz), 6.74 (d, 1H, J=8.2 Hz), 4.06 (br s, 2H).

References

[1] Patent: US2007/249649, 2007, A1. Location in patent: Page/Page column 74
[2] Patent: US2007/249608, 2007, A1. Location in patent: Page/Page column 41
[3] Patent: WO2007/123516, 2007, A1. Location in patent: Page/Page column 109-110
[4] Patent: WO2009/149820, 2009, A1. Location in patent: Page/Page column 82-83
[5] Journal of Medicinal Chemistry, 2013, vol. 56, # 21, p. 8860 - 8871

5-Amino-2-bromo-6-iodopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Amino-2-bromo-6-iodopyridine Suppliers

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View Lastest Price from 5-Amino-2-bromo-6-iodopyridine manufacturers

Dideu Industries Group Limited

Product: 5-Amino-2-bromo-6-iodopyridine 915006-52-9
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-01

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5-Amino-2-bromo-6-iodopyridine ISO 9001：2015 REACH

915006-52-9