Methyl 5-aMino-2-nitro benzoate

Product Name: Methyl 5-aMino-2-nitro benzoate
CAS No.: 35998-96-0
Chemical Name: Methyl 5-aMino-2-nitro benzoate
Synonyms: Methyl 5-aMino-2-nitro benzoate;5-aMino-2-nitro-benzoic acid Methyl ester;Benzoic acid, 5-amino-2-nitro-, methyl ester
CBNumber: CB92570948
Molecular Formula: C8H8N2O4
Formula Weight: 196.16
MOL File: 35998-96-0.mol

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Methyl 5-aMino-2-nitro benzoate Property

Melting point:: 98-100 °C
Boiling point:: 394.5±22.0 °C(Predicted)
Density: 1.386±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: -0.15±0.10(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 4298AJ
Product name: Methyl5-amino-2-nitrobenzoate
Packaging: 1g
Price: $208
Updated: 2021/12/16

Matrix Scientific

Product number: 132408
Product name: Methyl5-amino-2-nitrobenzoate
Purity: 97%
Packaging: 1g
Price: $352
Updated: 2021/12/16

AK Scientific

Product number: 4298AJ
Product name: Methyl5-amino-2-nitrobenzoate
Packaging: 10g
Price: $624
Updated: 2021/12/16

Matrix Scientific

Product number: 132408
Product name: Methyl5-amino-2-nitrobenzoate
Purity: 97%
Packaging: 5g
Price: $1239
Updated: 2021/12/16

Ambeed

Product number: A435238
Product name: Methyl5-amino-2-nitrobenzoate
Purity: 97%
Packaging: 250mg
Price: $20
Updated: 2021/12/16

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Methyl 5-aMino-2-nitro benzoate Chemical Properties,Usage,Production

Chemical Properties

Reddish brown solid

Synthesis

67-56-1

13280-60-9

35998-96-0

5-Amino-2-nitrobenzoic acid (Compound A) (910 mg) was dissolved in methanol (50 mL). Thionyl chloride (0.74 mL) was added slowly and dropwise to the above solution under cooling in an ice bath. Subsequently, the reaction mixture was heated to reflux for 12 hours. Upon completion of the reaction, the reaction solution was cooled to room temperature and concentrated under reduced pressure. The residue was purified by column chromatography using a chloroform-methanol solvent mixture as eluent to finally obtain methyl 5-amino-2-nitrobenzoate (410 mg, 42% yield).

References

[1] Tetrahedron Letters, 2005, vol. 46, # 44, p. 7477 - 7481
[2] Patent: EP1614676, 2006, A1. Location in patent: Page/Page column 179
[3] European Journal of Medicinal Chemistry, 2012, vol. 57, p. 468 - 482

Methyl 5-aMino-2-nitro benzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 5-aMino-2-nitro benzoate Suppliers

China 69 India 1 United Kingdom 1 United States 7 Global 78

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View Lastest Price from Methyl 5-aMino-2-nitro benzoate manufacturers

Career Henan Chemical Co

Product: Methyl 5-aMino-2-nitro benzoate 35998-96-0
Price: US $1.00/kg
Min. Order: 1kg
Purity: 95%-99%
Supply Ability: 1000kg
Release date: 2018-12-25

35998-96-0, Methyl 5-aMino-2-nitro benzoateRelated Search:

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Methyl 5-aMino-2-nitro benzoate

5-aMino-2-nitro-benzoic acid Methyl ester

Benzoic acid, 5-amino-2-nitro-, methyl ester

35998-96-0