Methyl 5-aMino-2-nitro benzoate
- Product Name
- Methyl 5-aMino-2-nitro benzoate
- CAS No.
- 35998-96-0
- Chemical Name
- Methyl 5-aMino-2-nitro benzoate
- Synonyms
- Methyl 5-aMino-2-nitro benzoate;5-aMino-2-nitro-benzoic acid Methyl ester;Benzoic acid, 5-amino-2-nitro-, methyl ester
- CBNumber
- CB92570948
- Molecular Formula
- C8H8N2O4
- Formula Weight
- 196.16
- MOL File
- 35998-96-0.mol
Methyl 5-aMino-2-nitro benzoate Property
- Melting point:
- 98-100 °C
- Boiling point:
- 394.5±22.0 °C(Predicted)
- Density
- 1.386±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- -0.15±0.10(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 4298AJ
- Product name
- Methyl5-amino-2-nitrobenzoate
- Packaging
- 1g
- Price
- $208
- Updated
- 2021/12/16
- Product number
- 132408
- Product name
- Methyl5-amino-2-nitrobenzoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $352
- Updated
- 2021/12/16
- Product number
- 4298AJ
- Product name
- Methyl5-amino-2-nitrobenzoate
- Packaging
- 10g
- Price
- $624
- Updated
- 2021/12/16
- Product number
- 132408
- Product name
- Methyl5-amino-2-nitrobenzoate
- Purity
- 97%
- Packaging
- 5g
- Price
- $1239
- Updated
- 2021/12/16
- Product number
- 35998960
- Product name
- Methyl5-amino-2-nitrobenzoate
- Packaging
- 1g
- Price
- $1579.4
- Updated
- 2021/12/16
Methyl 5-aMino-2-nitro benzoate Chemical Properties,Usage,Production
Chemical Properties
Reddish brown solid
Synthesis
67-56-1
13280-60-9
35998-96-0
5-Amino-2-nitrobenzoic acid (Compound A) (910 mg) was dissolved in methanol (50 mL). Thionyl chloride (0.74 mL) was added slowly and dropwise to the above solution under cooling in an ice bath. Subsequently, the reaction mixture was heated to reflux for 12 hours. Upon completion of the reaction, the reaction solution was cooled to room temperature and concentrated under reduced pressure. The residue was purified by column chromatography using a chloroform-methanol solvent mixture as eluent to finally obtain methyl 5-amino-2-nitrobenzoate (410 mg, 42% yield).
References
[1] Tetrahedron Letters, 2005, vol. 46, # 44, p. 7477 - 7481
[2] Patent: EP1614676, 2006, A1. Location in patent: Page/Page column 179
[3] European Journal of Medicinal Chemistry, 2012, vol. 57, p. 468 - 482
Methyl 5-aMino-2-nitro benzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 5-aMino-2-nitro benzoate manufacturers
- Product
- Methyl 5-aMino-2-nitro benzoate 35998-96-0
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 95%-99%
- Supply Ability
- 1000kg
- Release date
- 2018-12-25