Methyl 5-aMino-6-broMopicolinate

Product Name: Methyl 5-aMino-6-broMopicolinate
CAS No.: 797060-52-7
Chemical Name: Methyl 5-aMino-6-broMopicolinate
Synonyms: Methyl 5-aMino-6-broMopicolinate;Methyl 5-amino-6-bromo-2-pyridinecarboxylate;methyl 5-amino-6-bromopyridine-2-carboxylate;5-Amino-6-bromo-pyridine-2-carboxylic acid methyl ester;2-Pyridinecarboxylic acid, 5-amino-6-bromo-, methyl ester
CBNumber: CB92617610
Molecular Formula: C7H7BrN2O2
Formula Weight: 231.05
MOL File: 797060-52-7.mol

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Methyl 5-aMino-6-broMopicolinate Property

Boiling point:: 390.1±37.0 °C(Predicted)
Density: 1.662±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: -0.09±0.10(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 5643DW
Product name: Methyl5-amino-6-bromopicolinate
Packaging: 1g
Price: $660
Updated: 2021/12/16

AK Scientific

Product number: 5643DW
Product name: Methyl5-amino-6-bromopicolinate
Packaging: 100mg
Price: $223
Updated: 2021/12/16

Chemenu

Product number: CM255088
Product name: Methyl5-amino-6-bromopicolinate
Purity: 97%
Packaging: 1g
Price: $393
Updated: 2021/12/16

Crysdot

Product number: CD11055345
Product name: Methyl5-amino-6-bromopicolinate
Purity: 97%
Packaging: 1g
Price: $416
Updated: 2021/12/16

Alichem

Product number: 797060527
Product name: Methyl5-amino-6-bromopicolinate
Packaging: 250mg
Price: $1068.2
Updated: 2021/12/16

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Methyl 5-aMino-6-broMopicolinate Chemical Properties,Usage,Production

Synthesis

67515-76-8

797060-52-7

General procedure for the synthesis of methyl 5-amino-6-bromopyridine-2-carboxylate from methyl 5-aminopyridine-2-carboxylate: 2.0 mL of hydrogen peroxide solution (32% concentration) was slowly added to a mixed solution containing methyl 5-aminopyridine-2-carboxylate (2.0 g, 13.15 mmol) and 30 mL of 48% concentration hydrobromic acid. The reaction mixture was stirred at room temperature for 2 hours. Subsequently, an additional 0.32 mL of hydrogen peroxide solution was added and stirring was continued for 1 hour. Upon completion of the reaction, the mixture was cooled by an ice bath and the pH of the mixture was adjusted slowly by adding concentrated ammonia to 8. The mixture was extracted three times with ethyl acetate (60 mL each time) and the organic phases were combined. The organic phase was dried with anhydrous sodium sulfate, filtered and concentrated on a rotary evaporator. The crude product was purified by silica gel column chromatography (mobile phase: cyclohexane/ethyl acetate). 1.32 g of the target compound was finally obtained in 42.3% yield. The product was analyzed by HPLC-MS: log P = 0.96; mass (m/z): 231.0. 1H NMR (D6-DMSO) data: δ 3.79 (s, 3H), 6.40 (broad peak, 2H), 7.1 (d, 1H), 7.8 (d, 1H).

References

[1] Patent: US2015/216175, 2015, A1. Location in patent: Paragraph 0424
[2] Patent: EP1479680, 2004, A1. Location in patent: Page 49

Methyl 5-aMino-6-broMopicolinate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 5-aMino-6-broMopicolinate manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: Methyl 5-amino-6-bromo-2-pyridinecarboxylate 797060-52-7
Price: US $3.00-9.00/KG
Min. Order: 0.1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2025-06-25

797060-52-7, Methyl 5-aMino-6-broMopicolinateRelated Search:

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methyl 5-amino-6-bromopyridine-2-carboxylate

Methyl 5-amino-6-bromo-2-pyridinecarboxylate

Methyl 5-aMino-6-broMopicolinate

5-Amino-6-bromo-pyridine-2-carboxylic acid methyl ester

2-Pyridinecarboxylic acid, 5-amino-6-bromo-, methyl ester

797060-52-7