ChemicalBook > CAS DataBase List > 3-(4-Carboethoxy)phenyl propanal

3-(4-Carboethoxy)phenyl propanal

Product Name: 3-(4-Carboethoxy)phenyl propanal
CAS No.: 151864-81-2
Chemical Name: 3-(4-Carboethoxy)phenyl propanal
Synonyms: 4-CARBOETHOXYPHENYL BUTANAL;4-CARBOETHOXYPHENYL PROPANAL;ethyl 4-(3-oxopropyl)benzoate;4-ETHOXYCARBONYLHYDROCINNAMAL;3-(4-Carbethoxy)Phenylpropanal;4-(3-CARBETHOXY)PHENYLPROPANAL;3-(4-Carboethoxy)phenyl propana;Pemetrexed disodium Impurity 17;3-(4-CARBOETHOXY)PHENYL PROPANAL;4-(3-OXO-PROPYL)-BENZOIC ACID ETHYL ESTER
CBNumber: CB9270017
Molecular Formula: C12H14O3
Formula Weight: 206.24
MOL File: 151864-81-2.mol

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3-(4-Carboethoxy)phenyl propanal Property

Boiling point:: 312.4±25.0 °C(Predicted)
Density: 1.082±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Store in freezer, under -20°C
CAS DataBase Reference: 151864-81-2(CAS DataBase Reference)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: C176683
Product name: 3-(4-Carboethoxy)phenylPropanal
Packaging: 500mg
Price: $130
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC151389
Product name: 3-(4'-Carboxyphenyl)-propionaldehyde ethylester
Packaging: 250mg
Price: $165
Updated: 2021/12/16

AK Scientific

Product number: H647
Product name: 3-(4-Carboethoxy)phenylpropanal
Packaging: 1g
Price: $265
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC151389
Product name: 3-(4'-Carboxyphenyl)-propionaldehyde ethylester
Packaging: 1g
Price: $500
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0022289
Product name: 3-(4-CARBETHOXY) PHENYLPROPANAL
Purity: 95.00%
Packaging: 1G
Price: $738.57
Updated: 2021/12/16

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3-(4-Carboethoxy)phenyl propanal Chemical Properties,Usage,Production

Synthesis

51934-41-9

107-18-6

151864-81-2

Ethyl 4-iodobenzoate (200 g, 0.725 mol) and acryl alcohol (63 g, 1.087 mol) were added with stirring to a DMF (600) containing sodium bicarbonate (152 g, 1.812 mol), tetrabutylammonium bromide (117 g, 0.362 mol) and palladium(II) acetate (3.2 g, 0.014 mol) in a 600 mL) in suspension. The reaction mixture was heated to 75-80 °C and kept at this temperature for 3-3.5 h. The reaction was subsequently cooled to 40-50 °C. Under vigorous stirring, toluene (1 L) was added to the reaction mixture and stirring was continued for 15 minutes. The mixture was filtered through a diatomaceous earth pad and the diatomaceous earth pad was washed with toluene (2 x 200 mL). The filtrate and washings were combined, washed with water (3 x 1 L) and then evaporated to constant weight at 30-40 °C and 10 mmHg. 147.5 g (98.8% yield, 84% HPLC purity) of ethyl 4-(3-oxopropyl)benzoate crude product was obtained as a dark brown oil, which could be used in the next step without further purification.1H NMR (DMSO-d6): δ 1.38 (t, 3H), 2.81 (t, 2H), 3.03 (t, 2H), 4.39 (q, 2H) , 7.27 (d, 2H), 7.98 (d, 2H), 9.81 (s, 1H).

References

[1] Tetrahedron Letters, 1999, vol. 40, # 21, p. 4023 - 4026
[2] Patent: US2005/49296, 2005, A1. Location in patent: Page/Page column 7-8
[3] Organic Letters, 2009, vol. 11, # 22, p. 5342 - 5345
[4] Journal of Heterocyclic Chemistry, 2004, vol. 41, # 6, p. 941 - 946
[5] Patent: WO2006/63863, 2006, A1. Location in patent: Page/Page column 43-44; 1/2

3-(4-Carboethoxy)phenyl propanal Preparation Products And Raw materials

Raw materials

Preparation Products

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151864-81-2, 3-(4-Carboethoxy)phenyl propanalRelated Search:

Phenyl salicylate Stearoylbenzoylmethane Ethylparaben Diphenyl ether 2-Ethoxyethanol 4-Methylbenzenesulfonhydrazide Ethanol Ethyl acetate Benzoyl hydrazine Benzoyl cyanide Benzoyl peroxide Propionaldehyde Tris(trimethylsilyl)phosphate Trinexapac-ethyl Dimethyl succinate ISOXADIFEN-ETHYL PHENYL VALERATE Methyl acrylate

4-(3-CARBETHOXY)PHENYLPROPANAL

4-(3-OXO-PROPYL)-BENZOIC ACID ETHYL ESTER

3-(4'-CARBOXYPHENYL)-PROPIONALDEHYDE ETHYL ESTER

3-(4-CARBOETHOXY)PHENYL PROPANAL

4-CARBOETHOXYPHENYL PROPANAL

4-CARBOETHOXYPHENYL BUTANAL

4-ETHOXYCARBONYLHYDROCINNAMAL

3-(4-Carbethoxy)Phenylpropanal

Benzoic acid, 4-(3-oxopropyl)-, ethyl ester (9CI)

ethyl 4-(3-oxopropyl)benzoate

Benzoic acid, 4-(3-oxopropyl)-, ethyl ester

3-(4-Carboethoxy)phenyl propana

Pemetrexed disodium Impurity 17

Benzoic acid, 4-(3-oxopropyl)-, ethyl ester (9CI, ACI)

4-(3-oxopropyl)-Benzoic acid ethyl ester (9CI ACI)

151864-81-2

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