ChemicalBook > CAS DataBase List > Ethyl 1-benzylpyrrolidine-3-carboxylate

Ethyl 1-benzylpyrrolidine-3-carboxylate

Product Name
Ethyl 1-benzylpyrrolidine-3-carboxylate
CAS No.
5747-92-2
Chemical Name
Ethyl 1-benzylpyrrolidine-3-carboxylate
Synonyms
ETHYL 1 -BENZYL-PYRROLIDINE-3-CALATE;ETHYL 1-BENZYL-PYRROLIDINE-3-CARBOXYLATE;Ethyl1-benzylpyrrolidine-3-carboxylate,97%;1-BENZYL-PYRROLIDINE-3-CARBOXYLIC ACID ETHYL ESTER;3-Pyrrolidinecarboxylic acid, 1-(phenylMethyl)-, ethyl ester
CBNumber
CB9450640
Molecular Formula
C14H19NO2
Formula Weight
233.31
MOL File
5747-92-2.mol
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Ethyl 1-benzylpyrrolidine-3-carboxylate Property

Boiling point:
118-120 °C(Press: 0.75 Torr)
Density 
1.099±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
Liquid
pka
8.43±0.40(Predicted)
color 
Pale yellow
InChI
InChI=1S/C14H19NO2/c1-2-17-14(16)13-8-9-15(11-13)10-12-6-4-3-5-7-12/h3-7,13H,2,8-11H2,1H3
InChIKey
CYPXEPWPTXKUPL-UHFFFAOYSA-N
SMILES
N1(CC2=CC=CC=C2)CCC(C(OCC)=O)C1
CAS DataBase Reference
5747-92-2(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,T
Risk Statements 
36/37/38-25
Safety Statements 
26-36/37/39-45
RIDADR 
UN 2811 6.1 / PGIII
WGK Germany 
3
HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

Precautionary statements

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
ADE000011
Product name
Ethyl 1-benzyl-pyrrolidine-3-carboxylate
Purity
Aldrich
Packaging
1g
Price
$201
Updated
2023/06/20
Usbiological
Product number
448647
Product name
Ethyl 1-benzylpyrrolidine-3-carboxylate
Packaging
100mg
Price
$305
Updated
2021/12/16
TRC
Product number
E900003
Product name
Ethyl 1-benzyl-pyrrolidine-3-carboxylate
Packaging
500mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB34113
Product name
1-Benzyl-pyrrolidine-3-carboxylic acid ethyl ester
Packaging
1g
Price
$72
Updated
2021/12/16
AK Scientific
Product number
J94957
Product name
1-Benzyl-pyrrolidine-3-carboxylicacidethylester
Packaging
5g
Price
$75
Updated
2021/12/16
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Ethyl 1-benzylpyrrolidine-3-carboxylate Chemical Properties,Usage,Production

Uses

Ethyl 1-benzylpyrrolidine-3-carboxylate

Synthesis

64-17-5

10603-52-8

5747-92-2

General procedure for the synthesis of ethyl 1-benzylpyrrolidine-3-carboxylate from ethanol and 1-benzylpyrrolidine-3-carbonitrile: A solution of 1-benzylpyrrolidine-3-carbonitrile (1.5 g, 7.9 mmol) in ethanol (40 mL) was treated with a dioxane solution (20 mL) in 4 M HCl and stirred overnight at room temperature. Upon completion of the reaction, the reaction mixture was cooled to 0 °C and the pH was adjusted to neutral with saturated aqueous NaHCO3 solution, followed by extraction with ethyl acetate (EtOAc). The organic layers were combined, dried with anhydrous Na2SO4 and concentrated under reduced pressure. Purification by fast column chromatography (eluent: 35-50% EtOAc/hexane) afforded ethyl 1-benzylpyrrolidine-3-carboxylate (1.1 g, 58% yield).

References

[1] Patent: WO2003/103669, 2003, A1. Location in patent: Page 71-72

Ethyl 1-benzylpyrrolidine-3-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 1-benzylpyrrolidine-3-carboxylate manufacturers

Changsha YuTeng New Materials Co., Ltd.
Product
Ethyl 1-benzylpyrrolidine-3-carboxylate 5747-92-2
Price
US $0.00-0.00/g
Min. Order
100g
Purity
97%
Supply Ability
500kg/M
Release date
2024-11-07
Career Henan Chemical Co
Product
Ethyl 1-benzylpyrrolidine-3-carboxylate 5747-92-2
Price
US $0.01/KG
Min. Order
1KG
Purity
98%;99%
Supply Ability
1kg； 5kg；10kg；25kg
Release date
2020-01-07

5747-92-2, Ethyl 1-benzylpyrrolidine-3-carboxylateRelated Search:

Methyl acrylate N-Methyl-2-pyrrolidone N-Vinyl-2-pyrrolidone Ethyl propiolate ISOXADIFEN-ETHYL Povidone iodine 1-Methylpyrrolidine (S)-Pyrrolidine-3-carboxylic acid Trinexapac-ethyl Tris(trimethylsilyl)phosphate Polyvinylpyrrolidone Ethylparaben Pyrrolidine Ethyl acetate Ethanol Ethyl acrylate RESMETHRIN Ethyl cyanoacetate

  • ETHYL 1-BENZYL-PYRROLIDINE-3-CARBOXYLATE
  • 1-BENZYL-PYRROLIDINE-3-CARBOXYLIC ACID ETHYL ESTER
  • ETHYL 1 -BENZYL-PYRROLIDINE-3-CALATE
  • 3-Pyrrolidinecarboxylic acid, 1-(phenylMethyl)-, ethyl ester
  • Ethyl1-benzylpyrrolidine-3-carboxylate,97%
  • 5747-92-2
  • C14H19O2N
  • pharmacetical