ChemicalBook > CAS DataBase List > 3-AMINO-2-BROMO-6-METHOXYPYRIDINE

3-AMINO-2-BROMO-6-METHOXYPYRIDINE

Product Name: 3-AMINO-2-BROMO-6-METHOXYPYRIDINE
CAS No.: 135795-46-9
Chemical Name: 3-AMINO-2-BROMO-6-METHOXYPYRIDINE
Synonyms: 2-Bromo-6-methoxy-3-pyridinamine;3-Amino-6-methoxy-2-bromopyridine;5-AMino-6-broMo-2-Methoxypyridine;2-BROMO-3-AMINO-6-METHOXYPYRIDINE;3-AMINO-2-BROMO-6-METHOXYPYRIDINE;3-AMINO-2-CHLORO-6-METHOXYPYRIDINE;3-Pyridinamine, 2-bromo-6-methoxy-;3-Amino-2-bromo-6-methoxypyridine ,97%;3-AMINO-2-BROMO-6-METHOXYPYRIDINE ISO 9001：2015 REACH
CBNumber: CB9485154
Molecular Formula: C6H7BrN2O
Formula Weight: 203.04
MOL File: 135795-46-9.mol

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3-AMINO-2-BROMO-6-METHOXYPYRIDINE Property

Boiling point:: 293.9±35.0 °C(Predicted)
Density: 1.622±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 1.12±0.10(Predicted)
Appearance: Yellow to brown Solid

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Safety

Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: A602193
Product name: 3-Amino-2-bromo-6-methoxypyridine
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140331
Product name: 2-Bromo-6-methoxypyridin-3-amine
Packaging: 2g
Price: $87
Updated: 2021/12/16

Apolloscientific

Product number: OR315074
Product name: 2-Bromo-6-methoxypyridin-3-amine
Packaging: 1g
Price: $95
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-9-N9
Product name: 2-Bromo-6-methoxypyridin-3-amine
Packaging: 1g
Price: $104
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140331
Product name: 2-Bromo-6-methoxypyridin-3-amine
Packaging: 5G
Price: $173
Updated: 2021/12/16

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3-AMINO-2-BROMO-6-METHOXYPYRIDINE Chemical Properties,Usage,Production

Chemical Properties

Dark red solid

Synthesis

6628-77-9

135795-46-9

General procedure for the synthesis of 3-amino-6-methoxy-2-bromopyridine from 5-amino-2-methoxypyridine: 1. 1.83 g (14.7 mmol) of 5-amino-2-methoxypyridine, 1.21 g (14.7 mmol) of sodium acetate, and 12 mL of acetic acid were sequentially added to a reaction flask and stirred well. 2. 0.75 mL (14.7 mmol) of bromine was slowly added dropwise at room temperature, keeping the reaction at room temperature. 3. 3. After the dropwise addition, continue to stir the reaction mixture at room temperature for 30 minutes. 4. 4. Upon completion of the reaction, 200 mL of saturated sodium thiosulfate solution was added to the reaction mixture to quench the reaction. 5. The reaction mixture was transferred to a partition funnel and the aqueous phase was extracted twice with ethyl acetate. 6. The organic phases were combined, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to give 3 g of the purple solid product 3-amino-6-methoxy-2-bromopyridine (quantitative yield). Product characterization data: 1H NMR (250 MHz, DMSO-d6) δ: 7.18 (d, 1H), 6.64 (d, 1H), 4.91 (s, 2H), 3.71 (s, 3H).

References

[1] Patent: US2008/200495, 2008, A1. Location in patent: Page/Page column 9
[2] Tetrahedron Letters, 2011, vol. 52, # 41, p. 5292 - 5296
[3] Journal of Medicinal Chemistry, 1995, vol. 38, # 24, p. 4830 - 4838
[4] Patent: WO2005/30213, 2005, A1. Location in patent: Page/Page column 170-171
[5] Patent: US5366972, 1994, A

3-AMINO-2-BROMO-6-METHOXYPYRIDINE Preparation Products And Raw materials

Raw materials

Sodium acetate Ethyl acetate Bromine Dichloromethane Acetic acid Sodium hydroxide Magnesium sulfate PETROLEUM ETHER 5-Amino-2-methoxypyridine

Preparation Products

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3-AMINO-2-BROMO-6-METHOXYPYRIDINE Suppliers

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View Lastest Price from 3-AMINO-2-BROMO-6-METHOXYPYRIDINE manufacturers

Hebei Xinsheng New Material Technology Co., LTD.

Product: 3-AMINO-2-BROMO-6-METHOXYPYRIDINE 135795-46-9
Price: US $35.00-25.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 Ton
Release date: 2023-11-03

Dideu Industries Group Limited

Product: 3-AMINO-2-BROMO-6-METHOXYPYRIDINE 135795-46-9
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-03

Career Henan Chemical Co

Product: 3-AMINO-2-BROMO-6-METHOXYPYRIDINE 135795-46-9
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1kg-1000kg
Release date: 2020-01-08

135795-46-9, 3-AMINO-2-BROMO-6-METHOXYPYRIDINERelated Search:

3-Amino-6-bromo-2-methoxypyridine 3-AMINO-2-BROMO-6-METHOXYPYRIDINE 2-Chloro-6-methoxy-3-nitropyridine 3-AMINO-5-BROMO-2-METHOXYPYRIDINE 5-AMINO-3-BROMO-2-METHOXYPYRIDINE 2-AMINO-5-BROMO-3-METHOXYPYRIDINE 2-Bromo-6-methoxypyridine 4-AMINO-3-BROMO-2-METHOXYPYRIDINE 2-Amino-5-bromo-4-methoxypyridine-3-carbonitrile, 2-Amino-5-bromo-3-cyano-4-methoxypyridine 3-Pyridinamine,2-bromo-6-ethoxy-(9CI) 3-Amino-2-bromo-4-methoxypyridine 2-BROMO-6-ETHOXY-3-NITROPYRIDINE 2-BROMO-3-AMINO-6-METHOXY-4-PICOLINE 2-Amino-6-chloro-4-methoxypyridine 3-AMINO-5-BROMO-6-METHOXYPYRIDINE-2-CARBONITRILE 3-AMINO-5-BROMO-6-METHOXYPYRIDINE-2-CARBOXAMIDE 6-METHOXY-3-NITRO-2-BROMOPYRIDINE

2-Bromo-6-methoxy-3-pyridinamine

5-AMino-6-broMo-2-Methoxypyridine

3-AMINO-2-CHLORO-6-METHOXYPYRIDINE

3-AMINO-2-BROMO-6-METHOXYPYRIDINE

2-BROMO-3-AMINO-6-METHOXYPYRIDINE

3-Amino-2-bromo-6-methoxypyridine ,97%

3-Pyridinamine, 2-bromo-6-methoxy-

3-AMINO-2-BROMO-6-METHOXYPYRIDINE ISO 9001：2015 REACH

3-Amino-6-methoxy-2-bromopyridine

135795-46-9

C6H7BrN2O

amine| alkyl bromide

Pyridine

Pyridines