Synthesis
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Ethyl 2,3-dicyanopropionate

Synthesis
Product Name
Ethyl 2,3-dicyanopropionate
CAS No.
40497-11-8
Chemical Name
Ethyl 2,3-dicyanopropionate
Synonyms
3-dicyanopropionate;2,3-DICYANOPROPIONATE, 98%;2,3-Ethyldicyanopropionate;Ethy 2,3-dicyanopropionate;Ethyl 2,3-Dicyanopropanate;ethyl 2,3-dicyanopropanoate;ETHYL 2,3-DICYANOPROPIONATE;Ethyl 2,3-Dicyanopropionate, 98%+;2,3-Dicyanopropionate ethyl ester;2,3-Dicyanobenzoic acid,ethyl ester
CBNumber
CB9667312
Molecular Formula
C7H8N2O2
Formula Weight
152.15
MOL File
40497-11-8.mol
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Ethyl 2,3-dicyanopropionate Property

Boiling point:
120-135 °C
Density 
1.129±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform, Methanol
form 
Oil
color 
Clear Light Brown to Yellow
CAS DataBase Reference
40497-11-8(CAS DataBase Reference)
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Safety

HS Code 
2926907090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H332Harmful if inhaled

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P322Specific measures (see …on this label).

P330Rinse mouth.

P363Wash contaminated clothing before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
E1366
Product name
Ethyl 2,3-Dicyanopropionate
Packaging
5G
Price
$40
Updated
2024/03/01
TCI Chemical
Product number
E1366
Product name
Ethyl 2,3-Dicyanopropionate
Packaging
25G
Price
$152
Updated
2024/03/01
TRC
Product number
E915950
Product name
Ethyl 2,3-Dicyanopropionate
Packaging
250mg
Price
$50
Updated
2021/12/16
AK Scientific
Product number
A555
Product name
Ethyl 2,3-Dicyanopropionate
Packaging
5g
Price
$61
Updated
2021/12/16
AK Scientific
Product number
A555
Product name
Ethyl 2,3-Dicyanopropionate
Packaging
10g
Price
$107
Updated
2021/12/16
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Ethyl 2,3-dicyanopropionate Chemical Properties,Usage,Production

Synthesis

The preparation method of Ethyl 2,3-dicyanopropionate is to add potassium cyanide solution and ethyl cyanoacetate into the reaction flask, use dimethyl sulfoxide as solvent, slowly add formaldehyde solution to the solution, and maintain the reaction temperature at 5 ℃ After the addition, the reaction was continued at 20°C for 15h, then the reaction solution was added to ice water, the organic layer was separated, the aqueous layer was extracted with a solvent, the organic layers were mixed, dried and desolubilized to obtain the product. Reaction equation:
HCHO+KCN+CNCH2COOC2H5→CNCH2—CHCNCOOC2H5

Chemical Properties

Brown Oil

Uses

An intermediate for insecticide.

Ethyl 2,3-dicyanopropionate Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethyl 2,3-dicyanopropionate Suppliers

Service Chemical Inc.
Tel
--
Fax
--
Email
sales@chemos-group.com
Country
Germany
ProdList
6350
Advantage
71
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View Lastest Price from Ethyl 2,3-dicyanopropionate manufacturers

Hebei Chuanghai Biotechnology Co,.LTD
Product
Ethyl 2,3-dicyanopropionate 40497-11-8
Price
US $10.00/KG
Min. Order
1KG
Purity
99.%
Supply Ability
10 ton
Release date
2024-08-22
Hebei Mojin Biotechnology Co., Ltd
Product
Ethy 2,3-dicyanopropionate 40497-11-8
Price
US $100.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
5000kg/week
Release date
2021-06-09
Zhuozhou Wenxi import and Export Co., Ltd
Product
Ethyl 2,3-dicyanopropionate 40497-11-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27

40497-11-8, Ethyl 2,3-dicyanopropionateRelated Search:


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