ChemicalBook > CAS DataBase List > 3-CHLOROBENZHYDROL

3-CHLOROBENZHYDROL

Product Name: 3-CHLOROBENZHYDROL
CAS No.: 63012-03-3
Chemical Name: 3-CHLOROBENZHYDROL
Synonyms: AURORA KA-7060;3-CHLOROBENZHYDROL;3-CHLORODIPHENYLMETHANOL;(3-CHLORO-PHENYL)-PHENYL-METHANOL;Benzenemethanol, 3-chloro-α-phenyl-;Benzenemethanol, 3-chloro-a-phenyl-
CBNumber: CB9744152
Molecular Formula: C13H11ClO
Formula Weight: 218.68
MOL File: 63012-03-3.mol

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3-CHLOROBENZHYDROL Property

Melting point:: 40 °C
Boiling point:: 169°C/0.1mm
Density: 1?+-.0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 13.28±0.20(Predicted)
Appearance: White to off-white Solid
CAS DataBase Reference: 63012-03-3(CAS DataBase Reference)

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H303May be harmfulif swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: B405168
Product name: (3-Chlorophenyl)(phenyl)methanol
Packaging: 1g
Price: $310
Updated: 2021/12/16

AK Scientific

Product number: 9560AB
Product name: (3-Chlorophenyl)(phenyl)methanol
Packaging: 250mg
Price: $167
Updated: 2021/12/16

AK Scientific

Product number: 9560AB
Product name: (3-Chlorophenyl)(phenyl)methanol
Packaging: 1g
Price: $193
Updated: 2021/12/16

AK Scientific

Product number: 9560AB
Product name: (3-Chlorophenyl)(phenyl)methanol
Packaging: 5g
Price: $429
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0021690
Product name: 3-CHLOROBENZHYDROL
Purity: 95.00%
Packaging: 1G
Price: $757.97
Updated: 2021/12/16

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3-CHLOROBENZHYDROL Chemical Properties,Usage,Production

Uses

(3-Chlorophenyl)(phenyl)methanol is useful as T cell activators to treat viral infections and proliferative disorders, such as cancer.

Synthesis

1016-78-0

63012-03-3

General procedure for the synthesis of 3-chlorodiphenylmethanol from 3-chlorobenzophenone: (1) To a mixed solution of ethanol (100 mL) and tetrahydrofuran (THF, 100 mL) of 3-chlorobenzophenone (10.0 g, 46.2 mmol), sodium borohydride (876 mg, 23.1 mmol) was slowly added at room temperature. The reaction mixture was stirred at room temperature for 3 h. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The residue was poured into water and extracted with ethyl acetate. The organic phases were combined, washed with water and then dried over anhydrous magnesium sulfate. After filtration, the solvent was removed by distillation under reduced pressure to give 3-chlorodiphenylmethanol as a colorless oil in a yield of 9.53 g (94.4% yield). 1H-NMR (CDCl3) δ: 2.55 (1H, d, J = 3.6 Hz), 5.80 (1H, d, J = 3.6 Hz), 7.25 to 7.40 (9H, m).

References

[1] Organic Letters, 2000, vol. 2, # 5, p. 659 - 661
[2] Patent: EP1437344, 2004, A1. Location in patent: Page 48
[3] Recueil des Travaux Chimiques des Pays-Bas, 1912, vol. 31, p. 311
[4] Recueil des Travaux Chimiques des Pays-Bas, 1915, vol. 34, p. 162
[5] Recueil des Travaux Chimiques des Pays-Bas, 1919, vol. 38, p. 121

3-CHLOROBENZHYDROL Preparation Products And Raw materials

Raw materials

Preparation Products

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63012-03-3, 3-CHLOROBENZHYDROLRelated Search:

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3-CHLOROBENZHYDROL

AURORA KA-7060

Benzenemethanol, 3-chloro-a-phenyl-

(3-CHLORO-PHENYL)-PHENYL-METHANOL

3-CHLORODIPHENYLMETHANOL

Benzenemethanol, 3-chloro-α-phenyl-

63012-03-3