ChemicalBook > CAS DataBase List > Ethyl 4-bromoacetoacetate

Ethyl 4-bromoacetoacetate

Product Name
Ethyl 4-bromoacetoacetate
CAS No.
13176-46-0
Chemical Name
Ethyl 4-bromoacetoacetate
Synonyms
Ethyl 4-bromo-3-oxobutanoate;1KG,5KG;Ethyl 4-bromoacetoacetate;Ethyl 4-Vromoacetoacetate;4-broMo ethyl acetoacetate;Ethyl 4-bromo-3-oxo-butyrate;4-BroMoacetoacetic acid ethyl ester;4-Bromo-3-oxobutanoic acid Et ester;4-Bromo-3-oxo-butyric acid ethyl ester;4-BroMo-3-oxo-butyric acid Methyl ester
CBNumber
CB9874938
Molecular Formula
C6H9BrO3
Formula Weight
209.04
MOL File
13176-46-0.mol
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Ethyl 4-bromoacetoacetate Property

Boiling point:
231.6 °C
Density 
1.511
refractive index 
1.5281 (estimate)
storage temp. 
2-8°C(protect from light)
pka
9.56±0.46(Predicted)
form 
liquid
color 
Colourless
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Safety

Hazard Codes 
F
HS Code 
2918300090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
E900590
Product name
Ethyl4-Bromoacetoacetate
Packaging
250mg
Price
$55
Updated
2021/12/16
TRC
Product number
E900590
Product name
Ethyl4-Bromoacetoacetate
Packaging
1g
Price
$70
Updated
2021/12/16
Usbiological
Product number
449228
Product name
Ethyl 4-Bromoacetoacetate
Packaging
250mg
Price
$319
Updated
2021/12/16
Oakwood
Product number
076501
Product name
4-Bromo-3-oxo-butyric acid ethyl ester
Packaging
250mg
Price
$30
Updated
2021/12/16
SynQuest Laboratories
Product number
2129-9-01
Product name
Ethyl 4-bromo-3-oxobutanoate
Purity
90%
Packaging
1g
Price
$48
Updated
2021/12/16
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Ethyl 4-bromoacetoacetate Chemical Properties,Usage,Production

Synthesis

To a solution of Ethyl acetoacetate (10.0 g, 76.9 mmol, 1 .0 eq) in acetic acid (30 mL) was added bromine (12.3 g, 76.9 mmol, 1 .0 eq) at 0 °C over 10 min. The mixture was stirred at 0 °C for 1 h, the solvent was removed under reduced pressure, and the residue was diluted with water (50 mL). The aqueous mixture was extracted with CH2CI2 (50 mL x 3). The combined organic layers were washed with brine (60 mL x 2), dried over MgS04 and concentrated under reduced pressure to give ethyl 4-bromo-3-oxobutanoate (14.3 g, 85 per cent) as a yellow oil.

Ethyl 4-bromoacetoacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 4-bromoacetoacetate manufacturers

Hebei Chuanghai Biotechnology Co,.LTD
Product
Ethyl 4-bromoacetoacetate 13176-46-0
Price
US $30.00-10.00/kg
Min. Order
10kg
Purity
99%
Supply Ability
100000kg
Release date
2024-08-23
Honest Joy Holdings Limited
Product
Ethyl 4-bromoacetoacetate 13176-46-0
Price
US $0.00/KG
Min. Order
1KG
Purity
99.3%
Supply Ability
100 tons
Release date
2022-01-25
Zhuozhou Wenxi import and Export Co., Ltd
Product
Ethyl 4-broMoacetoacetate 13176-46-0
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27

13176-46-0, Ethyl 4-bromoacetoacetateRelated Search:


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  • 4-Bromo-3-oxo-butyric acid ethyl ester
  • Ethyl 4-Vromoacetoacetate
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  • Ethyl 4-bromo-3-oxobutanoate
  • 4-Bromo-3-oxobutanoic acid Et ester
  • 4-broMo ethyl acetoacetate
  • 4-BroMoacetoacetic acid ethyl ester
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