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4-(4-Chlorophenyl)piperidine

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4-(4-Chlorophenyl)piperidine Basic information

Product Name:
4-(4-Chlorophenyl)piperidine
Synonyms:
  • 4-(4-CHLOROPHENYL)PIPERIDINE
  • Piperidine, 4-(4-chlorophenyl)-
  • 4-Chlorophenyl Piperidine
  • 4-(4'-Chlorophenyl)piperidine
CAS:
26905-02-2
MF:
C11H14ClN
MW:
195.69
Mol File:
26905-02-2.mol
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4-(4-Chlorophenyl)piperidine Chemical Properties

Melting point:
0°C
Boiling point:
0°C
Density 
1.095±0.06 g/cm3(Predicted)
Flash point:
0°C
storage temp. 
2-8°C(protect from light)
solubility 
soluble in Methanol
form 
powder to crystal
pka
10.14±0.10(Predicted)
color 
White to Orange to Green
CAS DataBase Reference
26905-02-2
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36
Safety Statements 
26
HS Code 
2933399990
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4-(4-Chlorophenyl)piperidine Usage And Synthesis

Synthesis

To a solution of 5.0 g (21.7 mmol) of 4-(4-chloro-phenyl)-1,2,3,6-tetrahydro-pyridine in 20 mL methanol are added 500 mg Pd/C. The reaction mixture is stirred for 7 h at ambient temperature and 10 psi hydrogen. After the catalyst is separated, the solvent is eliminated using the rotary evaporator. Further purification is carried out by column chromatography on silica gel (eluant: dichloromethane/methanol/ammonia=5:4.9:0.1) to afford 4-(4-Chlorophenyl)piperidine.

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