Basic information Safety Supplier Related

(1R)-CAMPHOR OXIME

Basic information Safety Supplier Related

(1R)-CAMPHOR OXIME Basic information

Product Name:
(1R)-CAMPHOR OXIME
Synonyms:
  • D-CAMPHOR OXIME
  • (1R)-CAMPHOR OXIME
  • (+)-Camphor oxime
  • (2E)-1,7,7-Trimethylbicyclo[2.2.1]heptan-2-one oxime
  • 1,7,7-trimethyl-,oxime,(1theta)-bicyclo[2.2.1]heptan-2-on
  • 2-Norbornyl oxime
  • bicyclo[2.2.1]heptan-2-one,1,7,7-trimethyl-,oxime,(1R)-
  • Camphor, oxime, (1R)-
CAS:
2792-42-9
MF:
C10H17NO
MW:
167.25
EINECS:
220-525-0
Product Categories:
  • Bicyclic Monoterpenes
  • Biochemistry
  • Terpenes
Mol File:
2792-42-9.mol
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(1R)-CAMPHOR OXIME Chemical Properties

Melting point:
115-119 °C
solubility 
almost transparency in Methanol
form 
powder to crystal
color 
White to Almost white
optical activity
[α]20/D 40.5±1°, c = 5% in ethanol
BRN 
2413664
InChI
1S/C10H17NO/c1-9(2)7-4-5-10(9,3)8(6-7)11-12/h7,12H,4-6H2,1-3H3/b11-8+/t7-,10+/m1/s1
InChIKey
OVFDEGGJFJECAT-RZIOALPKSA-N
SMILES
CC1(C)[C@@H]2CC[C@@]1(C)C(\C2)=N\O
CAS DataBase Reference
2792-42-9(CAS DataBase Reference)
EPA Substance Registry System
Bicyclo[2.2.1]heptan-2-one, 1,7,7-trimethyl-, oxime, (1R,4R)- (2792-42-9)
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Safety Information

Safety Statements 
22-24/25
WGK Germany 
3
TSCA 
TSCA listed
HS Code 
2929900090
Storage Class
11 - Combustible Solids

MSDS

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(1R)-CAMPHOR OXIME Usage And Synthesis

Synthesis

In 500 liters of reaction kettle add camphor 50 grams, sodium methanol 43.2Kg and 80Kg ethanol, ice water cooling through 34Kg ethyl nitrite, aeration is completed to continue the reaction for 2 hours, add 100Kg of water, liquid separation, the lower layer of the solution with 10% hydrochloric acid and neutralization to the PH value of 1-2, extracted with 100Kg of dichloromethane two times, combined with the dichloromethane, dechlorination of dichloromethane, recrystallization with ethanol to get a light yellow solid camphor oxime 50kg, yield 84%. Ethanol recrystallization to get light yellow solid camphor oxime 50kg, yield 84%.

(1R)-CAMPHOR OXIMESupplier

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