3-Methoxyphenol
3-Methoxyphenol Basic information
- Product Name:
- 3-Methoxyphenol
- Synonyms:
-
- RESORCINOL MONOMETHYL ETHER
- 3-Hydroxy phenyl methyl ether
- 3-Methoxyphenol,3-Hydroxyanisol
- RESORCINOLMETA-MONOMETHYLETHER
- META-METHOXYPHENOL
- m-Methoxyphel
- 3-Methoxyphenol ,98%
- 3-Hydroxyanisol, Resorcinol monomethyl ether
- CAS:
- 150-19-6
- MF:
- C7H8O2
- MW:
- 124.14
- EINECS:
- 205-754-6
- Product Categories:
-
- Building Blocks
- C6 to C8
- Chemical Synthesis
- Organic Building Blocks
- Oxygen Compounds
- Phenols
- Aromatic Ethers
- Aromatics
- Intermediates & Fine Chemicals
- Pharmaceuticals
- bc0001
- Mol File:
- 150-19-6.mol
3-Methoxyphenol Chemical Properties
- Melting point:
- -17 °C
- Boiling point:
- 113-115 °C/5 mmHg (lit.)
- Density
- 1.131 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.552(lit.)
- Flash point:
- >230 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- Chloroform (Slightly), Ethyl Acetate (Slightly)
- form
- Liquid
- pka
- 9.65(at 25℃)
- color
- Clear pink-reddish to brown
- Odor
- at 1.00?%?in?dipropylene glycol. phenolic
- Water Solubility
- slightly soluble
- BRN
- 1209898
- InChIKey
- ASHGTJPOSUFTGB-UHFFFAOYSA-N
- LogP
- 1.340
- CAS DataBase Reference
- 150-19-6(CAS DataBase Reference)
- NIST Chemistry Reference
- 3-Methoxyphenol(150-19-6)
- EPA Substance Registry System
- Phenol, 3-methoxy- (150-19-6)
Safety Information
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-36/38-41-36/37/38-43-36-22
- Safety Statements
- 26-36/37/39-46-37/39-24/25
- RIDADR
- UN 2810 6.1/PG 3
- WGK Germany
- 3
- RTECS
- SL7524000
- TSCA
- Yes
- HazardClass
- 6.1
- PackingGroup
- III
- HS Code
- 29095090
- Toxicity
- human,TCLo,inhalation,230ug/m3/22W (0.23mg/m3),BEHAVIORAL: IRRITABILITYBEHAVIORAL: MUSCLE WEAKNESSBEHAVIORAL: HEADACHE,Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 37(3), Pg. 108, 1972.
MSDS
- Language:English Provider:3-Hydroxyanisole
- Language:English Provider:ACROS
- Language:English Provider:SigmaAldrich
- Language:English Provider:ALFA
3-Methoxyphenol Usage And Synthesis
Chemical Properties
Clear pink red liquid
Uses
3-Methoxyphenol may be used as an analytical standard for the determination of the analyte in wine, coffee beans, wood samples, and mainstream smoke by gas chromatography (GC) based techniques.
Uses
A phenol derivative, 3-Methoxyphenol can be used as catalysts and as building blocks in synthesis of organic compounds such as antioxidants.
Preparation
synthesis of 3-methoxyphenol: The 1 mole of resorcinol is treated rapidly with stirring, in a three-necked flask provided with a reflux condenser, stirrer, internal thermometer, and dropping funnel, with 1.25 mole of 10% sodium hydroxide. With vigorous stirring, 1 mole of dimethyl sulfate is added in such a way that the temperature remains below 40° C (water cooling). To complete the reaction and to destroy unchanged dimethyl sulfate, the mixture is then heated for 30 min on a boiling water bath. After cooling, the organic layer is separated off and the aqueous solution is extracted several times with ether. The combined organic phases are washed with dilute sodium carbonate and then with water, dried with calcium chloride, and fractionated. Unchanged resorcinol can be recovered by acidifying the aqueous reaction solution and the wash water and extracting them with ether. The yield of 3-methoxyphenol is 50%, b.p. 113-115 °C/5 mm; b.p. 144°C/25mm; n20/D 1.552; d=1.131 g/mL at 25 °C.
Organicum. Practical Handbook of Organic Chemistry, by Heinz Becker, Werner Berger and Günter Domschke, Addison-Wesley Pub. Co, 206-207, (1973)
Definition
ChEBI: 3-methoxyphenol is a member of the class of phenols that is phenol having a methoxy-substituent at the 3-position. It is a member of phenols and a monomethoxybenzene. It derives from a resorcinol.
General Description
3-Methoxyphenol is a phenolic aroma compound typically present in food and beverage products.
Safety Profile
Poison by ingestion and intraperitoneal routes. Moderately toxic by skin contact. Human systemic effects by inhalation: muscle weakness, headache, and irritabdtty. Human female reproductive effects by inhalation: menstrual cycle changes and dsorders. A severe eye irritant. When heated to decomposition it emits acrid smoke and irritating fumes. See also ETHERS.
3-Methoxyphenol Preparation Products And Raw materials
Preparation Products
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3-Methoxyphenol(150-19-6)Related Product Information
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- 2,6-Dimethoxyphenol
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