ChemicalBook > CAS DataBase List > 3-Pyridinemethanol,5-fluoro-(8CI,9CI)

3-Pyridinemethanol,5-fluoro-(8CI,9CI)

Product Name
3-Pyridinemethanol,5-fluoro-(8CI,9CI)
CAS No.
22620-32-2
Chemical Name
3-Pyridinemethanol,5-fluoro-(8CI,9CI)
Synonyms
(5-Fluoropyridin-3-yl);5-fluoronicotinyl alcohol;5-fluoropyridine-3-methanol;5-fluoro-3-PyridineMethanol;(5-Fluoro-3-pyridyl)methanol;(5-Fluoropyridin-3-yl)met...;3-Pyridinemethanol, 5-fluoro-;(5-Fluoro-3-pyridinyl)methanol;(5-Fluoro-pyridin-3-yl)-methanol;5-Fluoro-3-(hydroxymethyl)pyridine
CBNumber
CB01285350
Molecular Formula
C6H6FNO
Formula Weight
127.12
MOL File
22620-32-2.mol
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3-Pyridinemethanol,5-fluoro-(8CI,9CI) Property

Boiling point:
123 °C(Press: 0.4 Torr)
Density 
1.262±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
13.29±0.10(Predicted)
form 
liquid
color 
Pale yellow
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Safety

Risk Statements 
20/21/22-33-37/38
Safety Statements 
7/8-26-36/37/39-45
RIDADR 
UN2811
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
CDS021735
Product name
(5-Fluoro-3-pyridinyl)methanol
Packaging
25mg
Price
$107
Updated
2025/07/31
TRC
Product number
F596323
Product name
(5-Fluoropyridin-3-yl)methanol
Packaging
100mg
Price
$70
Updated
2021/12/16
Apolloscientific
Product number
PC520517
Product name
(5-Fluoro-3-pyridyl)methanol
Purity
97%
Packaging
1g
Price
$112
Updated
2021/12/16
Matrix Scientific
Product number
068915
Product name
(5-Fluoro-3-pyridyl)methanol
Purity
>95%
Packaging
1g
Price
$152
Updated
2021/12/16
AK Scientific
Product number
1380AB
Product name
(5-Fluoropyridin-3-yl)methanol
Packaging
1g
Price
$255
Updated
2021/12/16
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3-Pyridinemethanol,5-fluoro-(8CI,9CI) Chemical Properties,Usage,Production

Chemical Properties

Yellow liquid

Uses

(5-Fluoropyridin-3-yl)methanol

Synthesis

402-66-4

22620-32-2

Step 1: Synthesis of (5-fluoropyridin-3-yl)methanol To a solution of 5-fluoronicotinic acid (1.0 g, 7.09 mmol) in tetrahydrofuran (THF, 10 mL) was added triethylamine (TEA, 0.9 mL, 7.73 mmol), followed by dropwise addition of ethyl chloroformate (0.6 mL, 7.73 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 2 h and then filtered and the residue was washed with a small amount of THF. The filtrate was cooled to 0 °C and sodium borohydride (0.67 g, 17.73 mmol) was added followed by slow dropwise addition of water (5 mL). The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the mixture was partitioned between ethyl acetate and water. The organic layers were combined, dried over anhydrous sodium sulfate and concentrated to give the crude product. The crude product was purified by silica gel column chromatography to give (5-fluoropyridin-3-yl)methanol (197 mg, 21.8% yield) as a colorless oil.LCMS retention time 0.375 min; LCMS MH+ 128.

References

[1] Patent: WO2018/67786, 2018, A1. Location in patent: Page/Page column 142
[2] Patent: WO2014/143799, 2014, A2. Location in patent: Page/Page column 429; 430
[3] Journal of Organic Chemistry, 1988, vol. 53, # 15, p. 3513 - 3521

3-Pyridinemethanol,5-fluoro-(8CI,9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Pyridinemethanol,5-fluoro-(8CI,9CI) manufacturers

Dideu Industries Group Limited
Product
3-Pyridinemethanol,5-fluoro-(8CI,9CI) 22620-32-2
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-10-20
Career Henan Chemical Co
Product
3-Pyridinemethanol,5-fluoro-(8CI,9CI) 22620-32-2
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2020-01-09

22620-32-2, 3-Pyridinemethanol,5-fluoro-(8CI,9CI)Related Search:

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