Methyl 3-amino-5-bromobenzoate
- Product Name
- Methyl 3-amino-5-bromobenzoate
- CAS No.
- 706791-83-5
- Chemical Name
- Methyl 3-amino-5-bromobenzoate
- Synonyms
- 3-AMINO-5-BROMOBENZOATE;Methyl 3-Amino-5-bromobenzoate;METHYL-3-BROMO-5-AMINO BENZOATE;Benzoic acid, 3-amino-5-bromo-, methyl ester
- CBNumber
- CB01471014
- Molecular Formula
- C8H8BrNO2
- Formula Weight
- 230.06
- MOL File
- 706791-83-5.mol
Methyl 3-amino-5-bromobenzoate Property
- Melting point:
- 83-88℃
- Boiling point:
- 332.3±22.0 °C(Predicted)
- Density
- 1.578±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 2.38±0.10(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M328553
- Product name
- Methyl3-amino-5-bromobenzoate
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 455148
- Product name
- Methyl 3-amino-5-bromobenzoate
- Packaging
- 100mg
- Price
- $305
- Updated
- 2021/12/16
- Product number
- 065397
- Product name
- Methyl 3-amino-5-bromobenzoate
- Packaging
- 5g
- Price
- $162
- Updated
- 2021/12/16
- Product number
- X5364
- Product name
- Methyl3-amino-5-bromobenzoate
- Packaging
- 10g
- Price
- $177
- Updated
- 2021/12/16
- Product number
- HCH0105847
- Product name
- METHYL 3-AMINO-5-BROMOBENZOATE
- Purity
- 95.00%
- Packaging
- 500MG
- Price
- $837.38
- Updated
- 2021/12/16
Methyl 3-amino-5-bromobenzoate Chemical Properties,Usage,Production
Synthesis
3-Bromo-5-aminobenzoic acid (1.0 g, 4.62 mmol) was stirred in methanol (15mL) with ice cooling, and the yellow solution was treated with thionyl chloride (4.00 mL, 55.0 mmol) dropwise over 20 mm. The resulting mixture was allowed to warm to room temperature and left stirring overnight. The reaction mixture was quenched with aqueous saturated NaHCO3 solution at 0 C. The solvent was then removed under vacuum, and the residue was suspended in ethyl acetate (200 mL). The organic phase was washed with brine (100 mL), dried (Na2504) and concentrated to afford Methyl 3-amino-5-bromobenzoate as a yellow solid (1.08 g, 98%). NMR (400 MHz, Methanol-d) oe 7.10 (t, J 1.6 Hz, 1H), 6.83 (t, J 1.6 Hz, 1H), 6.57 (t, J= 1.6 Hz, 1H), 3.46 (s, 3H). 13C NMR (100 MHz, CDC13) oe: 52.3, 114.6, 121.6, 122.3, 122.9, 132.6, 147.7, 166.0. m/z (ESI, MH) 231.
Methyl 3-amino-5-bromobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Methyl 3-amino-5-bromobenzoate Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from Methyl 3-amino-5-bromobenzoate manufacturers
- Product
- 3-AMINO-5-BROMOBENZOATE 706791-83-5
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2023-05-05
- Product
- 3-AMINO-5-BROMOBENZOATE 706791-83-5
- Price
- US $3.00-0.20/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-03-26
- Product
- 3-AMINO-5-BROMOBENZOATE 706791-83-5
- Price
- US $50.00/kg
- Min. Order
- 1kg
- Purity
- 99.9%
- Supply Ability
- 10000MT
- Release date
- 2023-08-17