1-Naphthylhydrazine hydrochloride
- Product Name
- 1-Naphthylhydrazine hydrochloride
- CAS No.
- 2243-56-3
- Chemical Name
- 1-Naphthylhydrazine hydrochloride
- Synonyms
- 1-NapthylhydrazineHCl;1-NAPHTHYLHYDRAZINE HCL;Alpha-NapthylHydrazineHcl;Indocyanine Green Impurity 9;Naphthalen-1-ylhydrazine HCl;1-phthylhydrazine hydrochloride;1-NAPTHYLHYDRAZINE HYDROCHLORIDE;1-NAPHTHYLHYDRAZINE HYDROCHLORIDE;1-naphthylhydrazinium(1+) chloride;1-NaphthylhydrazineHydrochloride>
- CBNumber
- CB0304333
- Molecular Formula
- C10H11ClN2
- Formula Weight
- 194.66
- MOL File
- 2243-56-3.mol
1-Naphthylhydrazine hydrochloride Property
- Melting point:
- 119 °C
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder to crystal
- color
- White to Light gray to Light orange
- CAS DataBase Reference
- 2243-56-3(CAS DataBase Reference)
- EPA Substance Registry System
- 1-Naphthylhydrazine hydrochloride (2243-56-3)
Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-36/37/38-51-22
- Safety Statements
- 22-36/37/39
- WGK Germany
- 3
- HS Code
- 2928.00.2500
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- ANV00020
- Product name
- 1-Naphthalenyl hydrazine hydrochloride
- Purity
- AldrichCPR
- Packaging
- 1g
- Price
- $185
- Updated
- 2025/07/31
- Product number
- N0064
- Product name
- 1-Naphthylhydrazine Hydrochloride
- Purity
- >90.0%(HPLC)
- Packaging
- 1g
- Price
- $32
- Updated
- 2025/07/31
- Product number
- N0064
- Product name
- 1-Naphthylhydrazine Hydrochloride
- Purity
- >90.0%(HPLC)
- Packaging
- 5g
- Price
- $119
- Updated
- 2025/07/31
- Product number
- N378488
- Product name
- Naphthalen-1-ylhydrazineHydrochloride
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- AK116584
- Product name
- Naphthalen-1-ylhydrazinehydrochloride
- Purity
- 98%
- Packaging
- 100mg
- Price
- $7
- Updated
- 2021/12/16
1-Naphthylhydrazine hydrochloride Chemical Properties,Usage,Production
Synthesis
91-59-8
2243-56-3
2.1 Synthesis of 2-naphthylhydrazine hydrochloride To a hydrochloric acid solution of 2-naphthylamine (800 mg, 5.59 mmol), a solution of sodium peroxide (Na?O?, 578 mg, 8.38 mmol) in water (1.2 mL) was slowly added under water-ice bath cooling conditions (addition time: 2 min). Subsequently, 6.0 M hydrochloric acid (6 mL) was added to the reaction system. The resulting solution was stirred in a water-ice bath for 1 h. Stannous chloride (SnCl?, 3.71 g, 19.56 mmol) was then slowly added (addition time: 5 min). The resulting suspension was continued to be stirred in a water-ice bath for 3.5 h, after which it was filtered. The filter cake was washed sequentially with water at 0 °C (4 × 8 mL), water at room temperature (1 × 8 mL), ether at 0 °C (Et?O, 2 × 4 mL), ether/hexane (1:1, 2 × 4 mL) and hexane (2 × 5 mL). The solid was dried to give 690 mg of the target product (Rf = 0.7, 40% ethyl acetate/hexane unfolding agent, milky white solid, 63% yield). 1H NMR (DMSO-d6, 250 MHz, δ): 7.81 (m, 2H, ArH), 7.71 (d, J=7.5 Hz, 1H, ArH), 7.49-7.19 (m, 4H, ArH). MS-EI+ m/z: 159.1 ([M-HCl]+).
References
[1] Patent: WO2011/147910, 2011, A1. Location in patent: Page/Page column 29-30; 36-37
1-Naphthylhydrazine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
1-Naphthylhydrazine hydrochloride Suppliers
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View Lastest Price from 1-Naphthylhydrazine hydrochloride manufacturers
- Product
- 1-Naphthylhydrazine hydrochloride 2243-56-3
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-25
- Product
- 1-Naphthylhydrazine hydrochloride 2243-56-3
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11
- Product
- 1-Naphthylhydrazine Hydrochloride 2243-56-3
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27