ChemicalBook > CAS DataBase List > L(-)-10-Camphorsulfonyl chloride

L(-)-10-Camphorsulfonyl chloride

Product Name
L(-)-10-Camphorsulfonyl chloride
CAS No.
39262-22-1
Chemical Name
L(-)-10-Camphorsulfonyl chloride
Synonyms
((1R,4S)-7,7-DiMethyl-2-oxobicyclo[2.2.1]heptan-1-yl)Methanesulfonyl chloride;(1R)-(-)-10-CamphorsuL;R)-()-10-CaMphorsulfony;L(-)Camphor sulfonyl chloride;(-)-10-CAMPHORSULFONYL CHLORIDE;(-)-10-Camphorsulfonyl Chloride;(-)-CAMPHOR-10-SULFONYL CHLORIDE;L(-)-10-CAMPHORSULFONYL CHLORIDE;(+)-camphor-10-sulfonyl chloride;L-(-)-1-Camphorsulfonyl chloride
CBNumber
CB0356635
Molecular Formula
C10H15ClO3S
Formula Weight
250.74
MOL File
39262-22-1.mol
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L(-)-10-Camphorsulfonyl chloride Property

Melting point:
66-68 °C(lit.)
alpha 
-33 º (c=3, chloroform)
Boiling point:
349.4±15.0 °C(Predicted)
Density 
1.331±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
Acetone, Dichloromethane, Ethyl Acetate, Methanol
form 
Solid
color 
White
optical activity
[α]18/D 33°, c = 3 in chloroform
Water Solubility 
Decomposes
Sensitive 
Moisture Sensitive
BRN 
3205975
InChIKey
BGABKEVTHIJBIW-UHFFFAOYSA-N
CAS DataBase Reference
39262-22-1(CAS DataBase Reference)
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Safety

Hazard Codes 
C
Risk Statements 
34
Safety Statements 
26-36/37/39-45
RIDADR 
UN 3261 8/PG 2
WGK Germany 
3
F 
10-21
HazardClass 
8
PackingGroup 
II
HS Code 
29147090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
301949
Product name
(1R)-(?)-10-Camphorsulfonyl chloride
Purity
97%
Packaging
5g
Price
$65.6
Updated
2023/01/07
TCI Chemical
Product number
C1308
Product name
(-)-10-Camphorsulfonyl Chloride
Purity
>98.0%(T)
Packaging
5g
Price
$42
Updated
2024/03/01
TCI Chemical
Product number
C1308
Product name
(-)-10-Camphorsulfonyl Chloride
Purity
>98.0%(T)
Packaging
25g
Price
$168
Updated
2024/03/01
TRC
Product number
C175070
Product name
(1R)-(?)-10-Camphorsulfonyl chloride
Packaging
10g
Price
$415
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0415093
Product name
(1R)-(-)-CAMPHOR-10-SULFONYL CHLORIDE
Purity
95.00%
Packaging
2G
Price
$825
Updated
2021/12/16
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L(-)-10-Camphorsulfonyl chloride Chemical Properties,Usage,Production

Chemical Properties

white to light yellow crystal powde

Uses

A chiral derivative of Camphor.

Uses

L(-)-10-Camphorsulfonyl chloride is a useful synthetic intermediate,it is used for asymmetric hydroxylation.

Purification Methods

If free from OH bands in the IR, then recrystallise it from Et2O or pet ether; otherwise treat it with SOCl2 at 50o for 30minutes, evaporate, dry the residue over KOH in a vacuum and recrystallise it. The (±)-acid chloride has m 85o [Bartlett & Knox Org Synth 45 14 1965]. Itis characterised as the amide (prisms from EtOH) m 132o, [ ] 17 (+) and (-) 1.5o (EtOH). On repeated recrystallisation from EtOH the anilide has m 120.5-121o, [] 25 +76o (c 1, CHCl3). [Read & Storey J Chem Soc 2761 1930, Sutherland & Shriner J Am Chem Soc 58 62 1936, Halterman et al. J Am Chem Soc 109 8105 1987, Bartlet & Knox Org Synth 45 55 1945, Beilstein 11 IV 650.]

L(-)-10-Camphorsulfonyl chloride Preparation Products And Raw materials

Raw materials

Preparation Products

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L(-)-10-Camphorsulfonyl chloride Suppliers

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View Lastest Price from L(-)-10-Camphorsulfonyl chloride manufacturers

Hebei Weibang Biotechnology Co., Ltd
Product
L(-)-10-Camphorsulfonyl chloride 39262-22-1
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-10-25
Zibo Hangyu Biotechnology Development Co., Ltd
Product
L(-)-10-Camphorsulfonyl chloride 39262-22-1
Price
US $10.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
100tons
Release date
2024-08-27
Hebei Mujin Biotechnology Co.,Ltd
Product
L(-)-10-Camphorsulfonyl chloride 39262-22-1
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-08-31

39262-22-1, L(-)-10-Camphorsulfonyl chlorideRelated Search:

Ethanesulfonyl chloride Calcium chloride Benzyl chloride Tosyl chloride Choline chloride Ammonium chloride (2R)-Bornane-10,2-sultam Sulfuryl chloride (-)-CAMPHOR 4-Nitrobenzenesulfonyl chloride Mepiquat chloride Camphor (1R)-(-)-10-Camphorsulfonic acid Benzenesulfonyl chloride Sodium chloride Polyvinyl chloride L-carnitine (1R,2R)-(-)-1,2-Diaminocyclohexane

  • L(-)-10-CAMPHORSULFONYL CHLORIDE
  • (-)-CAMPHOR-10-SULFONYL CHLORIDE
  • (1R)-(-)-10-CAMPHORSULFONYL CHLORIDE
  • (1R)-(-)-CAMPHOR-10-SULPHONYL CHLORIDE
  • (1R)-(-)-CAMPHOR-10-SULFONIC ACID CHLORIDE
  • (1R)-CAMPHOR-10-SULFONIC ACID CHLORIDE
  • (1R)-(-)-CAMPHOR-10-SULFONYL CHLORIDE
  • (-)-10-CAMPHORSULFONYL CHLORIDE
  • [3-(chlorosulfonylmethyl)-2,2,3-trimethylcyclopentyl]methanesulfonyl chloride
  • (1R)-(-)-10-CAMPHORSULFONYL CHLORIDE, 97 %
  • (1R)-(-)-CAMPHOR-10-SULFONIC ACID CHLORIDE 98+%
  • 6,(1R)-(-)-10-Camphorsulfonylchloride
  • Bicyclo2.2.1heptane-1-methanesulfonyl chloride, 7,7-dimethyl-2-oxo-, (1R,4S)-
  • (-)-Camphor-10-sulphonyl chloride
  • L(-)Camphor sulfonyl chloride
  • (1R)-CaMphor-1-sulfonic acid chloride
  • (-)-Camphor-10-sulfonyl chloride, (1R)-Camphor-10-sulfonic acid chloride
  • (7,7-Dimethyl-2-oxo-1-bicyclo[2.2.1]heptanyl)methanesulfonyl chloride
  • (1R,4S)-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfochloride
  • [1R,4R,(-)]-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfonic acid chloride
  • L(-)-10-Camphorsulfonyl chloride,97%
  • (1R,4S)-7,7-DiMethyl-2-oxo-bicyclo[2.2.1]heptane-1-Methanesulfonyl Chloride
  • (1R)-(-)-CAMPHOR-10-SULFONIC ACID CHLORI
  • ((1R,4S)-7,7-DiMethyl-2-oxobicyclo[2.2.1]heptan-1-yl)Methanesulfonyl chloride
  • R)-()-10-CaMphorsulfony
  • L-10- of caMphorsulfonyl chloride
  • L(-)-10-Camphorsulfonyl chloride (1R)-Camphor-10-sulfonic acid chloride
  • (1<i>R</i>)-()-10-Camphorsulfonyl chloride
  • (1R)-(-)-10-Camphorsulfonyl chloride 97%
  • (1R)-(-)-Camphor-10-sulfonic acid chloride for synthesis
  • [(1S,4R)-7,7-dimethyl-3-oxo-4-bicyclo[2.2.1]heptanyl]methanesulfonyl chloride
  • (-)-10-Camphorsulfonyl Chloride &gt
  • (1R)-(-)-10-CamphorsuL
  • L(-)-10-Camphorsulfonyl chloride USP/EP/BP
  • (+)-camphor-10-sulfonyl chloride
  • L-(-)-1-Camphorsulfonyl chloride
  • (-)-10-Camphorsulfonyl Chloride
  • (-)-Camphor-10-sulfonyl chloride
  • 39262-22-1
  • C10H15O3Cl
  • Bicyclic Monoterpenes
  • Terpenes
  • for Resolution of Bases
  • for Resolution of Alcohols & Thiols
  • Optical Resolution
  • SULFONYL CHLORIDE
  • Peptide
  • Intermediates & Fine Chemicals
  • Pharmaceuticals
  • Sulfonyl Chlorides
  • chiral
  • Chiral Reagents
  • Bicyclic Monoterpenes
  • Biochemistry
  • for Resolution of Alcohols & Thiols
  • for Resolution of Bases
  • Optical Resolution
  • Synthetic Organic Chemistry