2-AMINO-3-CHLORO-5-NITROPYRIDINE

Product Name: 2-AMINO-3-CHLORO-5-NITROPYRIDINE
CAS No.: 22353-35-1
Chemical Name: 2-AMINO-3-CHLORO-5-NITROPYRIDINE
Synonyms: 3-Chloro-5-nitro-2-pyridinamine;3-chloro-5-nitropyridin-2-amine;2-AMINO-3-CHLORO-5-NITROPYRIDINE;2-amino 5-nitro 3-chloro pyridine;2-Pyridinamine, 3-chloro-5-nitro-;3-Chloro-5-nitro-pyridin-2-ylamine;2-AMINO-3-CHLORO-5-NITROPYRIDINE, 95+%;Pyridine,2-amino-3-chloro-5-nitro- (6CI,8CI);2-AMINO-3-CHLORO-5-NITROPYRIDINE ISO 9001：2015 REACH
CBNumber: CB0425012
Molecular Formula: C5H4ClN3O2
Formula Weight: 173.56
MOL File: 22353-35-1.mol

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2-AMINO-3-CHLORO-5-NITROPYRIDINE Property

Melting point:: 211-213℃
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: Light yellow to yellow Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A595730
Product name: 2-Amino-3-chloro-5-nitropyridine
Packaging: 500mg
Price: $85
Updated: 2021/12/16

TRC

Product number: A595730
Product name: 2-Amino-3-chloro-5-nitropyridine
Packaging: 1g
Price: $115
Updated: 2021/12/16

ChemScene

Product number: CS-W021548
Product name: 2-Amino-3-chloro-5-nitropyridine
Packaging: 1g
Price: $31
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA55264
Product name: 2-Amino-3-chloro-5-nitropyridine
Packaging: 500mg
Price: $100
Updated: 2021/12/16

ChemScene

Product number: CS-W021548
Product name: 2-Amino-3-chloro-5-nitropyridine
Packaging: 5g
Price: $129
Updated: 2021/12/16

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2-AMINO-3-CHLORO-5-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

4214-76-0

22353-35-1

Under argon protection, N-chlorosuccinimide (0.53 g, 3.95 mmol) was slowly added to a solution of 2-amino-5-nitropyridine (0.50 g, 3.59 mmol) in anhydrous toluene (7.18 mL). The reaction mixture was stirred continuously at 80 °C for 1 hour. After completion of the reaction, the mixture was cooled to room temperature and diluted with 15 mL of water. Subsequently, extraction was carried out with ethyl acetate and the organic layer was washed sequentially with saturated sodium bicarbonate solution and brine. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure, and the resulting crude product was purified by column chromatography (silica gel 60N, gradient elution of n-hexane/ethyl acetate = 80/20 to 60/40) to afford 2-amino-3-chloro-5-nitropyridine (0.40 g, 2.30 mmol, 64% yield) as a yellow solid. The structure of the product was analyzed by nuclear magnetic resonance hydrogen spectrum (1H NMR, 500 MHz, DMSO-d6) δ 8.84 (d, J = 2.5 Hz, 1H), 8.35 (d, J = 2.5 Hz, 1H), 7.91 (brs, 1H); nuclear magnetic resonance carbon spectrum (13C NMR, 125 MHz, DMSO-d6) δ 112.58, 132.14, 135.01, 145.25, 159.75; high-resolution mass spectrometry (HRMS, ESI-TOF, m/z) calculated values of C5H4ClN3O2Na [M + Na]+: 195.9884, 197.9856, measured values: 195.9878, 197.9847 confirmed.

References

[1] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 14, p. 3853 - 3860
[2] Journal of the Chemical Society, 1951, p. 2590,2593
[3] Zhurnal Obshchei Khimii, 1940, vol. 10, p. 1827,1836
[4] Chem. Zentralbl., 1940, vol. 111, # II, p. 614
[5] Journal of the Chemical Society, 1951, p. 2590,2593

2-AMINO-3-CHLORO-5-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-3-CHLORO-5-NITROPYRIDINE Suppliers

China 83 India 6 United Kingdom 3 United States 12 Global 104

Pure Chemistry Scientific Inc.

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View Lastest Price from 2-AMINO-3-CHLORO-5-NITROPYRIDINE manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 2-AMINO-3-CHLORO-5-NITROPYRIDINE 22353-35-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2025-06-03

Henan Fengda Chemical Co., Ltd

Product: 2-AMINO-3-CHLORO-5-NITROPYRIDINE 22353-35-1
Price: US $5.00-0.10/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-08

Dideu Industries Group Limited

Product: 2-AMINO-3-CHLORO-5-NITROPYRIDINE 22353-35-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-22

22353-35-1, 2-AMINO-3-CHLORO-5-NITROPYRIDINERelated Search:

2-AMINO-3-IODO-5-NITROPYRIDINE 3-Chloro-5-(trifluoromethyl)pyridin-2-amine 6-AMINO-5-CHLORO-NICOTINONITRILE 2-AMINO-4-CHLORO-5-NITROPYRIDINE 5-CHLORO-3-PYRIDINAMINE 3-CHLORO-5-NITROPYRIDINE 2-AMINO-3-CHLORO-5-NITROPYRIDINE 3-CHLORO-2-HYDRAZINO-5-NITROPYRIDINE 2-AMINO-6-CHLORO-3-NITROPYRIDINE,6-Amino-2-chloro-5-nitropyridine,2-Amino-6-chloro-3-nitropyridine 98% 3-Amino-2-chloro-4-nitropyridine 4-AMINO-2-CHLORO-3-NITROPYRIDINE 2-AMINO-5-CHLORO-3-NITROPYRIDINE 98+% GC,2-AMINO-5-CHLORO-3-NITROPYRIDINE, 98+%,2-AMINO-5-CHLORO-3-NITROPYRIDINE 2-AMINO-4-CHLORO-3-NITROPYRIDINE 2-Chloro-5-nitropyridin-4-amine 6-Amino-2-chloro-3-nitropyridine 2-AMINO-3-CHLORO-5-NITRO-6-PICOLINE 2-AMINO-3-CHLORO-5-NITRO-4-PICOLINE 2-Amino-5-Chloro-3-NitroPyridine5409392

2-AMINO-3-CHLORO-5-NITROPYRIDINE

3-chloro-5-nitropyridin-2-amine

3-Chloro-5-nitro-2-pyridinamine

Pyridine,2-amino-3-chloro-5-nitro- (6CI,8CI)

2-AMINO-3-CHLORO-5-NITROPYRIDINE, 95+%

3-Chloro-5-nitro-pyridin-2-ylamine

2-Pyridinamine, 3-chloro-5-nitro-

2-AMINO-3-CHLORO-5-NITROPYRIDINE ISO 9001：2015 REACH

2-amino 5-nitro 3-chloro pyridine

22353-35-1

Boronic Acid

Heterocycle-Pyridine series

amine| alkyl chloride| nitro-compound

Pyridine