ChemicalBook > CAS DataBase List > Ethyl nitroacetate
Ethyl nitroacetate
- Product Name
- Ethyl nitroacetate
- CAS No.
- 626-35-7
- Chemical Name
- Ethyl nitroacetate
- Synonyms
- NSC 42302;JACS-626-35-7;2-nitrobutanoate;Ethlnitroacetate;Ethyl nitrocetate;ETHYL NITROACETATE;NITRO ETHYL ACETATE;EthylNitroacetate>Ethylnitroacetate,97%;Ethyl nitroacetate,98%
- CBNumber
- CB1175310
- Molecular Formula
- C4H7NO4
- Formula Weight
- 133.1
- MOL File
- 626-35-7.mol
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Ethyl nitroacetate Property
- Boiling point:
- 105-107 °C/25 mmHg (lit.)
- Density
- 1.199 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.424(lit.)
- Flash point:
- 198 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
- pka
- pK1:5.85 (25°C)
- form
- Liquid
- color
- Clear colorless to slightly yellow
- Water Solubility
- Slightly soluble in water. Soluble in chloroform and ethyl acetate.
- BRN
- 1210027
- InChIKey
- FTKASJMIPSSXBP-UHFFFAOYSA-N
- CAS DataBase Reference
- 626-35-7(CAS DataBase Reference)
- NIST Chemistry Reference
- Acetic acid, nitro-, ethyl ester(626-35-7)
- EPA Substance Registry System
- Acetic acid, nitro-, ethyl ester (626-35-7)
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Safety
- Hazard Codes
- Xi
- Risk Statements
- 38
- Safety Statements
- 23-24/25-37
- WGK Germany
- 2
- RTECS
- AJ1074000
- Hazard Note
- Irritant
- TSCA
- T
- HazardClass
- IRRITANT, KEEP COLD
- HS Code
- 29159080
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H227Combustible liquid
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 192333
- Product name
- Ethyl nitroacetate
- Purity
- 97%
- Packaging
- 5g
- Price
- $43.1
- Updated
- 2024/03/01
Sigma-Aldrich
- Product number
- 192333
- Product name
- Ethyl nitroacetate
- Purity
- 97%
- Packaging
- 25g
- Price
- $166
- Updated
- 2024/03/01
TCI Chemical
- Product number
- N0657
- Product name
- Ethyl Nitroacetate
- Purity
- >95.0%(GC)
- Packaging
- 5g
- Price
- $56
- Updated
- 2024/03/01
TCI Chemical
- Product number
- N0657
- Product name
- Ethyl Nitroacetate
- Purity
- >95.0%(GC)
- Packaging
- 25g
- Price
- $164
- Updated
- 2024/03/01
Alfa Aesar
- Product number
- A14433
- Product name
- Ethyl nitroacetate, 97%
- Packaging
- 5g
- Price
- $63.65
- Updated
- 2024/03/01
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Ethyl nitroacetate Chemical Properties,Usage,Production
Chemical Properties
clear colourless to slightly yellow liquid
Uses
Ethyl nitroacetate has been used in the synthesis of γ-oxoacids via Michael addition reaction with α,β-unsaturated ketones, fuctionalization of C4-position on pyrimidine and C6-position on 2?-deoxyguanosine to produce novel nucleosides, facile synthesis of α,α-diisobutylglycine, synthesis of DL-4,4-difluoroglutamic acid. It is also used as an intermediate in the preparation of unsubstituted amino acids.
Uses
Ethyl Nitroacetate is an ester of nitrocarboxylic acid used as an intermediate in the preparation of unsubstituted amino acids.
Synthesis Reference(s)
The Journal of Organic Chemistry, 59, p. 1208, 1994 DOI: 10.1021/jo00084a047
Purification Methods
Purify the ester by repeated distillation. IR:max 1748 (CO2), 1570 and 1337 (NO2), and 800cm-1 [Haszeldine J Chem Soc 2525 1953]. The hydrazine salt crystallises from 95% EtOH or MeOH as yellow crystals m 104-105o [Ungnade & Kissinger J Org Chem 22 1661 1957, Emmons & Freeman J Am Chem Soc 77 4391 1955]. [Beilstein 2 IV 537.]
Ethyl nitroacetate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Ethyl nitroacetate manufacturers
Hebei Mojin Biotechnology Co., Ltd
- Product
- Ethyl nitroacetate 626-35-7
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 50000KG/month
- Release date
- 2023-09-06
Hebei Guanlang Biotechnology Co., Ltd.
- Product
- Ethyl nitroacetate 626-35-7
- Price
- US $10.00/PCS
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2021-03-11
Honest Joy Holdings Limited
- Product
- Ethyl nitroacetate 626-35-7
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99.1%
- Supply Ability
- 100 tons
- Release date
- 2022-02-21
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