4,5-DICHLOROPYRIMIDINE

Product Name: 4,5-DICHLOROPYRIMIDINE
CAS No.: 6554-61-6
Chemical Name: 4,5-DICHLOROPYRIMIDINE
Synonyms: 4,5-DICHLOROPYRIMIDINE;PyriMidine,4,5-dichloro-;Pyrimidine, 4,5-dichloro- (7CI,8CI,9CI)
CBNumber: CB21010527
Molecular Formula: C4H2Cl2N2
Formula Weight: 148.98
MOL File: 6554-61-6.mol

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4,5-DICHLOROPYRIMIDINE Property

Boiling point:: 82 °C(Press: 34 Torr)
Density: 1.493±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -1.41±0.16(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D438315
Product name: 4,5-Dichloropyrimidine
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD12030
Product name: 4,5-Dichloropyrimidine
Packaging: 100mg
Price: $80
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD12030
Product name: 4,5-Dichloropyrimidine
Packaging: 1g
Price: $400
Updated: 2021/12/16

Matrix Scientific

Product number: 072918
Product name: 4,5-Dichloropyrimidine
Purity: 95+%
Packaging: 5g
Price: $444
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: NUC0001073
Product name: 4,5-DICHLOROPYRIMIDINE
Purity: 95.00%
Packaging: 250MG
Price: $449
Updated: 2021/12/16

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4,5-DICHLOROPYRIMIDINE Chemical Properties,Usage,Production

Synthesis

197228-37-8

6554-61-6

The general procedure for the synthesis of 4,5-dichloropyrimidine from the compound (CAS:197228-37-8) is as follows: 112.5 g (673.7 mmol) of 5-chloro-6-oxo-1,6-dihydropyrimidin-1-ium chloride was mixed with 1.6 mL of dimethylamine in 630 mL of phosphorochloride. The reaction mixture was heated to reflux for 3 hours. Upon completion of the reaction, the excess phosphorus trichloride was removed by distillation under reduced pressure. After the reaction mixture was cooled, it was slowly poured into 1.5 L of ice water. The aqueous phase was extracted with 500 mL of dichloromethane, and the organic phases were combined and dried with anhydrous sodium sulfate. Finally, the organic phase was concentrated by decompression to give 72.3 g of 4,5-dichloropyrimidine in 66.3% yield.

References

[1] Patent: US2007/179295, 2007, A1
[2] Patent: US2007/275985, 2007, A1
[3] Patent: US2007/37828, 2007, A1
[4] Patent: WO2004/113342, 2004, A1. Location in patent: Page/Page column 49
[5] Patent: WO2005/851, 2005, A1. Location in patent: Page/Page column 59

4,5-DICHLOROPYRIMIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4,5-DICHLOROPYRIMIDINE Suppliers

China 104 Europe 1 India 1 United Kingdom 3 United States 10 Global 119

Capot Chemical Co., Ltd

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View Lastest Price from 4,5-DICHLOROPYRIMIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 4,5-Dichloropyrimidine 6554-61-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2020-05-15

Career Henan Chemical Co

Product: 4,5-DICHLOROPYRIMIDINE 6554-61-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-19

6554-61-6, 4,5-DICHLOROPYRIMIDINERelated Search:

2,4,5,6-TETRACHLOROPYRIMIDINE N-(2-Amino-4,6-dichloro-5-pyrimidinyl)formamide 4-BROMO-3,5-DICHLOROPYRIDINE (3,5-DICHLOROPYRIDIN-2-YL)METHANOL 2,5-Diamino-4,6-dihydroxypyrimidine hydrochloride 4,6-Dichloro-2-(methylthio)pyrimidine 2,4-Dichloro-5-fluoropyrimidine 2,5-DICHLOROPYRIMIDINE,PURITY:95% MIN(HPLC) 2,4-dichloro-5-formylpyrimidine 4,6-Dimethyl-2-methylsulfonylpyrimidine 2,5-Diamino-4,6-dichloropyrimidine hydrochloride 2-ETHOXY-4,6-DICHLOROPYRIMIDINE 2,6-Dichloropyridin-3-amine 5-Iodo-2,4-dichloropyrimidine 2,5-DIAMINO-4,6-DICHLOROPYRIMIDINE 98+% 2,4-Dichloropyrimidine, 98+%,2,4-DICHLOROPYRIMIDINE,2-4-DICHLOROPYRIMIDINE CRYSTALLINE,2,4-Dichloropyrimidine, GC 97% Methyl 4,6-dichloropyrimidine-2-carboxylate 4,6-Dichloropyrimidine ,98%,4 6-DICHLOROPYRIMIDINE 99%

4,5-DICHLOROPYRIMIDINE

Pyrimidine, 4,5-dichloro- (7CI,8CI,9CI)

PyriMidine,4,5-dichloro-

6554-61-6

Heterocycle-Pyrimidine series

PYRIMIDINE