ChemicalBook > CAS DataBase List > 2-Fluoro-N-methoxy-N-methylbenzamide

2-Fluoro-N-methoxy-N-methylbenzamide

Product Name
2-Fluoro-N-methoxy-N-methylbenzamide
CAS No.
198967-24-7
Chemical Name
2-Fluoro-N-methoxy-N-methylbenzamide
Synonyms
N-Methoxy-N-Methyl-2-fluorobenzaMide;2-Fluoro-N-methoxy-N-metylbenzamide ;2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE;Benzamide, 2-fluoro-N-methoxy-N-methyl-;FMMB 3-Fluoro-n-methoxy-n-methylbenzamide;2-Fluoro-N-methoxy its-N-methylbenzoyl Amine
CBNumber
CB2199861
Molecular Formula
C9H10FNO2
Formula Weight
183.18
MOL File
198967-24-7.mol
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2-Fluoro-N-methoxy-N-methylbenzamide Property

Boiling point:
299.9±23.0 °C(Predicted)
Density 
1.179±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Appearance
Colorless to light yellow Liquid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
F593778
Product name
2-Fluoro-N-methoxy-N-methylbenzamide
Packaging
100mg
Price
$65
Updated
2021/12/16
TRC
Product number
F593778
Product name
2-Fluoro-N-methoxy-N-methylbenzamide
Packaging
500mg
Price
$220
Updated
2021/12/16
AK Scientific
Product number
0228AB
Product name
2-Fluoro-N-methoxy-N-methylbenzamide
Packaging
1g
Price
$98
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0019969
Product name
2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
Purity
95.00%
Packaging
10G
Price
$1334.03
Updated
2021/12/16
Ambeed
Product number
A285446
Product name
2-Fluoro-N-methoxy-N-methylbenzamide
Purity
95%
Packaging
250mg
Price
$18
Updated
2021/12/16
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2-Fluoro-N-methoxy-N-methylbenzamide Chemical Properties,Usage,Production

Synthesis

6638-79-5

393-52-2

198967-24-7

The general procedure for the synthesis of 2-fluoro-N-methoxy-N-methylbenzamide from dimethylhydroxylamine hydrochloride and o-fluorobenzoyl chloride was as follows: N,O-dimethylhydroxylamine hydrochloride (23.4 g, 240 mmol) was suspended in tetrahydrofuran (THF, 100 mL) and cooled to 0 °C under nitrogen protection. Pyridine (32 mL, 400 mmol) was added rapidly. A solution of o-fluorobenzoyl chloride (9.5 mL, 80 mmol) in THF (50 mL) was added dropwise over 15 minutes. The ice bath was removed and the reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, water (100 mL) and ethyl acetate (AcOEt, 100 mL) were added to separate the organic and aqueous phases. The aqueous phase was extracted again with ethyl acetate (100 mL). All organic phases were combined and washed sequentially with 1N hydrochloric acid (2 x 100 mL) and 1N sodium hydroxide (100 mL). The organic phase was dried with magnesium sulfate (MgSO4) and concentrated to give a yellow oil (10.7 g). The oily substance was purified by vacuum distillation and the colorless oily 2-fluoro-N-methoxy-N-methylbenzamide (9.1 g, 62% yield) distilled at 0.22 Torr, 57-59 °C was collected. The product was characterized by 1H-NMR (300 MHz, CDCl3): δ 3.34 (s, 3H), 3.54 (br, 3H), 7.10 (m, 1H), 7.19 (m, 1H), 7.42 (m, 2H).

References

[1] RSC Advances, 2013, vol. 3, # 26, p. 10158 - 10162
[2] Patent: WO2013/142038, 2013, A2. Location in patent: Paragraph 0130
[3] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 21, p. 6974 - 6992
[4] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 4, p. 1415 - 1419
[5] Patent: WO2006/3096, 2006, A1. Location in patent: Page/Page column 73

2-Fluoro-N-methoxy-N-methylbenzamide Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Fluoro-N-methoxy-N-methylbenzamide manufacturers

Career Henan Chemical Co
Product
2-Fluoro-N-methoxy-N-methylbenzamide 198967-24-7
Price
US $1.00/KG
Min. Order
1KG
Purity
≥98%
Supply Ability
200KG
Release date
2019-08-30

198967-24-7, 2-Fluoro-N-methoxy-N-methylbenzamideRelated Search:

Chlorantraniliprole (Trifluoromethoxy)benzene 3-(Trifluoromethoxy)bromobenzene Benzamide 4-(Trifluoromethoxy)aniline Fluorine 3-FLUORO-4-[(N-METHOXY-N-METHYL)CARBAMOYL]BENZENEBORONIC ACID 98 4-FLUORO-3-(METHOXY(METHYL)CARBAMOYL)PHENYLBORONIC ACID N-METHOXY-N-METHYLBENZAMIDE 2,6-DIFLUORO-N-METHOXY-N-METHYLBENZENECARBOXAMIDE 4-CHLORO-2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 2,4-DIFLUORO-N-METHOXY-N-METHYLBENZAMIDE 2,4,6-TRIFLUORO-N-METHOXY-N-METHYLBENZENECARBOXAMIDE 3-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 4-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 3-bromo-4-fluoro-N-methoxy-N-methylbenzamide 4-BROMO-2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE 2-Fluoro-N-methoxy-N-methylbenzamide

  • 2-FLUORO-N-METHOXY-N-METHYLBENZAMIDE
  • FMMB 3-Fluoro-n-methoxy-n-methylbenzamide
  • 2-Fluoro-N-methoxy-N-metylbenzamide
  • N-Methoxy-N-Methyl-2-fluorobenzaMide
  • Benzamide, 2-fluoro-N-methoxy-N-methyl-
  • 2-Fluoro-N-methoxy its-N-methylbenzoyl Amine
  • 198967-24-7