6-Bromo-3-hydroxypicolinicacid

Product Name: 6-Bromo-3-hydroxypicolinicacid
CAS No.: 321596-58-1
Chemical Name: 6-Bromo-3-hydroxypicolinicacid
Synonyms: 6-Bromo-3-hydroxypicolinicacid;6-BroMo-3-hydroxypyridine-2-carboxylic acid;2-Pyridinecarboxylic acid, 6-bromo-3-hydroxy-
CBNumber: CB22499101
Molecular Formula: C6H4BrNO3
Formula Weight: 218
MOL File: 321596-58-1.mol

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6-Bromo-3-hydroxypicolinicacid Property

Boiling point:: 485.7±45.0 °C(Predicted)
Density: 1.985±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 2.32±0.25(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B993745
Product name: 6-Bromo-3-hydroxypicolinicAcid
Packaging: 100mg
Price: $200
Updated: 2021/12/16

TRC

Product number: B993745
Product name: 6-Bromo-3-hydroxypicolinicAcid
Packaging: 50mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 076584
Product name: 6-Bromo-3-hydroxypicolinic acid
Purity: 95+%
Packaging: 1g
Price: $329
Updated: 2021/12/16

Matrix Scientific

Product number: 076584
Product name: 6-Bromo-3-hydroxypicolinic acid
Purity: 95+%
Packaging: 500mg
Price: $214
Updated: 2021/12/16

AK Scientific

Product number: W5403
Product name: 6-Bromo-3-hydroxypicolinicacid
Packaging: 250mg
Price: $398.8
Updated: 2021/12/16

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6-Bromo-3-hydroxypicolinicacid Chemical Properties,Usage,Production

Synthesis

874-24-8

321596-58-1

General procedure for the synthesis of 6-bromo-3-hydroxypyridine-2-carboxylic acid from 3-hydroxy-2-pyridinecarboxylic acid: to a stirred suspension of 3-hydroxypyridine-2-carboxylic acid (2.00 g, 0.0144 mol) in DMF (30 mL) was slowly added a solution of N-bromosuccinimide (2.56 g, 0.0144 mol) in DMF (30 mL). After 1 h of reaction, water (50 mL) and 1 M NaOH aqueous solution (25 mL) were added, followed by extraction of the reaction mixture with chloroform (3 x 150 mL). The organic layers were combined and concentrated under reduced pressure and the resulting residue was purified by preparative HPLC (System D). The final product 6-bromo-3-hydroxypyridine-2-carboxylic acid was obtained as 366 mg in 12% yield. The product was assayed by analytical HPLC and the purity was 100% in both cases (System A and B); LRESIMS (ESI+) m/z = 218/220 (M + H)+.

References

[1] Patent: WO2009/150144, 2009, A1. Location in patent: Page/Page column 63

6-Bromo-3-hydroxypicolinicacid Preparation Products And Raw materials

Raw materials

Preparation Products

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321596-58-1