6-BROMO-3-CHLOROISOQUINOLINE

Product Name: 6-BROMO-3-CHLOROISOQUINOLINE
CAS No.: 552331-06-3
Chemical Name: 6-BROMO-3-CHLOROISOQUINOLINE
Synonyms: 6-BROMO-3-CHLOROISOQUINOLINE;Isoquinoline, 6-bromo-3-chloro-;6-Bromo-3-chloro-2-azanaphthalene;6-bromanyl-3-chloranyl-isoquinoline;6-BROMO-3-CHLOROISOQUINOLINE ISO 9001：2015 REACH
CBNumber: CB4821407
Molecular Formula: C9H5BrClN
Formula Weight: 242.5
MOL File: 552331-06-3.mol

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6-BROMO-3-CHLOROISOQUINOLINE Property

Boiling point:: 349.5±22.0 °C(Predicted)
Density: 1.673±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 1.28±0.38(Predicted)
form: solid
color: Pale yellow

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H319Causes serious eye irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Frontier Specialty Chemicals

Product number: I11568
Product name: 6-Bromo-3-chloroisoquinoline
Purity: 95%
Packaging: 250mg
Price: $90
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB42244
Product name: 6-Bromo-3-chloroisoquinoline
Packaging: 50mg
Price: $100
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-D-Y8
Product name: 6-Bromo-3-chloroisoquinoline
Purity: 97%
Packaging: 250mg
Price: $135
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB42244
Product name: 6-Bromo-3-chloroisoquinoline
Packaging: 100mg
Price: $160
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: I11568
Product name: 6-Bromo-3-chloroisoquinoline
Purity: 95%
Packaging: 1g
Price: $240
Updated: 2021/12/16

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6-BROMO-3-CHLOROISOQUINOLINE Chemical Properties,Usage,Production

Synthesis

552331-05-2

552331-06-3

General procedure for the synthesis of 6-bromo-3-chloroisoquinoline from 6-bromo-1,3-dichloroisoquinoline: a mixture of 6-bromo-1,3-dichloroisoquinoline (1.8 g, 6.5 mmol), red phosphorus (0.48 g, 15.5 mmol), and hydriodic acid (3 ml, 48%) in acetic acid (20 ml) was heated and refluxed for 8 hours. After completion of the reaction, it was filtered while hot and the filtrate was concentrated under reduced pressure. The concentrated residue was alkalized by addition of sodium hydroxide solution and subsequently extracted with ethyl acetate (200 mL). The organic phase was washed with saturated saline, dried over anhydrous magnesium sulfate, filtered and concentrated. The concentrate was purified by silica gel fast column chromatography to afford 6-bromo-3-chloroisoquinoline (0.81 g, 50% yield) using 30% ethyl acetate/hexane as eluent. Mass spectrum (DCI/NH3) m/e 244 (M+H)+.

References

[1] Patent: US2003/187026, 2003, A1
[2] Patent: US2003/199511, 2003, A1. Location in patent: Page/Page column 34-35

6-BROMO-3-CHLOROISOQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BROMO-3-CHLOROISOQUINOLINE Suppliers

China 84 India 1 United Kingdom 2 United States 10 Global 97

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552331-06-3, 6-BROMO-3-CHLOROISOQUINOLINERelated Search:

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6-BROMO-3-CHLOROISOQUINOLINE

6-Bromo-3-chloro-2-azanaphthalene

6-bromanyl-3-chloranyl-isoquinoline

Isoquinoline, 6-bromo-3-chloro-

6-BROMO-3-CHLOROISOQUINOLINE ISO 9001：2015 REACH

552331-06-3

552331-06-1

Building Blocks

Isoquinoline