ChemicalBook > CAS DataBase List > 2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE

2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE

Product Name
2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE
CAS No.
131747-55-2
Chemical Name
2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE
Synonyms
2-Fluoro-3-pyridinemethanol;2-Fluoro-3-pyridinecarbinol;3-Pyridinemethanol, 2-fluoro-;(2-Fluoropyridin-3-yl)methanol;3-Pyridinemethanol,2-fluoro-(9CI);2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE
CBNumber
CB2375153
Molecular Formula
C6H6FNO
Formula Weight
127.12
MOL File
131747-55-2.mol
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2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE Property

Boiling point:
249℃
Density 
1.262
Flash point:
105℃
storage temp. 
Inert atmosphere,2-8°C
pka
12.94±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
CAS DataBase Reference
131747-55-2(CAS DataBase Reference)
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Frontier Specialty Chemicals
Product number
F12928
Product name
2-(Fluoro-3-pyridine)methanol
Purity
97%
Packaging
1g
Price
$17
Updated
2021/12/16
AK Scientific
Product number
J50839
Product name
2-Fluoro-3-(hydroxymethyl)pyridine
Packaging
1g
Price
$30
Updated
2021/12/16
ChemScene
Product number
CS-D0977
Product name
2-Fluoro-3-(hydroxymethyl)pyridine
Purity
99.90%
Packaging
5g
Price
$50
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
F12928
Product name
2-(Fluoro-3-pyridine)methanol
Purity
97%
Packaging
5g
Price
$65
Updated
2021/12/16
SynQuest Laboratories
Product number
4H01-3-19
Product name
2-Fluoro-3-(Hydroxymethyl)pyridine
Purity
95%
Packaging
1g
Price
$70
Updated
2021/12/16
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2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE Chemical Properties,Usage,Production

Synthesis

36404-90-7

131747-55-2

General procedure for the synthesis of 2-fluoro-3-hydroxymethylpyridine using 2-fluoro-3-pyridinecarboxaldehyde as starting material: sodium borohydride (1.0 g, 26 mmol) was slowly added to a solution of 2-fluoro-3-pyridinecarboxaldehyde (1.6 mL, 16 mmol) in ethanol (14 mL), and the reaction mixture was stirred for 1 hour at room temperature. Upon completion of the reaction, water was added to the reaction mixture, followed by extraction with ethyl acetate. The organic layer was washed with saturated brine, dried over anhydrous magnesium sulfate and filtered. The filtrate was concentrated under reduced pressure to afford the target product 2-fluoro-3-hydroxymethylpyridine (1.3 g, 10 mmol, 63% yield) as a colorless oil.

References

[1] Patent: EP3333163, 2018, A1. Location in patent: Paragraph 1401; 1402
[2] Patent: WO2010/132999, 2010, A1. Location in patent: Page/Page column 98
[3] Patent: WO2011/48082, 2011, A1. Location in patent: Page/Page column 88
[4] Organic Letters, 2017, vol. 19, # 14, p. 3895 - 3898

2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE manufacturers

Honest Joy Holdings Limited
Product
2-Fluoro-3-(hydroxymethyl)pyridine 131747-55-2
Price
US $0.00/KG
Min. Order
1KG
Purity
98.3%
Supply Ability
100 tons
Release date
2022-01-25
Career Henan Chemical Co
Product
2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE 131747-55-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2019-12-25

131747-55-2, 2-FLUORO-3-(HYDROXYMETHYL)PYRIDINERelated Search:

6-FLUORO-2-METHYLNICOTINIC ACID 2-FLUORO-4-IODONICOTINIC ACID 2-FLUORO-4-IODONICOTINIC ACID METHYL ESTER 5-chloro-2-fluoro-3-Pyridinemethanol 2,6-Difluoropyridine-3-carboxylic acid 4,6-Difluoronicotinic acid 6-Fluoronicotinic acid 5-CHLORO-2-FLUORONICOTINIC ACID 2-FLUORO-3-(HYDROXYMETHYL)-4-IODOPYRIDINE 2-Fluoronicotinic acid 2-FLUORONICOTINIC ACID METHYL ESTER 2-FLUORO-3-METHYL-PYRIDINE-5-CARBOXYLIC ACID 6-FLUORONICOTINIC ACID METHYL ESTER 6-Chloro-3-fluoro-2-(hydroxymethyl)pyridine 2-FLUORO-5-(HYDROXYMETHYL)PYRIDINE,6-Fluoro-3-(Hydroxymethyl)Pyridine 2-CHLORO-5-FLUORO-4-(HYDROXYMETHYL)PYRIDINE 2-CHLORO-5-FLUORO-3-(HYDROXYMETHYL)PYRIDINE 3-Pyridinemethanol

  • 2-FLUORO-3-(HYDROXYMETHYL)PYRIDINE
  • 3-Pyridinemethanol,2-fluoro-(9CI)
  • 2-Fluoro-3-pyridinecarbinol
  • 2-Fluoro-3-pyridinemethanol
  • (2-Fluoropyridin-3-yl)methanol
  • 3-Pyridinemethanol, 2-fluoro-
  • 131747-55-2
  • PYRIDINE
  • Pyridines