(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Product Name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- CAS No.
- 103755-58-4
- Chemical Name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Synonyms
- 1-Phenyl-1H-1,2,3-Triazol-4-yl;1H-1,2,3-Triazole-4-methanol, 1-phenyl-;(1-PHENYL-1H-1,2,3-TRIAZOL-4-YL)METHANOL;(1-phenyl-1H-1,2,3-triazole-4-yl)methanol;1-Phenyl-1H-1,2,3-triazole-4-methanol, 97%
- CBNumber
- CB2409760
- Molecular Formula
- C9H9N3O
- Formula Weight
- 175.19
- MOL File
- 103755-58-4.mol
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol Property
- Melting point:
- 114-116°C
- Boiling point:
- 379.9±34.0 °C(Predicted)
- Density
- 1.27±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 12.96±0.10(Predicted)
- CAS DataBase Reference
- 103755-58-4(CAS DataBase Reference)
Safety
- HazardClass
- IRRITANT
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- P337388
- Product name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Packaging
- 250mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 044400
- Product name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Purity
- >95%
- Packaging
- 500mg
- Price
- $46
- Updated
- 2021/12/16
- Product number
- 044400
- Product name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Purity
- >95%
- Packaging
- 1g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- V0637
- Product name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Packaging
- 100mg
- Price
- $89
- Updated
- 2021/12/16
- Product number
- V0637
- Product name
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
- Packaging
- 250mg
- Price
- $99
- Updated
- 2021/12/16
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol Chemical Properties,Usage,Production
Synthesis
107-19-7
622-37-7
103755-58-4
General procedure: Azidobenzene (1 eq.), 2-propyn-1-ol (1.5 eq.) and copper sulfate pentahydrate (0.1 eq.) were dissolved in a solvent mixture of water and acetonitrile (12 mL, water:acetonitrile = 2:1, v/v) at room temperature. Hydrazine hydrate (1 eq.) was added dropwise to the above solution under vigorous stirring. The reaction mixture gradually changed to light yellow or light green color. The progress of the reaction is monitored by thin layer chromatography (TLC) and the reaction is usually completed within a few minutes (see Table 3 for specific times). Upon completion of the reaction, the product usually precipitates as a colorless solid (unless otherwise noted). The reaction mixture is diluted with excess water and subsequently filtered. The collected solid product is washed with water and dried. The resulting solid may be crystallized by dissolution in a suitable solvent or filtered through a pad of diatomaceous earth to obtain analytically pure 1-phenyl-1hydro-4-methanolyl-1,2,3-triazole.
References
[1] New Journal of Chemistry, 2006, vol. 30, # 8, p. 1137 - 1139
[2] Green Chemistry, 2012, vol. 14, # 5, p. 1298 - 1301
[3] Applied Catalysis A: General, 2013, vol. 453, p. 151 - 158
[4] Archiv der Pharmazie, 2015, vol. 348, # 11, p. 796 - 807
[5] New Journal of Chemistry, 2015, vol. 39, # 8, p. 5902 - 5907
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol manufacturers
- Product
- (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol 103755-58-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg;10kg;100kg
- Release date
- 2019-08-29