2,5-DIBROMO-M-XYLENE

Product Name: 2,5-DIBROMO-M-XYLENE
CAS No.: 100189-84-2
Chemical Name: 2,5-DIBROMO-M-XYLENE
Synonyms: 2,5-Dibromo-1,3-dimethylbenzene;5-DIBROMO-M-XYLENE;2,5-DIBROMO-M-XYLENE;2,5-Dibromo-3-methyl-toluene;1,4-DIBROMO-2,6-DIMETHYLBENZENE;Benzene, 2,5-dibroMo-1,3-diMethyl-;D848545 2,5-Dibromo-1,3-dimethylbenzene,98%
CBNumber: CB2665465
Molecular Formula: C8H8Br2
Formula Weight: 263.96
MOL File: 100189-84-2.mol

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2,5-DIBROMO-M-XYLENE Property

Melting point:: 26-28°
Boiling point:: 261.7±35.0 °C(Predicted)
Density: 1.710±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid-liquid mixture
InChI: InChI=1S/C8H8Br2/c1-5-3-7(9)4-6(2)8(5)10/h3-4H,1-2H3
InChIKey: XXFGKGMZLZIPCN-UHFFFAOYSA-N
SMILES: C1(C)=CC(Br)=CC(C)=C1Br

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D426120
Product name: 2,5-Dibromo-m-xylene
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: D426120
Product name: 2,5-Dibromo-m-xylene
Packaging: 500mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: J53399
Product name: 2,5-Dibromo-1,3-dimethylbenzene
Packaging: 1g
Price: $10
Updated: 2021/12/16

AK Scientific

Product number: B844
Product name: 2,5-Dibromo-1,3-dimethylbenzene
Packaging: 1g
Price: $14
Updated: 2021/12/16

Oakwood

Product number: 018507
Product name: 2,5-Dibromo-m-xylene
Packaging: 1g
Price: $15
Updated: 2021/12/16

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2,5-DIBROMO-M-XYLENE Chemical Properties,Usage,Production

Synthesis

24596-19-8

100189-84-2

General procedure for the synthesis of 2,5-dibromo-m-xylene from 4-bromo-2,6-dimethylaniline: 4-bromo-2,6-dimethylaniline (6.00 g, 30 mmol) was suspended in a 48% aqueous hydrobromic acid solution (20 mL), cooled to -10 °C, then sodium nitrite (2.28 g, 33 mmol) dissolved in water was slowly added, and the mixture was kept at that temperature with continuous stirring for 1 hour. Subsequently, sulfamic acid (0.58 g, 6 mmol) was added to quench the excess nitrite. The reaction mixture was transferred to a 48% aqueous hydrobromic acid solution (20 mL) containing ferrous sulfate heptahydrate (4.17 g, 15 mmol), gradually warmed to 80 °C and stirred at this temperature for 1 hour. After completion of the reaction, water was added to the mixture and extracted with hexane. The organic phases were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. Finally, the target product 2,5-dibromo m-xylene (6.19 g, 72% yield) was purified by medium-pressure column chromatography (silica gel as stationary phase and hexane as mobile phase).

References

[1] Journal of the American Chemical Society, 2018, vol. 140, # 18, p. 5925 - 5933
[2] Patent: JP2018/90535, 2018, A. Location in patent: Paragraph 0072; 0073; 0082; 0083
[3] Patent: JP2018/90536, 2018, A. Location in patent: Paragraph 0098; 0099; 0100; 0101
[4] Journal of Porphyrins and Phthalocyanines, 2010, vol. 14, # 9, p. 804 - 814
[5] Journal of Organic Chemistry, 2012, vol. 77, # 4, p. 2074 - 2079

2,5-DIBROMO-M-XYLENE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,5-DIBROMO-M-XYLENE Suppliers

China 102 France 1 India 2 Lithuania 1 United Kingdom 4 United States 11 Global 121

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View Lastest Price from 2,5-DIBROMO-M-XYLENE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2,5-DIBROMO-M-XYLENE 100189-84-2
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-14

Henan Fengda Chemical Co., Ltd

Product: 2,5-DIBROMO-M-XYLENE 100189-84-2
Price: US $101.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-28

Career Henan Chemical Co

Product: 2,5-dibromo-1,3-dimethylbenzene 100189-84-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons/month
Release date: 2020-01-09

100189-84-2, 2,5-DIBROMO-M-XYLENERelated Search:

4,5-DIBROMO-O-XYLENE 5-Bromo-m-xylene à,à'-dibromo-m-xylene,alpha,alpha'-Dibromo-meta-xylene,α,α’-dibromo-m-xylen 2,5-Dibromotoluene 2,5-DIBROMO-P-XYLENE,2,5-DIBROMO-P-XYLENE, 98+%,2,5-DIBROMO-4-XYLENE alpha,alpha'-Dibromo-p-xylene ALPHA,ALPHA-DIBROMO-O-XYLENE,ALPHA,ALPHA'-DIBROMO-2-XYLENE,alpha,alpha '-Dibromo-ortho-xylene,α,α’-dibromo-o-xylen alpha-Dibromo-m-xylene 4,5-Dibromo-m-xylene 3,5-Dibromo-o-xylene A,A'-DIBROMO-P-XYLENE-D8,ALPHA,ALPHA'-DIBROMO-P-XYLENE-D8 1,4-DIBROMO-O-XYLENE 2,5-DIBROMO-M-XYLENE 1,4-DIBROMO-2,3,5,6-TETRAMETHYLBENZENE 2,5-Dibromo-1,3-diethylbenzene OMEGA,OMEGA'-DIBROMO-O-XYLENE Ω,Ω'-DIBROMO-P-XYLENE A.A'-DIBROMO-M-XYLENE SOLUTION 100UG/ML IN HEXANE 5X1ML

2,5-DIBROMO-M-XYLENE

1,4-DIBROMO-2,6-DIMETHYLBENZENE

2,5-Dibromo-1,3-dimethylbenzene

Benzene, 2,5-dibroMo-1,3-diMethyl-

5-DIBROMO-M-XYLENE

D848545 2,5-Dibromo-1,3-dimethylbenzene,98%

2,5-Dibromo-3-methyl-toluene

100189-84-2

Bromine Compounds