ChemicalBook > CAS DataBase List > Methyl 2-(bromomethyl)-4-methoxybenzoate
Methyl 2-(bromomethyl)-4-methoxybenzoate
- Product Name
- Methyl 2-(bromomethyl)-4-methoxybenzoate
- CAS No.
- 15365-25-0
- Chemical Name
- Methyl 2-(bromomethyl)-4-methoxybenzoate
- Synonyms
- NISTC15365250;METHYL 2-BROMOMETHYL-4-METHOXY-BENZOATE;p-Anisic acid, 2-bromomethyl-, methyl ester;2-BROMOMETHYL-4-METHOXYBENZOICACID,METHYLESTER;Benzoic acid, 2-(broMoMethyl)-4-Methoxy-, Methyl ester
- CBNumber
- CB3104220
- Molecular Formula
- C10H11BrO3
- Formula Weight
- 259.1
- MOL File
- 15365-25-0.mol
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Methyl 2-(bromomethyl)-4-methoxybenzoate Property
- Melting point:
- 51 °C
- Boiling point:
- 350.4±32.0 °C(Predicted)
- Density
- 1.432±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
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N-Bromosuccinimide Price
TRC
- Product number
- M296168
- Product name
- Methyl2-(bromomethyl)-4-methoxybenzoate
- Packaging
- 25mg
- Price
- $45
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 072736
- Product name
- Methyl 2-bromomethyl-4-methoxybenzoate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $155
- Updated
- 2021/12/16
AK Scientific
- Product number
- W3346
- Product name
- Methyl2-bromomethyl-4-methoxybenzoate
- Packaging
- 5g
- Price
- $291
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 072736
- Product name
- Methyl 2-bromomethyl-4-methoxybenzoate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $306
- Updated
- 2021/12/16
AK Scientific
- Product number
- W3346
- Product name
- Methyl2-bromomethyl-4-methoxybenzoate
- Packaging
- 10g
- Price
- $451
- Updated
- 2021/12/16
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Methyl 2-(bromomethyl)-4-methoxybenzoate Chemical Properties,Usage,Production
Uses
Methyl 2-(bromomethyl)-4-methoxybenzoate
Synthesis
35598-05-1
15365-25-0
The general procedure for the synthesis of methyl 2-bromomethyl-4-methoxybenzoate from methyl 4-methoxy-2-methylbenzoate was as follows: N-bromosuccinimide (1.1 g, 6.2 mmol) and a catalytic amount of methyl 4-methoxy-2-methylbenzoate (1 g, 5.6 mmol) were pre-dissolved in carbon tetrachloride (5 mL), which was subsequently added dropwise to a solution containing 25 mL of carbon tetrachloride. After addition of benzoyl peroxide, the reaction mixture was refluxed for 2 hours. After completion of the reaction, it was cooled to room temperature and the mixture was poured into ice water. The aqueous phase was extracted with dichloromethane (3×), and the combined organic phases were dried over magnesium sulfate, filtered, and concentrated under vacuum to afford 2.1 g of the target product, methyl 2-bromomethyl-4-methoxybenzoate, as a light yellow solid in about 100% yield. Mass spectrometry analysis showed [M + H+] m/z 260.
References
[1] Patent: WO2011/85261, 2011, A1. Location in patent: Page/Page column 36
[2] Patent: WO2011/85128, 2011, A1. Location in patent: Page/Page column 56
[3] Journal of Medicinal Chemistry, 1987, vol. 30, # 10, p. 1798 - 1806
[4] Patent: US2008/249101, 2008, A1. Location in patent: Page/Page column 40
[5] Patent: WO2008/20306, 2008, A2. Location in patent: Page/Page column 35
Methyl 2-(bromomethyl)-4-methoxybenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 2-(bromomethyl)-4-methoxybenzoate manufacturers
Career Henan Chemical Co
- Product
- Methyl 2-(bromomethyl)-4-methoxybenzoate 15365-25-0
- Price
- US $6.68/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2020-01-10
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