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3-Bromophthalide

Product Name
3-Bromophthalide
CAS No.
6940-49-4
Chemical Name
3-Bromophthalide
Synonyms
TALM-002;3-BromophthaL;BROMOPHTHALIDE;3-Bromophtalide;3-BROMOPHTHALIDE;3-bromophthalein;3-Bromophthalide97%;3-Bromophthalide 3-;3-Bromophthalide >3-BROMOPHTHALIDE 98+%
CBNumber
CB3157574
Molecular Formula
C8H5BrO2
Formula Weight
213.03
MOL File
6940-49-4.mol
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3-Bromophthalide Property

Melting point:
86°C
Boiling point:
138 °C / 3mmHg
Density 
1.768±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
soluble in Methanol
form 
powder to crystal
color 
White to Light yellow to Light orange
InChIKey
CLMSHAWYULIVFQ-UHFFFAOYSA-N
CAS DataBase Reference
6940-49-4(CAS DataBase Reference)
EPA Substance Registry System
1(3H)-Isobenzofuranone, 3-bromo- (6940-49-4)
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Safety

Risk Statements 
38-41
Safety Statements 
26-36/37/39
HS Code 
2932209090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B1068
Product name
3-Bromophthalide
Purity
>98.0%(T)
Packaging
5g
Price
$55
Updated
2024/03/01
TCI Chemical
Product number
B1068
Product name
3-Bromophthalide
Purity
>98.0%(T)
Packaging
25g
Price
$144
Updated
2024/03/01
Oakwood
Product number
113900
Product name
3-Bromophthalide
Purity
97%
Packaging
1g
Price
$15
Updated
2021/12/16
Oakwood
Product number
113900
Product name
3-Bromophthalide
Purity
97%
Packaging
5g
Price
$45
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB33933
Product name
3-Bromophthalide
Packaging
50g
Price
$67.5
Updated
2021/12/16
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3-Bromophthalide Chemical Properties,Usage,Production

Synthesis

3-Bromophthalide is produced by reacting phthalide with N-bromosuccinimide in carbon tetrachloride solution.
Ten grams (0.075 mole) of phthalide (Note 1), 13.3 g. (0.075 mole) of N-bromosuccinimide, and 200 ml. of dry carbon tetrachloride are refluxed for 30 minutes in a 500-ml. flask carrying a reflux condenser equipped with a drying tube containing Drierite. The reaction mixture is exposed to the light of an ordinary 100-watt unfrosted light bulb placed 6–8 in. from the flask. The end of the reaction is indicated by the disappearance of N-bromosuccinimide from the bottom of the flask and accumulation of succinimide at the top of the reaction mixture. The succinimide is removed by filtration and the filtrate concentrated under atmospheric pressure to 15–20 ml. Cooling of this concentrate followed by filtration gives 12–13 g. (75–81%) of crude 3-bromophthalide, m.p. 74–80°. The crude material, when recrystallized from cyclohexane, gives colorless plates, m.p. 78–80°.

3-Bromophthalide Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromophthalide Suppliers

SHANGHAI BANGCHENG CHEMICAL Co.,Ltd.
Tel
021-69106960 13701823733
Fax
021-69106780
Email
13701823733@163.com
Country
China
ProdList
4767
Advantage
60
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44689
Advantage
61
Wuhan Chemwish Technology Co., Ltd
Tel
86-027-67849912
Fax
86-027-87531808
Email
sales@chemwish.com
Country
China
ProdList
35896
Advantage
56
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Email
sales@capotchem.com
Country
China
ProdList
18207
Advantage
66
Shanghai Sinch Parmaceuticals Tech. Co. Ltd.
Tel
+86-21-54098501
Fax
+86-21-54096319
Email
sales@sinch.com.cn
Country
China
ProdList
11598
Advantage
64
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11655
Advantage
64
XiaoGan ShenYuan ChemPharm co,ltd
Tel
15527768850
Email
1791901229@qq.com
Country
China
ProdList
8844
Advantage
52
Syntechem Co.,Ltd
Tel
Fax
E-Mail Inquiry
Email
info@syntechem.com
Country
China
ProdList
12984
Advantage
57
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View Lastest Price from 3-Bromophthalide manufacturers

ShenZhen H&D Pharmaceutical Technology Co., LTD
Product
Butyphthalide impurity 88 6940-49-4
Price
US $0.00-0.00/mg
Min. Order
10mg
Purity
0.98
Supply Ability
5g
Release date
2024-05-24
Hebei Zhanyao Biotechnology Co. Ltd
Product
3-Bromophthalide 6940-49-4
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 tons
Release date
2021-10-08
Zhuozhou Wenxi import and Export Co., Ltd
Product
3-Bromophthalide 6940-49-4
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10

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