ChemicalBook > CAS DataBase List > Pipecolamide

Pipecolamide

Product Name: Pipecolamide
CAS No.: 19889-77-1
Chemical Name: Pipecolamide
Synonyms: Pipecolamide;pipecolinamide;piperidinecarboxamide;Revefenacin Impurity 51;piperidine-2-carboxamide;2-Piperidinecarboxamide>Piperidine-2-carboxylic acid aMide
CBNumber: CB3947740
Molecular Formula: C6H12N2O
Formula Weight: 128.17
MOL File: 19889-77-1.mol

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Pipecolamide Property

Melting point:: 138-140°
Boiling point:: 311.7±31.0 °C(Predicted)
Density: 1.060±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: slightly sol. in Methanol
form: powder to crystal
pka: 16.77±0.20(Predicted)
color: White to Almost white
InChI: InChI=1S/C6H12N2O/c7-6(9)5-3-1-2-4-8-5/h5,8H,1-4H2,(H2,7,9)
InChIKey: XIMBESZRBTVIOD-UHFFFAOYSA-N
SMILES: N1CCCCC1C(N)=O

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36
HazardClass: IRRITANT
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical

Product number: P2028
Product name: 2-Piperidinecarboxamide
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $224
Updated: 2025/07/31

TRC

Product number: B448923
Product name: Piperidine-2-carboxamide
Packaging: 250mg
Price: $90
Updated: 2021/12/16

TRC

Product number: B448923
Product name: Piperidine-2-carboxamide
Packaging: 50mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: X0387
Product name: Piperidine-2-carboxamide
Packaging: 1g
Price: $67
Updated: 2021/12/16

Matrix Scientific

Product number: 043536
Product name: 2-Piperidinecarboxamide
Purity: 97%
Packaging: 5g
Price: $49
Updated: 2021/12/16

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Pipecolamide Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

28697-07-6

19889-77-1

General procedure for the synthesis of 2-piperidinecarboxamide from 1-N-benzyloxycarbonyl-2-piperidinecarboxylic acid:[Ref. Example 19] To a dichloromethane (20 mL) containing N-benzyloxycarbonylpiperidine-2-carboxylic acid (2.0 g), 1-hydroxybenzotriazole (1.6 g), and 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (2.3 g) at room temperature Concentrated ammonia (3 mL) and triethylamine (2 mL) were added to the solution, followed by stirring the reaction mixture for 3 days. Upon completion of the reaction, the mixture was partitioned between water and dichloromethane. The organic layer was dried with anhydrous magnesium sulfate, filtered and the solvent was evaporated under reduced pressure. The residue was dissolved in methanol (30 mL), 10% palladium-carbon catalyst (1 g, 50% wet) was added and stirred under hydrogen atmosphere for 20 hours. At the end of the reaction, the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to give the 2-piperidinecarboxamide solid product (970 mg, quantitative yield). m/z MS (ESI): 128 (M+).

References

[1] Patent: EP1762568, 2007, A1. Location in patent: Page/Page column 37-38

Pipecolamide Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Pipecolamide manufacturers

Anhui Dexinjia Biopharm Co., Ltd

Product: Piperidine-2-carboxamide 19889-77-1
Price: US $15.00-50.00/kg
Min. Order: 1kg
Purity: NLT98%
Supply Ability: 5 ton per month
Release date: 2023-04-02

Hebei Yanxi Chemical Co., Ltd.

Product: Pipecolamide 19889-77-1
Price: US $50.00/kg
Min. Order: 1kg
Purity: 0.99
Supply Ability: 10000
Release date: 2023-10-09

Qiuxian Baitai New Material Co., LTD

Product: 2-piperidine carboxamide 19889-77-1
Price: US $75.00/g
Min. Order: 1KG
Purity: 99%
Supply Ability: 5ton/Month
Release date: 2021-12-15

19889-77-1, PipecolamideRelated Search:

4-PIPERIDINECARBOXYLIC ACID T-BUTYL ESTER HCL Piperidine-3,5-dione hydrochloride METHYL PIPECOLINATE HYDROCHLORIDE 2,6-piperidinedicarboxylic acid 2-FORMYLPIPERIDINE HYDROCHLORIDE Ethyl piperidine-2-carboxylate hydrochloride VERRUCULOGEN Mepivacaine hydrochloride Pirlimycin Saquinavir Posatirelin Ropivacaine Bupivacaine Mepivacaine (S)-1-N-BOC-PIPECOLAMIDE 2',6'-Pipecoloxylidide Levobupivacaine hydrochloride H-D-Phe-Pip-Arg-pNA acetate

piperidinecarboxamide

Piperidine-2-carboxylic acid aMide

pipecolinamide

Pipecolamide

piperidine-2-carboxamide

2-Piperidinecarboxamide&gt

Revefenacin Impurity 51

19889-77-1