2-IODO-5-METHOXYANILINE

Product Name: 2-IODO-5-METHOXYANILINE
CAS No.: 153898-63-6
Chemical Name: 2-IODO-5-METHOXYANILINE
Synonyms: 2-IODO-5-METHOXYANILINE;2-Iodo-5-methoxybenzenamine;2-Iodo-5-methoxy-phenylamine;BenzenaMine, 2-iodo-5-Methoxy-;1H-Pyrazol-5-amine,1-(3-methylethyl)-
CBNumber: CB4130950
Molecular Formula: C7H8INO
Formula Weight: 249.05
MOL File: 153898-63-6.mol

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2-IODO-5-METHOXYANILINE Property

Melting point:: 33-36 °C(Solv: ethyl acetate (141-78-6))
Boiling point:: 298.4±30.0 °C(Predicted)
Density: 1.807±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka: 2.11±0.10(Predicted)
Appearance: White to light brown Solid
InChI: InChI=1S/C7H8INO/c1-10-5-2-3-6(8)7(9)4-5/h2-4H,9H2,1H3
InChIKey: CYDBBGSUZRDOPE-UHFFFAOYSA-N
SMILES: C1(N)=CC(OC)=CC=C1I

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: I708655
Product name: 2-Iodo-5-methoxyaniline
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: W3349
Product name: 2-Iodo-5-methoxyaniline
Packaging: 5g
Price: $444
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049825
Product name: 2-IODO-5-METHOXYANILINE
Purity: 95.00%
Packaging: 1G
Price: $852.55
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049825
Product name: 2-IODO-5-METHOXYANILINE
Purity: 95.00%
Packaging: 2.5G
Price: $1227.82
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049825
Product name: 2-IODO-5-METHOXYANILINE
Purity: 95.00%
Packaging: 5G
Price: $1548.26
Updated: 2021/12/16

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2-IODO-5-METHOXYANILINE Chemical Properties,Usage,Production

Synthesis

58755-70-7

153898-63-6

General procedure for the synthesis of 2-iodo-5-methoxyaniline from 4-iodo-3-nitroanisole: To a 100 mL methanol solution of 4-iodo-3-nitroanisole (5 g, 17.9 mmol) was added FeCl3 (50 mg, 0.3 mmol) and activated carbon (40 mg). The mixture was heated to reflux and hydrazine hydrate (1.75 g, 35 mmol) was added slowly and dropwise. After keeping the reaction at reflux for 8 h, it was cooled to room temperature and the reaction mixture was filtered through diatomaceous earth. The filtrate was concentrated and purified by column chromatography (eluent: hexane solution of 10% ethyl acetate) to afford 4.05 g of the target product 2-iodo-5-methoxyaniline as a light yellow oil (91% yield).1H NMR (300 MHz, CDCl3) δ 7.47 (1H, d, J = 8.7 Hz), 6.31 (1H, d, J = 2.8 Hz), 6.13 (1H, d, J = 2.8 Hz) 6.13 (1H, dd, J = 2.8, 8.7 Hz), 3.73 (3H, s).

References

[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358
[2] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[3] Patent: WO2003/106462, 2003, A1. Location in patent: Page 110
[4] Tetrahedron Letters, 2008, vol. 49, # 2, p. 363 - 366
[5] Angewandte Chemie - International Edition, 2010, vol. 49, # 48, p. 9262 - 9265

2-IODO-5-METHOXYANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-IODO-5-METHOXYANILINE Suppliers

China 88 Germany 1 India 3 United States 7 Global 99

Alchem Pharmtech,Inc.

Tel: 8485655694
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Aladdin Scientific

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Aceschem Inc.

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Synthonix Inc

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Matrix Scientific

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Ryan Scientific, Inc.

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BOSCHE SCIENTIFIC, LLC

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Email: Sales@BoscheSci.com
Country: United States
ProdList: 6477
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View Lastest Price from 2-IODO-5-METHOXYANILINE manufacturers

Career Henan Chemical Co

Product: 2-IODO-5-METHOXYANILINE 153898-63-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-28

153898-63-6, 2-IODO-5-METHOXYANILINERelated Search:

3-Methoxy-2-methylaniline Butanoic acid, 4-oxo-4-(propyl(2,4,6-triiodo-3-methoxyphenyl)amino)- ( 9CI) 2-NITRO-4-(TRIFLUOROMETHOXY)IODOBENZENE 2,2-DIFLUORO-5-AMINO-6-IODO-1,3-BENZODIOXOLE Iolixanic acid iopronic acid 5-IODO-6-NITRO-1,3-BENZODIOXOLE Butanoic acid, 4-(methyl(2,4,6-triiodo-3-propoxyphenyl)amino)-4-oxo- 4-IODO-3-NITROANISOLE 2-IODO-5-METHOXYANILINE

2-IODO-5-METHOXYANILINE

BenzenaMine, 2-iodo-5-Methoxy-

2-Iodo-5-methoxy-phenylamine

2-Iodo-5-methoxybenzenamine

1H-Pyrazol-5-amine,1-(3-methylethyl)-

153898-63-6