N-Ethyl-4-methoxybenzylamine
- Product Name
- N-Ethyl-4-methoxybenzylamine
- CAS No.
- 22993-76-6
- Chemical Name
- N-Ethyl-4-methoxybenzylamine
- Synonyms
- NSC 165789;N-Ethyl-4-methoxybenzylamine;N-Ethyl-p-Methoxy-benzylaMine;N-Ethyl-N-(4-methoxybenzyl)amine;N-[(4-methoxyphenyl)methyl]ethanamine;Benzenemethanamine, N-ethyl-4-methoxy-
- CBNumber
- CB41459678
- Molecular Formula
- C10H15NO
- Formula Weight
- 165.23
- MOL File
- 22993-76-6.mol
N-Ethyl-4-methoxybenzylamine Property
- Melting point:
- 180-180.5℃
- Boiling point:
- 244℃
- Density
- 0.9903 g/cm3 (20℃)
- refractive index
- 1.5195 (589.3 nm 20℃)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- solubility
- soluble in Ether, Methanol
- form
- Oil
- pka
- 10.17±0.10(Predicted)
- color
- Light Brown
- InChI
- InChI=1S/C10H15NO/c1-3-11-8-9-4-6-10(12-2)7-5-9/h4-7,11H,3,8H2,1-2H3
- InChIKey
- SYGACMXWLAQEPN-UHFFFAOYSA-N
- SMILES
- C1(CNCC)=CC=C(OC)C=C1
Safety
- HS Code
- 2922290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- PH009847
- Product name
- N-(4-methoxybenzyl)ethanamine
- Purity
- AldrichCPR
- Packaging
- 100MG
- Price
- $172
- Updated
- 2023/06/20
- Product number
- E925040
- Product name
- N-Ethyl-4-methoxybenzenemethanamine
- Packaging
- 1g
- Price
- $970
- Updated
- 2021/12/16
- Product number
- CHM0145222
- Product name
- ETHYL[(4-METHOXYPHENYL)METHYL]AMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1593.9
- Updated
- 2021/12/16
- Product number
- CHM0145222
- Product name
- ETHYL[(4-METHOXYPHENYL)METHYL]AMINE
- Purity
- 95.00%
- Packaging
- 100MG
- Price
- $704.55
- Updated
- 2021/12/16
- Product number
- V4536
- Product name
- N-Ethyl-4-methoxybenzenemethanamine
- Packaging
- 250mg
- Price
- $77
- Updated
- 2021/12/16
N-Ethyl-4-methoxybenzylamine Chemical Properties,Usage,Production
Chemical Properties
Light Brown Oil
Uses
N-Ethyl-4-methoxybenzenemethanamine (cas# 22993-76-6) is a compound useful in organic synthesis.
Synthesis
123-11-5
75-04-7
121-44-8
22993-76-6
N-Ethyl-4-methoxybenzylamine was synthesized as follows: anisaldehyde (15.6 g, 115 mmol) was mixed with ethylamine (2.0 M solution of THF, 87 mL, 174 mmol) in 1,2-dichloroethane (450 mL) under the protection of nitrogen, followed by the addition of glacial acetic acid (10.0 mL, 174 mmol). The reaction mixture was stirred at room temperature for 30 min and then cooled to 0 °C with an ice bath. Sodium triacetoxyborohydride (NaBH(OAc)3, 36.9 g, 174 mmol) was added in batches, after which the reaction mixture was stirred at room temperature overnight. After completion of the reaction, the mixture was concentrated and the residue was diluted with an alkaline solution (10 g NaOH dissolved in 100 mL of water) to a slightly alkaline color. The aqueous layer was extracted with ether and the organic phases were combined, washed sequentially with water and brine, dried and concentrated. The residue was purified by silica gel column chromatography, eluting first with dichloromethane solution containing 5% methanol, then with dichloromethane solution containing 4% triethylamine in 50% methanol, to afford the target product N-ethyl-4-methoxybenzylamine (11.2 g, 59% yield) as an oil.
References
[1] Patent: US5677346, 1997, A
N-Ethyl-4-methoxybenzylamine Preparation Products And Raw materials
Raw materials
Preparation Products
N-Ethyl-4-methoxybenzylamine Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11035
- Advantage
- 64
- Tel
- 021-50135380
- shchemsky@sina.com
- Country
- China
- ProdList
- 32321
- Advantage
- 50
- Tel
- 021-58388037;21-58388037 13472507714
- 35177634@qq.com;1589045147@qq.com
- Country
- China
- ProdList
- 803
- Advantage
- 55
- Tel
- 86-21-34053660
- Fax
- 86-21-34053661
- sale@labgogo.com
- Country
- China
- ProdList
- 9865
- Advantage
- 52
- Tel
- 150-2103-5486 18017383231
- Fax
- qq：2817624287
- 983544897@qq.com
- Country
- China
- ProdList
- 9342
- Advantage
- 55
- Tel
- +86-28-85122536 85324413
- Fax
- +86-28-85326443
- market@astatech.cn
- Country
- China
- ProdList
- 8026
- Advantage
- 55
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 022-022-23301225 18202662021
- Fax
- 022-25541300
- Mingmingxuetsu@163.com
- Country
- China
- ProdList
- 313
- Advantage
- 56
View Lastest Price from N-Ethyl-4-methoxybenzylamine manufacturers
- Product
- N-Ethyl-4-methoxybenzylamine 22993-76-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-07-03