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ChemicalBook > CAS DataBase List > 2-Iodobenzyl bromide

2-Iodobenzyl bromide

Application
Product Name
2-Iodobenzyl bromide
CAS No.
40400-13-3
Chemical Name
2-Iodobenzyl bromide
Synonyms
2-Iodobenzyl bromid;2-IODOBENZYL BROMIDE;O-IODOBENZYL BROMIDE;à-bromo-2-iodotoluene;a-Bromo-2-iodotoluene;α-Bromo-2-iodotoluene;o-Iodobenzoyl Bromide;2-IodobenzylBromide>2-Iodobenzylbromide,96%;ALPHA-BROMO-2-IODOTOLUENE
CBNumber
CB4180430
Molecular Formula
C7H6BrI
Formula Weight
296.93
MOL File
40400-13-3.mol
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2-Iodobenzyl bromide Property

Melting point:
54-60 °C(lit.)
Boiling point:
125 °C / 4mmHg
Density 
2.105±0.06 g/cm3(Predicted)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
solubility 
soluble in Methanol
form 
Crystalline Powder
color 
White to cream
Sensitive 
Light Sensitive
BRN 
2079736
CAS DataBase Reference
40400-13-3(CAS DataBase Reference)
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Safety

Hazard Codes 
C,N,T
Risk Statements 
22-34-43-51/53-63-42/43-36/37/38
Safety Statements 
26-36/37/39-61-45-23
RIDADR 
UN 3261 8/PG 2
WGK Germany 
2
HazardClass 
8
PackingGroup 
Ⅱ
HS Code 
29039990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

H334May cause allergy or asthma symptoms or breathing difficulties if inhaled

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
634603
Product name
2-Iodobenzyl bromide
Purity
97%
Packaging
5g
Price
$78.3
Updated
2022/05/15
TCI Chemical
Product number
I0635
Product name
2-Iodobenzyl Bromide
Packaging
1G
Price
$23
Updated
2025/07/31
TCI Chemical
Product number
I0635
Product name
2-Iodobenzyl Bromide
Packaging
5G
Price
$66
Updated
2025/07/31
TRC
Product number
I737230
Product name
2-Iodobenzyl bromide
Packaging
2.5g
Price
$75
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0020091
Product name
2-IODO BENZYL BROMIDE
Purity
95.00%
Packaging
5G
Price
$866.75
Updated
2021/12/16
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2-Iodobenzyl bromide Chemical Properties,Usage,Production

Application

2-Iodobenzylmethyl bromide is a halocarbon compound mainly used in laboratory research and development processes and chemical production processes.

Chemical Properties

White solid

Synthesis

5159-41-1

40400-13-3

General procedure for the synthesis of 2-iodobenzyl bromide from 2-iodobenzyl alcohol: 48% hydrobromic acid (10 mL) and 98% sulfuric acid (2 mL) were added to 2-iodobenzyl alcohol (0.94 g, 4.0 mmol). The resulting suspension was placed in an oil bath and heated and stirred at 150 °C for 2 hours. After completion of the reaction, the mixture was cooled to room temperature and extracted with dichloromethane (2 x 10 mL). The organic layers were combined, dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by fast column chromatography (silica gel, 0-20% dichloromethane/hexane gradient elution) to afford the target compound 2-iodobenzyl bromide (1.0 g, 84% yield).

References

[1] Tetrahedron, 2005, vol. 61, # 13, p. 3311 - 3324
[2] Journal of Organic Chemistry, 2012, vol. 77, # 13, p. 5705 - 5713
[3] Helvetica Chimica Acta, 1995, vol. 78, p. 765 - 771
[4] Tetrahedron, 1993, vol. 49, # 20, p. 4439 - 4446
[5] Tetrahedron, 2002, vol. 58, # 44, p. 9007 - 9018

2-Iodobenzyl bromide Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Iodobenzyl bromide Suppliers

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View Lastest Price from 2-Iodobenzyl bromide manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2-Iodobenzyl bromide 40400-13-3
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2024-11-07
Hebei Zhuanglai Chemical Trading Co.,Ltd
Product
2-Iodobenzyl bromide 40400-13-3
Price
US $10.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20ton
Release date
2024-06-07
Henan Fengda Chemical Co., Ltd
Product
2-Iodobenzyl bromide 40400-13-3
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26

40400-13-3, 2-Iodobenzyl bromideRelated Search:

1,2-Diiodobenzene Bromotrimethylsilane Rocuronium bromide 2-Iodobenzoic acid Ethidium bromide Allyl bromide 2-(Trifluoromethyl)benzyl chloride 2-Bromophenol 1,4-Diiodobenzene 2-(Chloromethyl)benzonitrile (Diacetoxyiodo)benzene alpha-Chloro-o-fluorotoluene 2-Chlorobenzyl chloride Benzyl bromide Sodium bromate 4-Nitrobenzyl bromide Methyl bromide 3-IODOBENZYL BROMIDE,M-IODOBENZYL BROMIDE,m-Iodobenzyl Bromide 3-Iodobenzyl Bromide,3-Iodobenzyl bromide, 98+%,3-Iodobenzyl bromide 99%

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