4-Bromomethylbenzamide
- Product Name
- 4-Bromomethylbenzamide
- CAS No.
- 58914-40-2
- Chemical Name
- 4-Bromomethylbenzamide
- Synonyms
- DK831;4-Bromomethylbenzamide;Benzamide, 4-(bromomethyl)-
- CBNumber
- CB42471118
- Molecular Formula
- C8H8BrNO
- Formula Weight
- 214.06
- MOL File
- 58914-40-2.mol
4-Bromomethylbenzamide Property
- Melting point:
- 179-181 °C(Solv: ethyl acetate (141-78-6); chloroform (67-66-3))
- Boiling point:
- 338.4±25.0 °C(Predicted)
- Density
- 1.555±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 15.88±0.50(Predicted)
- form
- liquid
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
N-Bromosuccinimide Price
- Product number
- B870130
- Product name
- 4-(bromomethyl)benzamide
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 214679
- Product name
- 4-(Bromomethyl)benzamide
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 214679
- Product name
- 4-(Bromomethyl)benzamide
- Purity
- 95+%
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- 089816
- Product name
- 4-(Bromomethyl)benzamide
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- 089816
- Product name
- 4-(Bromomethyl)benzamide
- Purity
- 95+%
- Packaging
- 1g
- Price
- $250
- Updated
- 2021/12/16
4-Bromomethylbenzamide Chemical Properties,Usage,Production
Synthesis
7719-09-7
6232-88-8
58914-40-2
1. Suspend p-bromomethylbenzoic acid (8.00 g, 37.2 mmol) in carbon tetrachloride (80 mL) under nitrogen protection with stirring. Sulfoxide chloride (6.8 mL, 93 mmol) was added slowly. 2. The reaction mixture was heated to reflux for 95 hours. Upon completion of the reaction, the reaction mixture was concentrated by rotary evaporator under reduced pressure to remove solvent and unreacted sulfoxide chloride. 3. The concentrated residue was dissolved in dichloromethane (150 mL) and ammonia (NH3) was passed through for 10 minutes and a yellowish precipitate was observed to form. 4. 5% aqueous sodium bicarbonate solution (70 mL) was added to the reaction mixture with vigorous stirring and the precipitate was collected by filtration. 5. The precipitate was washed with deionized water and subsequently dried under reduced pressure at 60 °C to afford 4-(bromomethyl)benzamide as a colorless solid (7.35 g, 92% yield).
References
[1] Patent: US6750348, 2004, B1. Location in patent: Page column 110
4-Bromomethylbenzamide Preparation Products And Raw materials
Raw materials
Preparation Products
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