ChemicalBook > CAS DataBase List > 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
- Product Name
- 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
- CAS No.
- 4664-00-0
- Chemical Name
- 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
- Synonyms
- NSC 405554;AKOS 93366;QUINOLINIMIDE;3-azaphthalimid;Moxifloxacin Imp.X;QUINOLINICACIDAMIDE;quinolinicacidimide;pyridinedicarboxamide;2,3-Pyridinedicarbimide;Pyridine-2,3-dicarbimide
- CBNumber
- CB4463896
- Molecular Formula
- C7H4N2O2
- Formula Weight
- 148.12
- MOL File
- 4664-00-0.mol
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5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Property
- Melting point:
- 233-234°C
- Boiling point:
- 268.69°C (rough estimate)
- Density
- 1.4015 (rough estimate)
- refractive index
- 1.5300 (estimate)
- storage temp.
- Refrigerator
- solubility
- Dichloromethane, Ether, Ethyl Acetate, Methanol
- pka
- 8.08±0.20(Predicted)
- form
- Solid
- color
- Brown
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N-Bromosuccinimide Price
TRC
- Product number
- Q711500
- Product name
- Quinolinimide
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
AK Scientific
- Product number
- 6385AB
- Product name
- 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
- Packaging
- 5g
- Price
- $164
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 157822
- Product name
- 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
- Packaging
- 0.500g
- Price
- $240
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 157822
- Product name
- 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
- Packaging
- 1g
- Price
- $300
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- CHM0069556
- Product name
- 2,3-PYRIDINEDICARBOXIMIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $721.57
- Updated
- 2021/12/16
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5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Chemical Properties,Usage,Production
Chemical Properties
Light yellow solid
Uses
Quinolinimide (cas# 4664-00-0) is a compound useful in organic synthesis.
Synthesis
89-00-9
4664-00-0
General procedure for the synthesis of 2,3-pyridinedicarboximide from 2,3-pyridinedicarboxylic acid: 167 g of 2,3-pyridinedicarboxylic acid (1.0 mol) and 300 mL of concentrated ammonia (28%) were added to a 1000 mL three-necked flask, followed by refluxing and stirring for 6 hours at 140 °C. The reaction was carried out in a liquid mixture of 2,3-pyridinedicarboxylic acid (1.0 mol) and 300 mL of concentrated ammonia (28%). During the reaction, the liquid reaction mixture gradually changed to dark brown color. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the complete reaction of 2,3-pyridinedicarboxylic acid, the reaction mixture was cooled to room temperature. Under continuous stirring, the reaction mixture was slowly poured into 500 mL of cold water, and a large amount of gray solid precipitated immediately. The solid product was collected by filtration and the filter cake was washed with cold water and subsequently dried under vacuum at 60 °C overnight to give 125 g of gray powdery product in 84% yield.
References
[1] Patent: CN102746294, 2016, B. Location in patent: Paragraph 0077; 0078
[2] Heterocycles, 2002, vol. 57, # 10, p. 1881 - 1890
[3] Bioorganic and Medicinal Chemistry, 2001, vol. 9, # 8, p. 2061 - 2071
[4] European Journal of Medicinal Chemistry, 2012, vol. 55, p. 58 - 66,9
[5] Molecules, 2000, vol. 5, # 3, p. 481 - 482
5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione manufacturers
Dideu Industries Group Limited
- Product
- QUINOLINIMIDE 4664-00-0
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-26
Career Henan Chemical Co
- Product
- QUINOLINIMIDE 4664-00-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-03
4664-00-0, 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dioneRelated Search:
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