ChemicalBook > CAS DataBase List > 3-Iodopyridin-2-amine

3-Iodopyridin-2-amine

Product Name
3-Iodopyridin-2-amine
CAS No.
104830-06-0
Chemical Name
3-Iodopyridin-2-amine
Synonyms
3-iodo-2-aMinopyridine;3-IODOPYRIDIN-2-AMINE;3-Iodopyrid-2-ylaMine;3-IODO-2-PYRIDINAMINE;2-AMINO-3-IODOPYRIDINE;2-Pyridinamine, 3-iodo-;3-IODO-PYRIDIN-2-YLAMINE;2-Amino-3-iodopyridine >2-Amino-3-iodopyridine,98%;2-Amino-3-iodopyridine 97%
CBNumber
CB4704524
Molecular Formula
C5H5IN2
Formula Weight
220.01
MOL File
104830-06-0.mol
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3-Iodopyridin-2-amine Property

Melting point:
87-91 °C
Boiling point:
289.6±25.0 °C(Predicted)
Density 
2.055±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
soluble in Methanol
pka
4.50±0.36(Predicted)
form 
Powder, Crystalline Powder or Needles
color 
White to pale brown
Sensitive 
Air & Light Sensitive
InChI
InChI=1S/C5H5IN2/c6-4-2-1-3-8-5(4)7/h1-3H,(H2,7,8)
InChIKey
UUDNBWSHTUFGDQ-UHFFFAOYSA-N
SMILES
C1(N)=NC=CC=C1I
CAS DataBase Reference
104830-06-0(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
22-37/38-41
Safety Statements 
26-39
WGK Germany 
2
HazardClass 
IRRITANT
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
704474
Product name
2-Amino-3-iodopyridine
Purity
96%
Packaging
5g
Price
$79.8
Updated
2023/06/20
TCI Chemical
Product number
A2542
Product name
2-Amino-3-iodopyridine
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$29
Updated
2025/07/31
TCI Chemical
Product number
A2542
Product name
2-Amino-3-iodopyridine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$89
Updated
2025/07/31
TRC
Product number
I719433
Product name
3-Iodopyridin-2-amine
Packaging
250mg
Price
$55
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA32708
Product name
2-Amino-3-iodopyridine
Packaging
1g
Price
$60
Updated
2021/12/16
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3-Iodopyridin-2-amine Chemical Properties,Usage,Production

Chemical Properties

Light yellow Needles

Uses

2-Amino-3-iodopyridine (3-Iodopyridin-2-amine) can be coupled with formyl derivatives under a copper-catalyzed indole synthesis method, and then constructed azide analogs through copper-mediated conjugated adducts things. The nucleophilicity of 2-Amino-3-iodopyridine is lower than that of the corresponding aniline used in the synthesis of indole, a potential obstacle for future synthesis[1].

Synthesis

113975-31-8

104830-06-0

General procedure for the synthesis of 2-amino-3-iodopyridine from N-(3-iodopyridin-2-yl)palmitamide: N-(3-iodopyridin-2-yl)neopentanamide (13.80 g, 45.36 mmol) was dissolved in 24 wt% sulfuric acid solution (394 mL), and the reaction mixture was stirred for 60 min under reflux conditions. After completion of the reaction, it was cooled to room temperature and neutralized with 4N sodium hydroxide solution and solid sodium bicarbonate. The aqueous phase was extracted with dichloromethane (3 x 200 mL), the organic phases were combined and dried over anhydrous magnesium sulfate. After filtration, the solvent was removed by rotary evaporator to give 3-iodopyridin-2-amine (9.70 g, 97% yield) as a cream colored solid.

References

[1] Patent: US2009/156593, 2009, A1. Location in patent: Page/Page column 17
[2] Patent: US2006/183758, 2006, A1. Location in patent: Page/Page column 8
[3] Patent: US2009/82403, 2009, A1. Location in patent: Page/Page column 51
[4] Patent: US2007/105904, 2007, A1. Location in patent: Page/Page column 53
[5] Patent: US2010/331282, 2010, A1. Location in patent: Page/Page column 10

3-Iodopyridin-2-amine Preparation Products And Raw materials

Raw materials

Ethanol Potassium hydroxide Potassium iodide 2-Chloro-3-pyridinamine Sodium sulfite Potassium carbonate Chloroform Sodium nitrite Hydrochloric acid Ammonia

Preparation Products

2-AMINO-3,5-DIIODOPYRIDINE
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View Lastest Price from 3-Iodopyridin-2-amine manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
3-Iodopyridin-2-amine 104830-06-0
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-09-29
PNP Biotech Co. Ltd
Product
2-Amino-3-iodopyridine 104830-06-0
Price
US $0.00/kg
Min. Order
25kg
Purity
98%
Supply Ability
Inquiry
Release date
2023-07-04
Dideu Industries Group Limited
Product
3-Iodopyridin-2-amine 104830-06-0
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-01

104830-06-0, 3-Iodopyridin-2-amineRelated Search:

Triethylamine 2-Chloro-3-hydroxypyridine N-Ethylmethylamine 4-Dimethylaminopyridine Triethanolamine Dibenzylamine 3-Hydroxypyridine 2-Aminopyridine 3-Aminopyridine Bis(2-ethylhexyl)amine 2-AMINO-3,5-DIIODOPYRIDINE 3-IODO-2-NITROPYRIDINE 1-(3-IODO-PYRIDIN-2-YL)-PIPERAZINE 5-Bromo-3-iodopyridin-2-amine N-CYCLOPROPYL-3-IODOPYRIDIN-2-AMINE 2-AMINO-3-IODO-5-NITROPYRIDINE 2-Amino-3-iodo-6-methylpyridine 4-(3-IODO-PYRIDIN-2-YL)-MORPHOLINE

  • 3-IODOPYRIDIN-2-AMINE
  • 3-IODO-PYRIDIN-2-YLAMINE
  • 2-Amino-3-iodopyridine 97%
  • 3-IODO-PYRIDIN-2-YLAMINE,98%
  • 3-iodo-2-aMinopyridine
  • 3-Iodopyrid-2-ylaMine
  • 2-Amino-3-iodopyridine,98%
  • 2-AMINO-3-IODOPYRIDINE
  • 2-Amino-3-iodopyridine &gt
  • 2-Pyridinamine, 3-iodo-
  • 3-Iodopyridin-2-amine ISO 9001：2015 REACH
  • 3-IODO-2-PYRIDINAMINE
  • 2-Amino-3-iodopyridine, 95%
  • 104830-06-0
  • 104830-06
  • 104803-06-0
  • Boronic Acid
  • Amines
  • Pyridines
  • Pyridine
  • Amines and Anilines
  • Heterocycles