ChemicalBook > CAS DataBase List > 2-Fluoro-5-nitroanisole

2-Fluoro-5-nitroanisole

Product Name
2-Fluoro-5-nitroanisole
CAS No.
454-16-0
Chemical Name
2-Fluoro-5-nitroanisole
Synonyms
2-Fluoro-5-nitroanisole;2-Fluoro-5-nitroasinole;4-Fluoro-3-methoxynitrobenzene;3-Methoxy-4-fluoronitrobenzene;Anisole, 2-fluoro-5-nitro- (8CI);1-Fluoro-2-methoxy-4-nitrobenzene;Benzene, 1-fluoro-2-methoxy-4-nitro-;4-Fluoro-3-methoxynitrobenzene 2-Fluoro-5-nitroanisole;2-Fluoro-5-nitroanisole[4-Fluoro-3-Methoxynitrobenzene];4-Fluoro-3-methoxynitrobenzene, 1-Fluoro-2-methoxy-4-nitrobenzene, 2-Fluoro-5-nitrophenyl methyl ether
CBNumber
CB51466501
Molecular Formula
C7H6FNO3
Formula Weight
171.13
MOL File
454-16-0.mol
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2-Fluoro-5-nitroanisole Property

Melting point:
69-71 °C
Boiling point:
270.3±20.0 °C(Predicted)
Density 
1.321±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), Methanol (Slightly)
form 
Solid
color 
Light Yellow to Yellow
InChI
InChI=1S/C7H6FNO3/c1-12-7-4-5(9(10)11)2-3-6(7)8/h2-4H,1H3
InChIKey
AZNKKZHZGDZSIF-UHFFFAOYSA-N
SMILES
C1(F)=CC=C([N+]([O-])=O)C=C1OC
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Safety

Hazard Codes 
Xi
HS Code 
2909309090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
F597580
Product name
2-Fluoro-5-nitroanisole
Packaging
500mg
Price
$60
Updated
2021/12/16
TRC
Product number
F597580
Product name
2-Fluoro-5-nitroanisole
Packaging
1g
Price
$70
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-3-69
Product name
2-Fluoro-5-nitroanisole
Purity
97%
Packaging
2g
Price
$10
Updated
2021/12/16
AK Scientific
Product number
J98486
Product name
2-Fluoro-5-nitroanisole
Packaging
1g
Price
$10
Updated
2021/12/16
AK Scientific
Product number
X0181
Product name
2-Fluoro-5-nitroanisole
Packaging
1g
Price
$14
Updated
2021/12/16
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2-Fluoro-5-nitroanisole Chemical Properties,Usage,Production

Synthesis

22510-08-3

74-88-4

454-16-0

GENERAL STEPS: Potassium carbonate (K2CO3, 5.27 g, 38.1 mmol) was added to a solution of 2-fluoro-5-nitrophenol (5.0 g, 31.84 mmol) in N,N-dimethylformamide (DMF, 50 mL), and the mixture was stirred for 15 minutes at room temperature. Subsequently, iodomethane (3 mL, 47.7 mmol) was added and the reaction mixture continued to be stirred for 2 hours at room temperature. Upon completion of the reaction, the mixture was poured into ice water and the solid product was isolated by filtration. The solid was washed well with deionized water and subsequently dried under vacuum to afford the off-white solid product 2-fluoro-5-nitroanisole (4.0 g, 73.5% yield). The structure of the product was confirmed by 1H NMR (300 MHz, CDCl3): δ 7.89-7.84 (m, 2H), 7.25-7.17 (m, 1H), 3.98 (s, 3H).

References

[1] Patent: WO2015/104653, 2015, A1. Location in patent: Page/Page column 57
[2] Patent: US2016/368906, 2016, A1. Location in patent: Paragraph 0229
[3] Patent: US2014/57911, 2014, A1. Location in patent: Paragraph 0635

2-Fluoro-5-nitroanisole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Fluoro-5-nitroanisole manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2-Fluoro-5-nitroanisole 454-16-0
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2025-03-10
R&D Scientific Inc.
Product
2-Fluoro-5-nitroanisole 454-16-0
Price
US $890.00/g
Min. Order
1g
Purity
98
Supply Ability
5000 Kg
Release date
2025-04-07
Shaanxi Dideu Medichem Co. Ltd
Product
2-Fluoro-5-nitroanisole 454-16-0
Price
US $0.00-0.00/KG
Min. Order
10mg
Purity
99%HPLC
Supply Ability
2000tons
Release date
2020-01-19

454-16-0, 2-Fluoro-5-nitroanisoleRelated Search:

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  • 2-Fluoro-5-nitroanisole
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  • 1-Fluoro-2-methoxy-4-nitrobenzene
  • Anisole, 2-fluoro-5-nitro- (8CI)
  • 4-Fluoro-3-methoxynitrobenzene, 1-Fluoro-2-methoxy-4-nitrobenzene, 2-Fluoro-5-nitrophenyl methyl ether
  • 2-Fluoro-5-nitroanisole[4-Fluoro-3-Methoxynitrobenzene]
  • Benzene, 1-fluoro-2-methoxy-4-nitro-
  • 2-Fluoro-5-nitroasinole
  • 4-Fluoro-3-methoxynitrobenzene 2-Fluoro-5-nitroanisole
  • 454-16-0
  • 445-93-6
  • Multisubstituted Benzene
  • Aromatic Halides (substituted)