Benzyl 2-methylpiperidine-1,2-dicarboxylate
- Product Name
- Benzyl 2-methylpiperidine-1,2-dicarboxylate
- CAS No.
- 180609-56-7
- Chemical Name
- Benzyl 2-methylpiperidine-1,2-dicarboxylate
- Synonyms
- N-Cbz-piperidine-2-carboxylate;Methyl 1-Cbz-piperidine-2-carboxylate;Benzyl 2-methylpiperidine-1,2-dicarboxylate;1-benzyl 2-methyl piperidine-1,2-dicarboxylate;1,2-Piperidinedicarboxylic acid 2-methyl-1-(phenylmethyl)ester
- CBNumber
- CB51563897
- Molecular Formula
- C15H19NO4
- Formula Weight
- 277.32
- MOL File
- 180609-56-7.mol
Benzyl 2-methylpiperidine-1,2-dicarboxylate Property
- Boiling point:
- 390.4±42.0 °C(Predicted)
- Density
- 1.187
- storage temp.
- Sealed in dry,Room Temperature
- pka
- -3.33±0.40(Predicted)
- Appearance
- Light yellow to yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M339075
- Product name
- MethylN-Cbz-piperidine-2-carboxylate
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- X0396
- Product name
- Methyl-N-Cbz-piperidine-2-carboxylate
- Packaging
- 100g
- Price
- $483
- Updated
- 2021/12/16
- Product number
- CHM0096319
- Product name
- METHYL N-CBZ-PIERIDINE-2-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.77
- Updated
- 2021/12/16
- Product number
- X0396
- Product name
- Methyl-N-Cbz-piperidine-2-carboxylate
- Packaging
- 1g
- Price
- $62
- Updated
- 2021/12/16
- Product number
- A212019
- Product name
- MethylN-Cbz-piperidine-2-carboxylate
- Purity
- 97%
- Packaging
- 1g
- Price
- $6
- Updated
- 2021/12/16
Benzyl 2-methylpiperidine-1,2-dicarboxylate Chemical Properties,Usage,Production
Synthesis
28697-07-6
74-88-4
180609-56-7
Example 36; 2-(2-methylpiperidin-2-yl)-1H-benzimidazole-4-carboxamide; Example 36A; 1-Benzyl-2-methylpiperidine-1,2-dicarboxylate. 1-[(Benzyloxy)carbonyl]piperidine-2-carboxylic acid (5 g) and iodomethane (2.5 mL) were dissolved in DMF (40 mL), potassium bicarbonate (3.8 g) was added, and the reaction mixture was stirred for 18 hours at room temperature. Upon completion of the reaction, the reaction mixture was concentrated and the residue was partitioned between ethyl acetate and water. The organic phase was separated, concentrated and the residue was purified by fast chromatography (silica gel, ethyl acetate/hexane as eluent) to give Example 36A (4.88 g, yield: 93%). The mass spectrum (DCI/NH3) showed m/z 278 (M + H)+.
References
[1] Patent: US2006/229289, 2006, A1. Location in patent: Page/Page column 20-21
Benzyl 2-methylpiperidine-1,2-dicarboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
Benzyl 2-methylpiperidine-1,2-dicarboxylate Suppliers
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View Lastest Price from Benzyl 2-methylpiperidine-1,2-dicarboxylate manufacturers
- Product
- Benzyl 2-methylpiperidine-1,2-dicarboxylate 180609-56-7
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- JD 458
- Release date
- 2019-09-01