7-BroMo-quinoline-3-carbonitrile
- Product Name
- 7-BroMo-quinoline-3-carbonitrile
- CAS No.
- 1375108-40-9
- Chemical Name
- 7-BroMo-quinoline-3-carbonitrile
- Synonyms
- 7-BroMo-quinoline-3-carbonitrile;7-methylquinoline-3-carbonitrile;3-Quinolinecarbonitrile, 7-bromo-
- CBNumber
- CB52611069
- Molecular Formula
- C10H5BrN2
- Formula Weight
- 233.06
- MOL File
- 1375108-40-9.mol
7-BroMo-quinoline-3-carbonitrile Property
- Boiling point:
- 379.7±22.0 °C(Predicted)
- Density
- 1.66±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 0.14±0.25(Predicted)
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 9276DT
- Product name
- 7-Bromoquinoline-3-carbonitrile
- Packaging
- 100mg
- Price
- $455
- Updated
- 2021/12/16
- Product number
- CD11269593
- Product name
- 7-Bromoquinoline-3-carbonitrile
- Purity
- 97%
- Packaging
- 250mg
- Price
- $223
- Updated
- 2021/12/16
- Product number
- CM144385
- Product name
- 7-bromoquinoline-3-carbonitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $526
- Updated
- 2021/12/16
- Product number
- CD11269593
- Product name
- 7-Bromoquinoline-3-carbonitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $557
- Updated
- 2021/12/16
- Product number
- 1375108409
- Product name
- 7-Bromoquinoline-3-carbonitrile
- Packaging
- 1g
- Price
- $579.89
- Updated
- 2021/12/16
7-BroMo-quinoline-3-carbonitrile Chemical Properties,Usage,Production
Synthesis
2032-34-0
59278-65-8
1375108-40-9
3,3-Diethoxypropionitrile (1.80 mL, 12.00 mmol), 2-amino-4-bromobenzaldehyde (2 g, 10.00 mmol) and p-toluenesulfonic acid monohydrate (0.380 g, 2.000 mmol) were mixed in toluene (30 mL). The reaction mixture was heated under reflux conditions for 3 hours by a Dean-Stark apparatus. After completion of the reaction, it was cooled to room temperature and the solvent was removed by evaporation under reduced pressure. The residue was dissolved in a small amount of DMF, diluted with chloroform and washed sequentially with water and sodium bicarbonate solution. The aqueous layer was extracted with chloroform, the organic phases were combined, washed with brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. Purification by fast column chromatography (eluent: dichloromethane/methanol, 0-3%) and the resulting product was ground in ether to give 7-bromo-3-cyanoquinoline (1.75 g, 75% yield).1H NMR (400 MHz, DMSO-d6) δ ppm: 7.95 (dd, J = 8.72, 1.89 Hz, 1H), 8.08 (d, J = 8.84 Hz, 1H), 8.38 (d, J = 2.02 Hz, 1H), 9.13 (d, J = 1.52 Hz, 1H), 9.21 (d, 1H).
References
[1] Patent: WO2013/28447, 2013, A1. Location in patent: Page/Page column 119-120
[2] Patent: WO2013/52716, 2013, A1. Location in patent: Page/Page column 50; 65
[3] Patent: WO2013/177253, 2013, A2. Location in patent: Page/Page column 61
[4] Patent: WO2014/8223, 2014, A2. Location in patent: Page/Page column 73
7-BroMo-quinoline-3-carbonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 7-BroMo-quinoline-3-carbonitrile manufacturers
- Product
- 7-BroMo-quinoline-3-carbonitrile 1375108-40-9
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 200g
- Release date
- 2020-02-01