7-BroMo-quinoline-3-carbonitrile

Product Name: 7-BroMo-quinoline-3-carbonitrile
CAS No.: 1375108-40-9
Chemical Name: 7-BroMo-quinoline-3-carbonitrile
Synonyms: 7-BroMo-quinoline-3-carbonitrile;7-methylquinoline-3-carbonitrile;3-Quinolinecarbonitrile, 7-bromo-
CBNumber: CB52611069
Molecular Formula: C10H5BrN2
Formula Weight: 233.06
MOL File: 1375108-40-9.mol

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7-BroMo-quinoline-3-carbonitrile Property

Boiling point:: 379.7±22.0 °C(Predicted)
Density: 1.66±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 0.14±0.25(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 9276DT
Product name: 7-Bromoquinoline-3-carbonitrile
Packaging: 100mg
Price: $455
Updated: 2021/12/16

Chemenu

Product number: CM144385
Product name: 7-bromoquinoline-3-carbonitrile
Purity: 97%
Packaging: 1g
Price: $526
Updated: 2021/12/16

Crysdot

Product number: CD11269593
Product name: 7-Bromoquinoline-3-carbonitrile
Purity: 97%
Packaging: 1g
Price: $557
Updated: 2021/12/16

Alichem

Product number: 1375108409
Product name: 7-Bromoquinoline-3-carbonitrile
Packaging: 1g
Price: $579.89
Updated: 2021/12/16

Abosyn

Product number: 61-10264
Product name: 7-Bromoquinoline-3-carbonitrile
Purity: 95-98%
Packaging: 1g
Price: $675
Updated: 2021/12/16

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7-BroMo-quinoline-3-carbonitrile Chemical Properties,Usage,Production

Synthesis

2032-34-0

59278-65-8

1375108-40-9

3,3-Diethoxypropionitrile (1.80 mL, 12.00 mmol), 2-amino-4-bromobenzaldehyde (2 g, 10.00 mmol) and p-toluenesulfonic acid monohydrate (0.380 g, 2.000 mmol) were mixed in toluene (30 mL). The reaction mixture was heated under reflux conditions for 3 hours by a Dean-Stark apparatus. After completion of the reaction, it was cooled to room temperature and the solvent was removed by evaporation under reduced pressure. The residue was dissolved in a small amount of DMF, diluted with chloroform and washed sequentially with water and sodium bicarbonate solution. The aqueous layer was extracted with chloroform, the organic phases were combined, washed with brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. Purification by fast column chromatography (eluent: dichloromethane/methanol, 0-3%) and the resulting product was ground in ether to give 7-bromo-3-cyanoquinoline (1.75 g, 75% yield).1H NMR (400 MHz, DMSO-d6) δ ppm: 7.95 (dd, J = 8.72, 1.89 Hz, 1H), 8.08 (d, J = 8.84 Hz, 1H), 8.38 (d, J = 2.02 Hz, 1H), 9.13 (d, J = 1.52 Hz, 1H), 9.21 (d, 1H).

References

[1] Patent: WO2013/28447, 2013, A1. Location in patent: Page/Page column 119-120
[2] Patent: WO2013/52716, 2013, A1. Location in patent: Page/Page column 50; 65
[3] Patent: WO2013/177253, 2013, A2. Location in patent: Page/Page column 61
[4] Patent: WO2014/8223, 2014, A2. Location in patent: Page/Page column 73

7-BroMo-quinoline-3-carbonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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7-BroMo-quinoline-3-carbonitrile Suppliers

China 38 India 1 United States 2 Global 41

Shijiazhuang Sdyano Fine Chemical Co., Ltd.

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Aikon International Limited

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View Lastest Price from 7-BroMo-quinoline-3-carbonitrile manufacturers

Career Henan Chemical Co

Product: 7-BroMo-quinoline-3-carbonitrile 1375108-40-9
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 200g
Release date: 2020-02-01

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1375108-40-9