4-Methyl-3-nitrobenzoic acid methyl ester

Synthesis

Product Name: 4-Methyl-3-nitrobenzoic acid methyl ester
CAS No.: 7356-11-8
Chemical Name: 4-Methyl-3-nitrobenzoic acid methyl ester
Synonyms: NSC29086;NSC 29086;ST5331831;ZINC01651943;632171_ALDRICH;EINECS 230-886-6;RARECHEM AL BF 0233;Telmisartan Impurity 29;METHYL 4-METHYL-3-NITROBENZOATE;METHYL 3-NITRO-4-METHYLBENZOATE
CBNumber: CB5337101
Molecular Formula: C9H9NO4
Formula Weight: 195.17
MOL File: 7356-11-8.mol

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4-Methyl-3-nitrobenzoic acid methyl ester Property

Melting point:: 49-53°C
Boiling point:: 298.0±20.0 °C(Predicted)
Density: 1?+-.0.06 g/cm3(Predicted)
Flash point:: 110 °C
storage temp.: Sealed in dry,Room Temperature
solubility: Soluble in methanol.
form: powder to crystal
color: White to Light yellow
CAS DataBase Reference: 7356-11-8(CAS DataBase Reference)
EPA Substance Registry System: Benzoic acid, 4-methyl-3-nitro-, methyl ester (7356-11-8)

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Safety

Hazard Codes: Xn
Risk Statements: 22-43
Safety Statements: 37/39
WGK Germany: 2
TSCA: Yes
HS Code: 29163990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 632171
Product name: Methyl 4-methyl-3-nitrobenzoate
Packaging: 5g
Price: $69
Updated: 2023/06/20

TCI Chemical

Product number: M2146
Product name: Methyl 4-Methyl-3-nitrobenzoate
Purity: >98.0%(GC)
Packaging: 5g
Price: $40
Updated: 2024/03/01

TCI Chemical

Product number: M2146
Product name: Methyl 4-Methyl-3-nitrobenzoate
Purity: >98.0%(GC)
Packaging: 25g
Price: $115
Updated: 2024/03/01

Alfa Aesar

Product number: B25299
Product name: Methyl 4-methyl-3-nitrobenzoate, 99%
Packaging: 5g
Price: $39
Updated: 2021/12/16

Alfa Aesar

Product number: B25299
Product name: Methyl 4-methyl-3-nitrobenzoate, 99%
Packaging: 25g
Price: $135
Updated: 2021/12/16

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4-Methyl-3-nitrobenzoic acid methyl ester Chemical Properties,Usage,Production

Synthesis

Methyl 4-methyl-3-nitrobenzoate is synthesized by the following steps:Acid 33 (100 g, 0.552 mol) was dissolved in MeOH (1000 ml). Conc. H2SO4 (30 ml) was added cautiously to this solution. The mixture was refluxed for 8 hours. Solvent was distilled off. Ice-cold water was added to the residue. It was then extracted with EtOAc, washed with NaHCO3 solution, water, dried (anhydrous Na2SO4), filtered and concentrated in vacuo to furnish faint yellow a solid. (91.57 g).

Chemical Properties

White solid

Uses

Methyl 4-methyl-3-nitrobenzoate is used as pharmaceutical intermediate.

4-Methyl-3-nitrobenzoic acid methyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

1-TERT-BUTYL 6-METHYL 3-FORMYL-1H-INDOLE-1,6-DICARBOXYLATE Indole-6-carboxaldehyde 6-HYDROXYMETHYLINDOLE

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4-Methyl-3-nitrobenzoic acid methyl ester Suppliers

Americas 1 China 143 Europe 3 Germany 3 India 8 Japan 1 Switzerland 2 Ukraine 1 United Kingdom 6 United States 20 Global 188

J & K SCIENTIFIC LTD.

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Alfa Aesar

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Pure Chemistry Scientific Inc.

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View Lastest Price from 4-Methyl-3-nitrobenzoic acid methyl ester manufacturers

Asia Chem I and E (Jiangsu) Co Ltd

Product: 4-Methyl-3-nitrobenzoate 7356-11-8
Price: US $55.82/Kg/Drum
Min. Order: 25Kg/Drum
Purity: 99.00%HPLC
Supply Ability: 13tons/month
Release date: 2021-09-22

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4-Methyl-3-nitrobenzoic acid methyl ester 7356-11-8
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-11

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4-Methyl-3-nitrobenzoic acid methyl ester 7356-11-8
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

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7356-11-8

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1993077

356-11-8

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Esters

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Carbonyl Compounds

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Carbonyl Compounds

Chemical Synthesis

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