ChemicalBook > CAS DataBase List > 6-Quinolinecarbaldehyde

6-Quinolinecarbaldehyde

Product Name: 6-Quinolinecarbaldehyde
CAS No.: 4113-04-6
Chemical Name: 6-Quinolinecarbaldehyde
Synonyms: inecarbaL;AKOS AUF01714;AKOS BBS-00005338;6-Formylquinoline;6-quinolineMethanal;RARECHEM AK ML 0559;6-QUINOLINECARBALDEHYDE;QUINOLINE-6-CARBALDEHYDE;6-QUINOLINECARBOXALDEHYDE;QUINOLINE-6-CARBOXALDEHYDE
CBNumber: CB5408618
Molecular Formula: C10H7NO
Formula Weight: 157.17
MOL File: 4113-04-6.mol

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6-Quinolinecarbaldehyde Property

Melting point:: 74-75°C
Boiling point:: 314.3±15.0 °C(Predicted)
Density: 1.223±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: powder to crystal
pka: 4.13±0.10(Predicted)
color: White to Yellow to Green
CAS DataBase Reference: 4113-04-6(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38-36/38-36
Safety Statements: 26-37/39-36
HazardClass: IRRITANT
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: Q0097
Product name: 6-Quinolinecarboxaldehyde
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $110
Updated: 2025/07/31

TCI Chemical

Product number: Q0097
Product name: 6-Quinolinecarboxaldehyde
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $387
Updated: 2025/07/31

Frontier Specialty Chemicals

Product number: JK100124
Product name: 6-Quinolinecarbaldehyde
Purity: 97%
Packaging: 5g
Price: $421
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0027930
Product name: 6-QUINOLINECARBALDEHYDE
Purity: 95.00%
Packaging: 0.5G
Price: $770
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0027930
Product name: 6-QUINOLINECARBALDEHYDE
Purity: 95.00%
Packaging: 5G
Price: $1617
Updated: 2021/12/16

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6-Quinolinecarbaldehyde Chemical Properties,Usage,Production

Chemical Properties

white to light yellow powde

Synthesis

100516-88-9

4113-04-6

General procedure for the synthesis of quinoline-6-carbaldehyde from 6-hydroxymethylquinoline: method adapted from Meyers et al. (Meyers, A. G.; Zhong, B.; Movassaghi, M.; Kung, D. W.; Lanman, B. A.; Kwon, S. Tetrahedron Lett. 2000, 41, 1359-1362). Dess-Martin periodinane (2.57 g, 6.05 mmol) was added to a 0.28 M solution of 6-hydroxymethylquinoline (0.459 g, 2.88 mmol) in water-saturated dichloromethane (10 mL). The reaction mixture was stirred for 10 min and then dichloromethane (3 x 1 mL) was added in batches over 15 min. Subsequently, the reaction mixture was diluted with ether (10 mL) and 80% saturated aqueous sodium bicarbonate solution (10 mL) of sodium thiosulfate (7.87 g, 31.7 mmol) was added. The mixture was stirred rapidly for 45 minutes. The organic and aqueous layers were separated and the aqueous layer was extracted with ether (2 x 20 mL). The combined organic layers were washed sequentially with saturated aqueous sodium bicarbonate solution (30 mL), water (2 x 30 mL) and saturated sodium chloride solution (2 x 30 mL). The organic layer was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by column chromatography (30-60% ethyl acetate/hexane) to give 0.383 g (85%) of quinoline-6-carbaldehyde (S4a) as a white solid with a melting point of 76.2-76.5 °C. 1H NMR (400 MHz, CDCl3): δ 7.53 (dd, 1H, J = 4.4, 8.4 Hz), 8.18-8.23 (m, 2H ), 8.33 (dd, 1H, J = 2.0, 8.4 Hz), 8.36 (s, 1H), 9.05 (dd, 1H, J = 2.0, 4.4 Hz), 10.20 (s, 1H).13C NMR (100 MHz, CDCl3): δ 122.4, 126.8, 127.8, 130.9, 133.8, 134.4 , 137.6, 151.0, 153.3, 191.6. HRMS-FAB (m/z): calculated value of 157.0528 for [MH]+ C10H7NO; measured value of 157.0521.

References

[1] Patent: WO2004/7491, 2004, A1. Location in patent: Page 56
[2] Journal of the American Chemical Society, 2008, vol. 130, # 20, p. 6404 - 6410
[3] Patent: WO2009/75778, 2009, A2. Location in patent: Page/Page column 49; 50-51
[4] Patent: US2005/54670, 2005, A1. Location in patent: Page/Page column 27

6-Quinolinecarbaldehyde Preparation Products And Raw materials

Raw materials

Benzoyl peroxide N-Bromosuccinimide Sodium sulfate Sodium chloride XYLENE Glycerol Sodium iodide Carbon tetrachloride Benzene Ethyl acetate Methanol Sodium hydroxide Selenium dioxide p-Toluidine 6-Methylquinoline PETROLEUM ETHER Sulfuric acid

Preparation Products

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View Lastest Price from 6-Quinolinecarbaldehyde manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 6-Quinolinecarbaldehyde 4113-04-6
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-11-06

4113-04-6, 6-QuinolinecarbaldehydeRelated Search:

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RARECHEM AK ML 0559

QUINOLINE-6-CARBALDEHYDE

6-QUINOLINECARBALDEHYDE

6-QUINOLINECARBOXALDEHYDE

AKOS BBS-00005338

AKOS AUF01714

QUINOLINE-6-CARBOXALDEHYDE

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6-Quinolinecarbaldehyde ,97%

6-quinolineMethanal

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inecarbaL

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6-Quinolinecarbaldehyde ISO 9001：2015 REACH

4113-04-6

808379

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4112-04-6

4113-4-6

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