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3-Amino-1-adamantanol

Product Name
3-Amino-1-adamantanol
CAS No.
702-82-9
Chemical Name
3-Amino-1-adamantanol
Synonyms
3-AMINO-1-ADAMANTANOL;3-AMINOADAMANTAN-1-OL;3-Amino-1-admantanol;4-aminoadamantan-1-ol;3-Amino-1-Adamantanamine;3-Hydroxy-1-aminoadamantane;1-AMINO-3-HYDROXYADAMANTANE;C1oH17NO;AKOS BB-9784;CHEMBRDG-BB 4003530
CBNumber
CB5777891
Molecular Formula
C10H17NO
Formula Weight
167.25
MOL File
702-82-9.mol
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3-Amino-1-adamantanol Property

Melting point:
265 °C (dec.)(lit.)
Boiling point:
266.8±23.0 °C(Predicted)
Density 
1.252±0.06 g/cm3(Predicted)
Flash point:
230 °F
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Crystalline Powder
pka
15.07±0.40(Predicted)
color 
White to yellow
Water Solubility 
Soluble in organic solvents,insoluble in water.
InChI
InChI=1S/C10H17NO/c11-9-2-7-1-8(3-9)5-10(12,4-7)6-9/h7-8,12H,1-6,11H2
InChIKey
DWPIPTNBOVJYAD-UHFFFAOYSA-N
SMILES
C12(O)CC3CC(CC(N)(C3)C1)C2
CAS DataBase Reference
702-82-9(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29221990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
523690
Product name
3-Amino-1-adamantanol
Purity
96%
Packaging
1g
Price
$26
Updated
2024/03/01
Sigma-Aldrich
Product number
523690
Product name
3-Amino-1-adamantanol
Purity
96%
Packaging
5g
Price
$40
Updated
2024/03/01
TCI Chemical
Product number
A2079
Product name
3-Amino-1-adamantanol Hydrate
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$17
Updated
2024/03/01
TCI Chemical
Product number
A2079
Product name
3-Amino-1-adamantanol Hydrate
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$40
Updated
2024/03/01
Alfa Aesar
Product number
H64137
Product name
3-Amino-1-adamantanol, 98+%
Packaging
5g
Price
$48.65
Updated
2024/03/01
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3-Amino-1-adamantanol Chemical Properties,Usage,Production

Description

3-Amino-1-adamantanol is an important adamantane drug intermediate mainly used in the synthesis of inhibitors with antihyperglycaemic properties for the preparation of Vildagliptin, a dipeptidyl peptidase 4 (DPP-4) inhibitor used in the treatment of type 2 diabetes.

Chemical Properties

White solid

Uses

It is employed in the synthesis of inhibitors with antihyperglycemic properties. vil- dagliptin is synthesised from 3-Amino-1-adamantanol.

Uses

3-Amino-1-hydroxyadamantane can be employed in the synthesis of inhibitors with antihyperglycemic properties.

Uses

As reagent, 3-Amino-1-hydroxyadamantane can be used in the preparation of Vildagliptin.

Synthesis

A preparation method of 3-amino-1-adamantanol comprises the following steps: (1) adding amantadine or a salt thereof to sulfuric acid at 10-30 DEG C and adding a mixed acid dropwise to perform a nitration reaction to obtain a reaction liquid; (2) adding the reaction liquid to water and mixing the reaction liquid with water to obtain a mixed solution; (3) performing a hydroxylation reaction under the effect of alkaline to obtain the 3-amino-1-adamantanol. The preparation method employs the raw material, is easy to obtain, is simple in operations, is environmentally protective, is low in cost, and is high in yield, which is generally higher than 80%, maximally 90.1%.

3-Amino-1-adamantanol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Amino-1-adamantanol manufacturers

Hebei Zhuanglai Chemical Trading Co.,Ltd
Product
3-Amino-1-adamantanol 702-82-9
Price
US $40.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
5000kg/week
Release date
2024-05-17
Nanjing Fred Technology Co., Ltd
Product
3-Amino-1-hydroxyadamantane 702-82-9
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1 ton
Release date
2024-01-02
HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD
Product
3-Amino-1-adamantanol 702-82-9
Price
US $99.00-66.00/kg
Min. Order
0.0010000000474974513kg
Purity
99%
Supply Ability
5000
Release date
2024-08-19

702-82-9, 3-Amino-1-adamantanolRelated Search:


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  • 3-AMino-1-HydroxyadaMantane SynonyMs: 3-AMinoadaMantan-1-ol
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  • 3 - aMino adaMantane alcohol
  • 3-Amino-1-hydroxyadamantane 3-Aminoadamantan-1-ol
  • 3-Amino-1-adamantanol 3-Amino-1-adamantanol
  • 3-aminoadamantan-1-ol hydrochloride
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  • Vildagliptin Amino Alcohol ImpurityQ: What is Vildagliptin Amino Alcohol Impurity Q: What is the CAS Number of Vildagliptin Amino Alcohol Impurity Q: What is the storage condition of Vildagliptin Amino Alcohol Impurity Q: What are the applications of Vildagliptin Amino Alcohol Impurity
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  • C1oH17NO
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  • 3-Aminoadamantan-ol
  • 702-82-9
  • 02-82-9
  • 702-82-7
  • 702-89-2
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