tert-butyl(3-hydroxyphenethyl)carbamate

Product Name: tert-butyl(3-hydroxyphenethyl)carbamate
CAS No.: 129150-68-1
Chemical Name: tert-butyl(3-hydroxyphenethyl)carbamate
Synonyms: 3-[2-(Boc-amino)ethyl]phenol;tert-butyl(3-hydroxyphenethyl)carbamate;tert-Butyl N-(3-hydroxyphenethyl)carbamate;tert-butyl N-[2-(3-hydroxyphenyl)ethyl]carbamate;N-(t-butoxycarbonyl)-2-(3-hydroxyphenyl)-ethylamine;Carbamic acid, N-[2-(3-hydroxyphenyl)ethyl]-, 1,1-dimethylethyl ester
CBNumber: CB63144006
Molecular Formula: C13H19NO3
Formula Weight: 237.29
MOL File: 129150-68-1.mol

More

Less

tert-butyl(3-hydroxyphenethyl)carbamate Property

Boiling point:: 397.1±25.0 °C(Predicted)
Density: 1.100±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 9.98±0.10(Predicted)
Appearance: Off-white to light yellow Solid

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

AK Scientific

Product number: 1984AQ
Product name: tert-butyl3-hydroxyphenethylcarbamate
Packaging: 250mg
Price: $333.2
Updated: 2021/12/16

Chemenu

Product number: CM248716
Product name: tert-Butyl3-hydroxyphenethylcarbamate
Purity: 95+%
Packaging: 5g
Price: $880
Updated: 2021/12/16

Alichem

Product number: 129150681
Product name: tert-Butyl3-hydroxyphenethylcarbamate
Packaging: 5g
Price: $931.59
Updated: 2021/12/16

Ambeed

Product number: A101127
Product name: tert-Butyl3-hydroxyphenethylcarbamate
Purity: 97%
Packaging: 100mg
Price: $66
Updated: 2021/12/16

Crysdot

Product number: CD12155457
Product name: tert-Butyl3-hydroxyphenethylcarbamate
Purity: 97%
Packaging: 1g
Price: $265
Updated: 2021/12/16

More

Less

tert-butyl(3-hydroxyphenethyl)carbamate Chemical Properties,Usage,Production

Synthesis

132513-29-2

129150-68-1

Step B: Synthesis of tert-butyl [2-(3-hydroxyphenyl)ethyl]carbamate; 1 g of 10% Pd/C catalyst was added to a 100 mL ethanol solution containing 13 g (0.039 mol) of tert-butyl [2-(3-benzyloxyphenyl)ethyl]carbamate. The reaction mixture was subjected to hydrogenation at 40 psi hydrogen pressure overnight. Upon completion of the reaction, the catalyst was removed by filtration and washed with ethanol. Subsequently, the solvent was evaporated under reduced pressure to give 9.4 g of tert-butyl 3-hydroxyphenethylcarbamate as a colorless oil in quantitative yield.1H-NMR (CDCl3) δ: 7.22-7.12 (m, 1H); 6.78-6.66 (m, 3H); 4.56 (bs, 1H); 3.42-3.30 (m, 2H); 2.74 (t, 2H); 1.44 (s, 9H).

References

[1] Patent: WO2007/71311, 2007, A1. Location in patent: Page/Page column 55-56
[2] Patent: WO2014/95920, 2014, A1. Location in patent: Page/Page column 70
[3] Journal of Organic Chemistry, 1990, vol. 55, # 24, p. 6000 - 6017
[4] Patent: WO2009/68177, 2009, A1. Location in patent: Page/Page column 39
[5] Patent: US2010/210631, 2010, A1. Location in patent: Page/Page column 14

tert-butyl(3-hydroxyphenethyl)carbamate Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

tert-butyl(3-hydroxyphenethyl)carbamate Suppliers

China 22 India 1 United States 1 Global 24

Shanghai Raise Chemical Technology Co.,Ltd

Tel: 15026594951
Fax: 0556-5030632
Email: rs@raise-chem.com
Country: China
ProdList: 4454
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Nantong MYBio-pharm. Co., Ltd.

Tel: 0513-85921823 18662920231
Fax: 86-513-85012876
Email: sales@ntminyanmedical.com
Country: China
ProdList: 4107
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Amatek Scientific Co. Ltd.

Tel: 0512-56316828
Fax: 0512-56316826
Email: info@amateksci.com
Country: China
ProdList: 28785
Advantage: 58

Chengdu Feibai Pharmaceutical Co., Ltd.

Tel: 028-84641798 18782128315
Email: 3302391190@qq.com
Country: China
ProdList: 9799
Advantage: 55

Shanghai zhigan biotechnology co., LTD

Tel
Email: zhiqianbio@126.com
Country: China
ProdList: 19778
Advantage: 58

Jiangsu aikang biomedical research and development co., LTD

Tel: 025-58859352 13155353615
Email: qzhang@aikonchem.com
Country: China
ProdList: 15525
Advantage: 58

Nantong puyue biomedical Co., Ltd

Tel: 0513-0513-0513-89158300 18014392889
Fax: 0513-89158198
Email: sales@puyerbiopharma.com
Country: China
ProdList: 4956
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing1@energy-chemical.com
Country: China
ProdList: 44894
Advantage: 58

129150-68-1, tert-butyl(3-hydroxyphenethyl)carbamateRelated Search:

4-Hydroxyphenylacetic acid Benzeneacetic acid,4-nitro-, 1,1-dimethylethyl ester CARBAMIC ACID, (3-BROMO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER tert-butyl 6-broMonaphthalen-2-ylcarbaMate tert-Butyl 7-amino-1H-indole-1-carboxylate TERT-BUTYL 2-CYCLOHEXYLHYDRAZINECARBOXYLATE [1-(4-BROMO-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER 1-BOC-4-(CYANOACETYL)PIPERIDINE tert-Butyl 4-cyanobenzyl(methyl)carbamate TERT-BUTYL 4-CYANOBENZYLCARBAMATE Carbamic acid, (1,1-dimethyl-2-propynyl)-, 1,1-dimethylethyl ester (9CI) (3-BROMO-PYRIDIN-4-YL)-CARBAMIC ACID TERT-BUTYL ESTER Carbamic acid, (2-hydroxy-2-methylpropyl)-, 1,1-dimethylethyl ester (9CI) tert-butyl 3-bromo-2-hydroxyphenylcarbamate tert-butyl 3-hydroxy-4-methylphenylcarbamate tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate N-TERT-BUTOXYCARBONYL-2-METHYLAMINO-ETHYLAMINE X HCL

tert-butyl(3-hydroxyphenethyl)carbamate

N-(t-butoxycarbonyl)-2-(3-hydroxyphenyl)-ethylamine

3-[2-(Boc-amino)ethyl]phenol

Carbamic acid, N-[2-(3-hydroxyphenyl)ethyl]-, 1,1-dimethylethyl ester

tert-butyl N-[2-(3-hydroxyphenyl)ethyl]carbamate

tert-Butyl N-(3-hydroxyphenethyl)carbamate

129150-68-1